Advertisement

Síntesis del Cianoacrilato de n-butilo Asistida por Microondas

  • A. B. RubénEmail author
  • M. S. Ricardo
  • R. C. Yaquelin
Conference paper
Part of the IFMBE Proceedings book series (IFMBE, volume 33)

Abstract

Traditional synthesis of n-butylcyanoacrylate takes place heating n-butylcyanoacetate with paraformaldehyde in presence of toluene, acetic acid and pyperydine. Oligomers of n-butylcyanoacrylate were obtained as intermediary. They were isolated in some cases and pyrolyzed under vacuum with anionic and cationic inhibitors yielding n-butylcyanoacrylate. Traditional heating sources were used in the overall process which takes place proximately in 9 hours. The main goal of our work was the preparation of n-butylcyanoacrylate assisted by microwaves. A domestic microwave was used and the process was regulated by selecting an appropriate power.

Palabras claves

irradiación de microondas cianoacrilato de n-butilo policianoacrilato de n-butilo 

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

Copyright information

© Springer Berlin Heidelberg 2013

Authors and Affiliations

  • A. B. Rubén
    • 1
    Email author
  • M. S. Ricardo
    • 2
  • R. C. Yaquelin
    • 1
  1. 1.Facultad de QuímicaUniversidad de La HabanaCiudad de La HabanaCuba
  2. 2.Instituto de Ciencia y Tecnología de los MaterialesUniversidad de La HabanaCiudad de La HabanaCuba

Personalised recommendations