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The Use of Scattering and Spectroscopic Synchrotron Radiation Methods in Materials Science

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Applications of Synchrotron Light to Scattering and Diffraction in Materials and Life Sciences

Part of the book series: Lecture Notes in Physics ((LNP,volume 776))

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Abstract

Materials science is a very broad research field in which a variety of X-ray-based characterisation techniques play an important role in determining the structure of the materials under investigation. However, these techniques can also be used in many ways to determine the dynamic material properties and the influence that a variety of parameters can have on the final material properties during the manufacturing process. In many instances the high intensity and collimation of synchrotron radiation sources are beneficial, and often required, to obtain the desired information. This can be for instance the case in time-resolved X-ray scattering experiments but also in many imaging techniques where a low divergence but large beam size and tunable photon energy can render much better results compared to conventional X-ray sources. For X-ray spectroscopic techniques the tunability of the photon energy practically confines them at present to accelerator-based central laboratories. In this chapter an overview of some new developments and existing possibilities will be discussed. The main emphasis will be on X-ray scattering techniques on materials that evolve from an amorphous towards a more ordered state.

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References

  1. Bras W., Ryan A. J. Adv. Colloid Interface Sci. 75, 1 (1998).

    Google Scholar 

  2. Bark M., Zachmann H.G., Alamo R., et al. Makromol. Chem. Macromol. Chem. Phys. 193, 2363 (1992).

    Google Scholar 

  3. Bras W., Derbyshire G.E., Ryan A. J., et al. Nucl. Instrum. Methods Phys. Res. A-Accelerators Spectrometers Detectors and Associated Equipment 326, 587 (1993).

    Google Scholar 

  4. de Jager M.W., Gooris G.S., Dolbnya I.P., et al. Chem. Phys. Lipids 124, 123 (2003).

    Article  Google Scholar 

  5. Goderis B., Peeters M., Mathot V.B.F., et al. J. Polym. Sci. B Polym. Phys. 38, 1975 (2000).

    Article  ADS  Google Scholar 

  6. Polushkin E., van Ekenstein G.A., Dolbnya I., et al. Macromolecules 36, 1421 (2003).

    Article  ADS  Google Scholar 

  7. Greaves G.N., Sen S. Adv. Phys. 56, 1 (2007).

    Google Scholar 

  8. Smolsky I.L., Liu P., Niebuhr M., et al. J. Appl. Crystallogr. 40, S453 (2007).

    Article  Google Scholar 

  9. Bras W. J. Macromol. Sci. Phys. B37, 557 (1998).

    Article  Google Scholar 

  10. Narayanan T. , Diat O., Bosecke P., Nucl. Instrum. Methods Phys. Res. A-Accelerators Spectrometers Detectors And Associated Equipment 467, 1005 (2001).

