Abstract
BACKGROUND: Doped with metal oxide, zirconia is one of the most currently used ceramics for making a wide range of all-ceramic restorations in dental prosthetics. Its use entails very good mechanical properties and the possibility of obtaining a desirable aesthetic effect of manufactured prostheses.
OBJECTIVE: The main purpose/aim of this study was to investigate the influence of calcination temperature on the morphology and specific surface area development of a ZrO2 – CeO2 – Y2O3 – Al2O3 powder system obtained with a humidfree sol-gel process.
METHODS: Powders were obtained by the sol-gel method in an inert gas atmosphere at ambient temperature using, for this purpose, zirconium n-propoxide. Morphology was examined by scanning electron microscopy (SEM), and specific surface area was investigated with full-adsorption isotherms in nitrogen with a Brunauer-Emmett-Teller model (BET).
RESULTS: Depending on the calcination temperature, different morphologies and surface areas were observed.With an increase in temperature, grain growth was observed.
CONCLUSIONS: The influence of calcination temperature on morphology and specific surface area of the as-obtained powders was clearly evidenced.
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Nakonieczny, D.S. et al. (2018). Influence of Calcination Temperatures on the Morphology and Specific Surface Area Development of ZrO2-CeO2-Y2O3-Al2O3 Powders Obtained via Sol-Gel Route. In: Gzik, M., Tkacz, E., Paszenda, Z., Piętka, E. (eds) Innovations in Biomedical Engineering . IBE 2017. Advances in Intelligent Systems and Computing, vol 623 . Springer, Cham. https://doi.org/10.1007/978-3-319-70063-2_38
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DOI: https://doi.org/10.1007/978-3-319-70063-2_38
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