Abstract
Instrumentation, data analysis, radiation damage, and related issues of synchrotron radiation micro- and nanodiffraction techniques applied to soft condensed matter science are reviewed in this chapter. The current instrumental capabilities at the ESRF-ID13 beamline provide beam sizes from a few microns into the range of 100 nm. A further reduction to about 30 nm can be expected. The reduction of beam size is accompanied by an increase in beam divergence, which limits the accessible lower Q-limit as compared to SAXS cameras with optimized resolution due to low-divergence beams. The availability of recursive data reduction routines allows the extraction of structural information from large 2D detector data sets.
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References
Sawyer L.C., Grubb D.T. Polymer Microscopy. Chapman&Hall,London (1996).
Riekel C. Rep. Prog. Phys. 63, 233 (2000).
Sawyer L.C., Chen R.T., Jamieson M.G., Musselman I.H., Russell P.E. J. Mat. Sci. 28, 225 (1993).
Müller M., Riekel C., Vuong R., Chanzy H. Polymer 41, 2627(2000).
Riekel C., Davies R. Curr. Opin. Colloid InterfaceSci. 9, 396 (2005).
Roth S.V., Burghammer M., Janotta A., Riekel C. Macromolecules 36, 1585 (2003).
Gebhardt R., Hanfland M., Mezouar M., Riekel C. Biomacromolecules 8, 2092 (2007).
Lemke H., Burghammer M., Flot D., Roessle M., Riekel C. Biomacromolecules 5, 1316 (2004).
Rubens P., Snauwaert J., Heremans K., Stute R.Carbohyd. Polym. 39, 231 (1999).
Hammersley A. In www.esrf.fr/computing/scientific/FIT2D/.
Davies R. J. Appl. Cryst. 39, 267 (2006).
Riekel C., Burghammer M., Schertler G. Curr. Opin. Struct. Biol. 15, 556 (2005).
Lichtenegger H., Müller M., Paris O., Riekel C., Fratzl P. J. Appl. Cryst. 32, 1127(1999).
Popov D., Burghammer M., Buleon A., Montesanti N., Putaux J.L., Riekel C. Macromolecules 39, 3704 (2006).
Imberty A., Chanzy H., Pérez S., Buléon A., Tran V. J. Mol. Biol.201, 365 (1988).
Hendrix J., Koch M., Bordas M. H. J. J. Appl. Cryst. 12, 467 (1979).
Rosenbaum G., Holmes K.C. InSynchrotron Radiation Research, pp 533. H. Winick and S.Doniach(Eds.) Plenum Press, New York (1980).
Riekel C., Burghammer M., Müller M. J. Appl. Cryst. 33, 421 (2000).
Engström P., Riekel C. J. Synchr. Rad. 3, 97 (1996).
Müller M., Burghammer M., Flot D., Riekel C., Morawe,C., Murphy B., Cedola A. J. Appl. Cryst. 33, 1231 (2000).
Noehammer B., David C., Burghammer M., Riekel C. Appl.Phys. Lett. 86, 163104 (2005).
Snigirev A.A., Snigireva I.I., Riekel C., MillerA., Wess L., Wess T. J. de Physique 3, 443 (1994).
Lengeler B., Schroer C.G., Benner B., Guenzler T.F., Kuhlmann M., Tuemmler J., Simionovici A.S., Drakopoulos M., Snigirev A., Snigireva I. Nucl. Instrum. Methods Phys. Res. A467–468, 944 (2001).
Schroer C.G., Kurapova O., Patommel J., Boye P., Feldkamp J., Lengeler B., Burghammer M., Riekel C., Vincze L. Hart A. v. d., Kuechler M. Appl. Phys. Lett.87, 124103 (2005).
Jark W., DiFonzo S., Lagomarsino S., Cedola A., Fabrizio E.D., Bram A., Riekel C. J. Appl. Phys. 80, 4831(1996).
