Skip to main content
SpringerLink
Log in

Kristallstrukturanalyse

  • Chapter
Book cover Einführung in die Röntgenfeinstrukturanalyse

Zusammenfassung

Das Ziel einer Kristallstrukturanalyse ist es, die Anordnung der Atome innerhalb der Elementarzelle zu bestimmen. Die wichtigsten Angaben hierfür erhält man aus Beugungsexperimenten. Aus der Geometrie der Röntgenbeugung kann man, wie bereits besprochen (2.3), die Größe und Symmetrie der Elementarzelle bestimmen. Dadurch ist man in der Lage, jede Interferenz einer bestimmten Netzebenenschar im Kristall zuzuordnen (Indizierung). Außerdem erhält man aus Beugungsexperimenten Reflexintensitäten. Diese können durch Anbringen der in (5) besprochenen Korrekturen in beobachtete Strukturfaktoren |F0| umgewandelt werden und ermöglichen es, im Verlauf einer Kristallstrukturanalyse die genaue Anordnung der Atome im Kristall festzulegen.

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Log in via an institution
Chapter
USD 29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD 49.99
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
USD 64.99
Price excludes VAT (USA)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

Literatur

  1. Torkar, K., Krischner, H. und Radi, H., Mh. Chem. 96 (1965) 932.

    Google Scholar 

  2. Schönflies, A., Kristallsysteme und Kristallstruktur, Leipzig (1891).

    Google Scholar 

  3. Hermann, C., Z. Krist. 68 (1928) 257;

    Google Scholar 

  4. Mauguin, C., Z. Krist. 76 (1931) 542.

    MATH  Google Scholar 

  5. Stewart, J. M., The X-ray system, version of 1976, Technical report TR-446 of the computer science center University of Maryland.