    Google Scholar 

  11. Bras W., Derbyshire G.E., Devine A., et al. J. Appl. Crystallogr. 28, 26 (1995).

    Article  Google Scholar 

  12. Russell T.P., Koberstein J. T. J. Polym. Sci. B Polym. Phys. 23, 1109 (1985).

    Article  Google Scholar 

  13. Bryant G.K. , Gleeson H.F., Ryan A.J., et al. Rev. Sci. Instrum. 69, 2114 (1998).

    Article  ADS  Google Scholar 

  14. Bras W., Derbyshire G.E., Bogg D., et al. Science 267, 996 (1995).

    Article  ADS  Google Scholar 

  15. Jimenez-Ruiz M., Sanz A., Nogales A., et al. Rev. Sci. Instrum. 76 (2005).

    Google Scholar 

  16. Wurm A., Soliman R., Goossens J.G.P., et al. J. Non-Cryst. Solids 351, 2773 (2005).

    Article  ADS  Google Scholar 

  17. Broennimann C., Eikenberry E.F., Henrich B., et al. J. Synchrotron Radiat. 13, 120 (2006).

    Article  Google Scholar 

  18. Panine P., Finet S., Weiss T.M., et al. Adv. Colloid Interface Sci. 127, 9 (2006).

    Article  Google Scholar 

  19. Brown W., Mortensen K. Scattering in Polymeric and Colloidal Systems. Gordon and Breach (2000).

    Google Scholar 

  20. Bras W., Diakun G.P, Diaz J.F., et al. Biophys. J. 74, 1509 (1998).

    Article  ADS  Google Scholar 

  21. Keymeulen H.R., Diaz A., Solak H.H., et al. J. Appl. Phys. 102 (2007).

    Google Scholar 

  22. Mesu J.G., van der Eerden A.M.J., de Groot F.M.F., et al. J. Phys. Chem. B 109, 4042 (2005).

    Article  Google Scholar 

  23. Gommes C.J., Goderis B., Pirard J. P. J. Phys. Chem. C 111, 11150 (2007).

    Article  Google Scholar 

  24. Jensen H., Bremholm M., Nielsen R.P., et al. Angew. Chem. Int. Ed. 46, 1113 (2007).

    Article  Google Scholar 

  25. Pontoni D., Bolze J., Dingenouts N., et al. J. Phys. Chem. B 107, 5123 (2003).

    Article  Google Scholar 

  26. DiMasi E., Kwak S.Y., Amos F.F., et al. Phys. Rev. Lett. 97 (2006).

    Google Scholar 

  27. Bras W., Dolbnya I.P., Detollenaere D., et al. J. Appl. Crystallogr. 36, 791 (2003).

    Article  Google Scholar 

  28. Heeley E.L., Maidens A.V., Olmsted P.D., et al. Macromolecules 36, 3656 (2003).

    Article  ADS  Google Scholar 

  29. Michel F.M., Ehm L., Antao S.M., et al. Science 316, 1726 (2007).

    Article  ADS  Google Scholar 

  30. Chupas P.J., Chapman K.W, Jennings G., et al. J. Am. Chem. Soc. 129, 13822 (2007).

    Article  Google Scholar 

  31. Mesu J.G., Beale A.M. , de Groot F.MF., et al. J. Phys. Chem. B 110, 17671 (2006).

    Google Scholar 

  32. Als-Nielsen J., McMorrow D. Elements of Modern X-Ray Physics. Wiley (2001).

    Google Scholar 

  33. Petukhov A.V., Aarts D., Dolbnya I.P., et al. Phys. Rev. Lett. 88 (2002).

    Google Scholar 

  34. Dolbnya I.P., Petukhov A.V., Aarts D., et al. Europhys. Lett. 72, 962 (2005).

    Article  ADS  Google Scholar 

  35. Harada T., Matsuoka H. , Curr. Opin. Colloid Interface Sci. 8, 501 (2004).

    Article  Google Scholar 

  36. Willey T.M. , van Buuren T., Lee J.R.I. , et al. Propellants Explos. Pyrot. 31, 466 (2006).

    Google Scholar 

  37. Lengeler B., Schroer C.G. , Richwin M., et al. Appl. Phys. Lett. 74, 3924 (1999).

    Article  ADS  Google Scholar 

  38. Thijssen J.H.J., Petukhov A.V., Hart D.C.T., et al. Adv. Mater. 18, 1662 (2006).

    Article  Google Scholar 

  39. Petukhov A.V., van der Beek D., Dullens R.P.A., et al. Phys. Rev. Lett. 95 (2005).

    Google Scholar 

  40. Frings P., Vanacken J., Detlefs C., et al. Rev. Sci. Instrum. 77 (2006).