Volkringer C., Popov D., Loiseau T., Guillou N., Ferey G., Haouas M., Taulelle F., Mellot-Draznieks C., Burghammer M., Riekel C. Nat. Mater. 6, 760 (2007).
Moukhametzianov R., Burghammer M., Edwards P., Fransen M., Petitdemange S., Popov D., Fransen M., McMullan G., Schertler G., Riekel C. Acta Cryst D. 64, 158 (2008).
Roth S.V., Burghammer M., Riekel C., Müller-Buschbaum P., Diethert A., Panagiotou P., Walter H. Appl. Phys. Lett. 82, 1935(2003).
Gebhardt R., Burghammer M., RiekelC., Roth S., Müeller-Buschbaum P. Macromol. Biosci. 8, 347(2008).
Kocsis M., Somogyi A. J. Synchotron Rad. 10, 187 (2003).
Davies R.J., Riekel C., Bennet J.A., Eichhorn S.J., Young R. J. Appl. Phys. Lett. 91, 044102 (2007).
Chanzy H., Putaux J.L., Dupeyre D., Davies R., Burghammer M., Montanari S., Riekel C. J. Struct. Biol. 154, 100 (2006).
Henderson, R. Proc. Roy. Soc. B 241, 6 (1990).
Nave C., Hill M. A. J. Synchotron Rad. 12,299 (2005).
Schoeck J., Davies R.J., Martel A., Riekel C. Biomacromolecules 8, 602 (2007).
Buléon A., Pontoire B., Riekel C., Chanzy H., Helbert W., Vuong R. Macromolecules 30, 3952 (1997).
Pfohl T., Mugele F., Seemann R., Herminghaus S. Chem. Phys. Chem. 4, 1291 (2003).
Cojoc D., Ferrari E., Garbin V., Fabrizio E. D., Amenitsch H., Rappolt M., Sartori B., Laggner P., Burghammer M., Riekel C. Appl. Phys. Lett. 91, 234107 (2007).
Paris O., Müller M. Nucl. Instrum. Methods Phys. Res. B 200, 390 (2003).
Davies R.J., Burghammer M., Riekel C. Macromolecules 40, 5038 (2007).
Koenig C., Burghammer M., Riekel C., Davies R. Appl. Phys. Lett. 92, 101903 (2008).
Seidel R., Gourrier A., Burghammer M., Riekel C., Jeronimidis G., Paris O. Micron, 39, 198 (2008).
Ludwig W., Lauridsen E.M., Schmidt S., Poulson H.F. , Baruchel J. J. Appl. Cryst. 40, 905 (2007).
Schroer C.G., Kuhlmann M., Roth S.V., Gehrke R., Stribeck N., Almendarez-Camerillo A., Lengeler, B. Appl. Phys. Lett. 88, 164102 (2006).
Cloetens P., Mache R., Schlenker M., Lerbs-Mache L. Proc. Natl. Acad. Sci. USA103, 14626 (2006).
DiFonzo S., Jark W., Lagomarsino S., Giannini C., DeCaro L., Cedola A., Müller M. Nature 403, 638 (2000).
Shapiro D., Thibault P., Beetz T., Elser V., Howells M., Jacobsen C., Kirz J., Lima E., Miao H., Neiman A.M., Sayre D. Proc. Natl. Acad. Sci. USA 102, 15343(2005)
ESRF: Science and Technology Programme 2008 (2007) In www.esrf.eu
Badenhuizen, N.P. The Biogenesis of Starch Granules of Higher Plants. Appleton Century Crofts, New York (1969).
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Riekel, C., Burghammer, M., Davies, R., Gebhardt, R., Popov, D. (2009). Fundaments of Soft Condensed Matter Scattering and Diffraction with Microfocus Techniques. In: Gomez, M., Nogales, A., Garcia-Gutierrez, M., Ezquerra, T. (eds) Applications of Synchrotron Light to Scattering and Diffraction in Materials and Life Sciences. Lecture Notes in Physics, vol 776. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-540-95968-7_4
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