    Google Scholar 

  6. Nowacki, W., Fouriersynthese von Kristallen, Birkhäuser, Basel (1952).

    MATH  Google Scholar 

  7. Patterson, A. L., Phys. Rev. 46 (1934) 372;

    Article  ADS  Google Scholar 

  8. Harker, D., J. Chem. Phys. 4 (1936) 381.

    Article  ADS  Google Scholar 

  9. Cochran, W., Acta Cryst. 4 (1951) 408.

    Article  Google Scholar 

  10. Friedlander, P. H., Love, W. und Sayre, D., Acta Cryst. 8 (1955) 732.

    Article  Google Scholar 

  11. Hughes, E. W., J. Amer. Chem. Soc. 63 (1941) 1737.

    Article  Google Scholar 

  12. Trueblood, K. N., Acta Cryst. 9 (1956) 359.

    Article  Google Scholar 

  13. Buerger, M. J., Vector space and its application in crystal-structure investigation, J. Wiley, New York (1959).

    Google Scholar 

  14. Bijvoet, J. M., Proc. Koninkl. Ned. Akad. Wetenschap. (B) 52 (1949) 313.

    Google Scholar 

  15. Sayre, D., Acat Cryst. 5 (1952) 60.

    Article  Google Scholar 

  16. Howells, E. R., Phillips, D. C. und Rogers, D., Acta Cryst. 3 (1950) 210.

    Article  Google Scholar 

  17. Wilson, A. J. C., Acta Cryst. 2 (1949) 318.

    Article  MathSciNet  Google Scholar 

  18. Debye, P., Ann. Phys. Lpz. 46 (1915) 809.

    Article  ADS  Google Scholar 

  19. Woolfson, M. M., Computational Crystallography, ed. by Sayre, D., Clarandon Press, Oxford (1982)110.

    Google Scholar 

  20. Lipson, H., Woolfson, M. M., Acta Cryst. 6 (1952) 439.

    Google Scholar 

  21. Cochran, W., Acta Cryst. 8 (1955) 473.

    Article  Google Scholar 

  22. Hauptmann, H., Acta Cryst. A31 (1975) 680.

    Google Scholar 

  23. Hauptmann, H., Acta Cryst. A32 (1976) 877.

    Google Scholar 

  24. Vaughan, P. A., Am. Cryst. Ass. Ann. Meeting, Ind. (1956).

    Google Scholar 

  25. Giacovazzo, C., Acta Cryst. A33 (1977) 933.

    Google Scholar 

  26. Hauptmann, H., Acta Cryst. A34 (1978) 525.

    Google Scholar 

  27. Hauptmann, H., Computational Crystallography, ed. by Sayre, D., Clarandon Press, Oxford (1982) 75.

    Google Scholar 

  28. Woolfson, M. M., Acta Cryst. 7 (1954) 61.

    Article  Google Scholar 

  29. Karle, J., Hauptmann, H., Acta Cryst. 9 (1956) 635.

    Article  MathSciNet  Google Scholar 

  30. Karle, L L., Karle, J., Acta Cryst. 17 (1964) 835.

    Article  Google Scholar 

  31. Zachariasen, W. H., Acta Cryst. 5 (1952) 68.

    Article  Google Scholar 

  32. Woolfson, M. M., Direct Methods in Crystallography, Oxford (1961).

    MATH  Google Scholar 

  33. Germanin, G., Woolfson, M. M., Acta Cryst. B24 (1968) 91.

    Google Scholar 

  34. De Titta et al., Acta Cryst. A31 (1975) 472.

    Google Scholar 

  35. Karle, J., Karle, I. L., Acta Cryst. 21 (1966) 849.

    Article  Google Scholar 

  36. Germain, G., Main, P., Woolfson, M. M., Acta Cryst. A27 (1971) 368.

    Google Scholar 

  37. Schenk, H., Computing in Crystallography, Bangalore (1980).

    Google Scholar 

  38. Main, P., Lessinger, L., Woolfson, M. M., Germain, G., Declercq, J. P., MULTAN 77, University of York, England (1977).

    Google Scholar 

  39. Overbeek, O., Schenk, H., Computing in Crystallography, Delft University Press (1978).

    Google Scholar 

  40. Coppens, P., Int. Rev. of Science 2/11, Butterworth (1975) 21.

    Google Scholar 

  41. Hirshfeld, F. L. (Ed.), Israel J. Chem. 16 (1978) 87.

    Google Scholar 

  42. Klyne, W., Prelog, V., Experientia 16 (1960) 521.

    Article  Google Scholar 

  43. Sheldrick, G. M., SHELX 82. Program for Crystal Structure Determination. University of Cambridge, England (1982);

    Google Scholar 

  44. Sheldrick, G. M., SHELX 86. Programm for Crystal Structure Determination. Universität Göttingen (1987);

    Google Scholar 

  45. Sheldrick, G. M., SHELXTL 81 User Manuel, Rev. 3, Nicolet XRD Corp., Cupertino California, USA (1981).

    Google Scholar 

  46. Stewart, J. M., et al., Rep. TR-446. Comp. Sci. Center, University of Maryland, USA (1976);

    Google Scholar 

  47. Stewart, J. M., et al., XTAL Programmers Manual, Techn. Rep. TR-873. Comp. Sci. Center, University of Maryland, USA (1982).

    Google Scholar 

  48. Busing, W. R., et al., ORGLS, Rep. ORNL-TM-305. ORNL, Tenn., USA (1963);

    Google Scholar 

  49. Busing, W. R., et al., ORFFE, Rep. ORNL-TM-306. ORNL, Tenn., USA (1964);

    Google Scholar 

  50. Busing, W. R., et al., WMIN, Rep. ORNL-5747. ORNL, Tenn. USA (1981). (ORNL = Oak Ridge National Laboratories, Tennessee, USA).

    Google Scholar 

Download references

Authors
  1. Harald Krischner
    View author publications

    You can also search for this author in PubMed Google Scholar

Rights and permissions

Reprints and permissions

Copyright information

© 1990 Friedr. Vieweg & Sohn Verlagsgesellschaft mbH, Braunschweig

About this chapter

Cite this chapter

Krischner, H. (1990). Kristallstrukturanalyse. In: Einführung in die Röntgenfeinstrukturanalyse. Vieweg+Teubner Verlag, Wiesbaden. https://doi.org/10.1007/978-3-322-98972-7_6

Download citation

  • DOI: https://doi.org/10.1007/978-3-322-98972-7_6

  • Publisher Name: Vieweg+Teubner Verlag, Wiesbaden

  • Print ISBN: 978-3-322-98973-4

  • Online ISBN: 978-3-322-98972-7

  • eBook Packages: Springer Book Archive

Publish with us

Policies and ethics

Search

Navigation