    Google Scholar 

  41. Irving T.C., Maughan D.W. Biophys. J. 78, 2511 (2000).

    Google Scholar 

  42. Howse J.R., Topham P., Crook C.J., et al. Nano Lett. 6, 73 (2006).

    Article  ADS  Google Scholar 

  43. Rabai G., Orban M., Epstein I.R., Acc. Chem. Res. 23, 258 (1990).

    Article  Google Scholar 

  44. Muthukumar M. In Interphases and Mesophases in Polymer Crystallization III, Vol. 191, p. 241 (2005).

    Article  Google Scholar 

  45. Ezquerra T.A., Sics I., Nogales A., et al. Europhys. Lett. 59, 417 (2002).

    Article  ADS  Google Scholar 

  46. Beale A.M., van der Eerden A.M.J., Jacques S.D.M. , et al. J. Am. Chem. Soc. 128, 12386 (2006).

    Article  Google Scholar 

  47. Avrami M. J. Chem. Phys. 7, 1103 (1939).

    ADS  Google Scholar 

  48. Bras W., Greaves G.N., Oversluizen M., et al. J. Non-Cryst. Solids 351, 2178 (2005).

    Article  ADS  Google Scholar 

  49. Cumming A., Wiltzius P., Bates F.S., et al. Phys. Rev. A 45, 885 (1992).

    Article  ADS  Google Scholar 

  50. Dent A.J., Oversluizen M., Greaves G.N., et al. Physica B 209, 253 (1995).

    ADS  Google Scholar 

  51. Megens M. , vanKats C.M., Bosecke P., et al. Langmuir 13, 6120 (1997).

    Article  Google Scholar 

  52. Vos W.L., Megens M., vanKats C.M., et al. Langmuir 13, 6004 (1997).

    Article  Google Scholar 

  53. Durville F., Champagnon B., Duval E., et al. Phys. Chem. Glasses 25, 126 (1984).

    Google Scholar 

  54. Goodisman J., Brumberger H. J. Appl. Crystallogr. 4, 347 (1971).

    Article  Google Scholar 

  55. Azin N.J., Camerucci M.A., Cavalieri A.L., Ceram. Int. 31, 189 (2005).

    Article  Google Scholar 

  56. Donald I. W. J. Mater. Sci. 30, 904 (1995).

    Article  ADS  Google Scholar 

  57. Bamford H., Tipper C. In Comprehensive Chemical Kinetics, Vol. 22 Chap. 3. H. Bamford and C. Tipper (Eds.), Elsevier, N.Y. (1980).

    Google Scholar 

  58. Wagner R., Kampmann R. In Materials Science and Technology, (Vol. 5). P. Haasen and E. J. Krames R.W. Cahn (Eds.), VCH (1991).

    Google Scholar 

  59. Rao P. , Doremus R. J. Non-Cryst. Solids 203, 202 (1996).

    Google Scholar 

  60. Diaz-Mora N., Zanotto E.D., Hergt R., et al. J. Non-Cryst. Solids 273, 81 (2000).

    Article  ADS  Google Scholar 

  61. Birch F. Phys. Rev. A 71, 809 (1947).

    Article  ADS  Google Scholar 

  62. Suzuki I. , Ohno I., Anderson O. L. Am. Mineral. 85, 304 (2000).

    Google Scholar 

  63. Martignago F., Negro A.D., Carbonin S. Phys. Chem. Mineral. 30, 401 (2003).

    Article  ADS  Google Scholar 

  64. Gilbert B., Huang F., Zhang H.Z., et al. Science 305, 651 (2004).

    Article  ADS  Google Scholar 

  65. Dubiel M., Schneider R., Hofmeister H., et al. Eur. Phys. J. D 43, 291 (2007).

    ADS  Google Scholar 

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Bras, W. (2009). The Use of Scattering and Spectroscopic Synchrotron Radiation Methods in Materials Science. In: Gomez, M., Nogales, A., Garcia-Gutierrez, M., Ezquerra, T. (eds) Applications of Synchrotron Light to Scattering and Diffraction in Materials and Life Sciences. Lecture Notes in Physics, vol 776. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-540-95968-7_5

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  • DOI: https://doi.org/10.1007/978-3-540-95968-7_5

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  • Online ISBN: 978-3-540-95968-7

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