Skip to main content

Interphase Mechanics in Fatigued Carbon Fiber Composite Materials

  • Conference paper
  • First Online:
Micro and Nanomechanics, Volume 5

Abstract

Carbon fiber composites display considerable heterogeneity in strength and stiffness depending on the respective constituent properties, reinforcement alignments, and interfacial relationships. Typically the inherent material anisotropy and complexity lead to relatively diverse material fatigue failures depending on the loading conditions and carbon fiber reinforcement orientations. The current work seeks to better understand the mechanisms by which fatigue damage precipitates and the smallest scales (sub-micron) at which material phenomena may be observed and tracked before becoming observable on the millimeter scale or larger. Unidirectional IM7-8552 composite samples were fabricated for transverse (90°) and longitudinal (0°) fiber loading. Samples were tested in bending using a three-point set-up and in single axis tension developing the cyclic life response at several loading stresses. Baseline and failed samples were partitioned and polished for instrumented indentation and atomic force microscopy (AFM) which probed the local mechanical and morphological behavior of the composite interphase. Attempts are made to characterize the local material behavior around the fiber-matrix interphase to understand material response of this region with respect to fatigue cycling. The fiber-matrix interphase results are compared to numerical modelling in order to better understand the interphase behavior and fatigue degradation of the composite materials.

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Chapter
USD 29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD 129.00
Price excludes VAT (USA)
  • Available as EPUB and PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
USD 169.99
Price excludes VAT (USA)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info
Hardcover Book
USD 169.99
Price excludes VAT (USA)
  • Durable hardcover edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

References

  1. Strong, A.B.: Fundamentals of Composites Manufacturing. Society of Manufacturing Engineers, Dearborn (2008)

    Google Scholar 

  2. Daniel, I., Ishai, O.: Engineering Mechanics of Composite Materials, 2nd edn. Oxford University Press, New York (2006)

    Google Scholar 

  3. Jesson, D., Watts, J.: The interface and interphase in polymer matrix composites: effect on mechanical properties and methods for identification. Polym. Rev. 52, 321–354 (2012)

    Article  Google Scholar 

  4. Gibson, R.F.: A review of recent research on nanoindentation of polymer composites and their constituents. Compos. Sci. Technol. 105, 51–65 (2014)

    Article  Google Scholar 

  5. Gao, S.L., Mader, E.: Characterization of interphase nanoscale property variations in glass fibre reinforced polypropylene and epoxy resin. Compos. Part A. 33, 559–576 (2002)

    Article  Google Scholar 

  6. Gu, Y., Li, M., Wang, J., Zhang, Z.: Characterization of the interphase in carbon fiber/polymer composites using nanoscale dynamic mechanical imaging technique. Carbon. 48, 3229–3235 (2010)

    Article  Google Scholar 

  7. Hodzic, A., Kim, J.K., Stachurski, Z.H.: Nano-indentation and nano-scratch of polymer/glass interfaces. II: model of interphases in water aged composite materials. Polymer. 42, 5701–5710 (2001)

    Article  Google Scholar 

  8. Saha, R., Nix, W.D.: Effects of the substrate on the determination of thin film mechanical properties by nanoindentation. Acta Mater. 50, 23–28 (2002)

    Article  Google Scholar 

  9. Zidi, M., Carpentier, L., Chateauminois, A., Sidoroff, F.: Quantitative analysis of the micro-indentation behaviour of fibre-reinforced composites: development and validation of an analytical model. Comp. Sci. Tech. 60, 429–437 (2000)

    Article  Google Scholar 

  10. Jakes, J.E., Frihart, C.R., Beecher, J.F., Moon, R.J., Stone, D.S.: Experimental method to account for structural compliance in nanoindentation measurements. J. Mater. Res. 23(4), 1113–1127 (2008)

    Article  Google Scholar 

  11. Randall, N.X., Vandamme, M.: Nanoindentation analysis as a two-dimensional tool for mapping the mechanical properties of complex surfaces. J. Mater. Res. 24, 679–690 (2011)

    Article  Google Scholar 

  12. Hardiman, M., Vaughan, T.J., McCarthy, C.T.: Fibrous composite matrix characterization using nanoindentation: the effect of fibre constraint and the evolution from bulk to in-situ matrix properties. Compos. Part A. 68, 296–303 (2015)

    Article  Google Scholar 

  13. Nuriel, S., Katz, A., Wagner, H.D.: Measuring fiber-matrix interfacial adhesion by means of a ‘drag-out’ micromechanical test. Compos. Part A. 36, 33–37 (2005)

    Article  Google Scholar 

  14. Nairn, J.A.: Analytical fracture mechanics analysis of the pull-out test including the effects of friction and thermal stresses. Adv. Compos. Lett. 9, 373–383 (2000)

    Google Scholar 

  15. Nair, S.S., Wang, S., Hurley, D.C.: Nanoscale characterization of natural fibers and their composites using contact-resonance force microscopy. Compos. Part A. 41, 624–631 (2010)

    Article  Google Scholar 

  16. Hu, Z., Farahikia, M., Delfanian, F.: Fiber bias effect on characterization of carbon fiber-reinforced polymer composites by nanoindentation testing and modeling. J. Comp. Mater. 49, 3359–3372 (2015)

    Article  Google Scholar 

  17. VanLandingham, M.R., Dagastine, R.R., Eduljee, R.F., McCullough, R.L., Gillespie, J.W.: Characterization of nanoscale property variations in polymer composite systems: 1. Experimental results. Compos. Part A. 30, 75–83 (1999)

    Article  Google Scholar 

  18. Diez-Pascual, A.M., Gomez-Fatou, M.A., Ania, F., Flores, A.: Nanoindentation assessment of the interphase in carbon nanotube-based hierarchical composites. J. Phys. Chem. 116, 24193–24200 (2012)

    Article  Google Scholar 

  19. ASTM D7264: Standard test method for flexural properties of polymer matrix composite materials. ASTM International, West Conshohocken (2015)

    Google Scholar 

  20. ASTM D3039: Standard test method for tensile properties of polymer matrix composite materials. ASTM International, West Conshohocken (2014)

    Google Scholar 

  21. Oliver, W.C., Pharr, G.M.: An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments. J. Mater. Res. 7(6), 1564–1583 (1992)

    Article  Google Scholar 

Download references

Acknowledgements

FG is a contractor to the US Army Research Laboratory under Cooperative Agreement W911NF-16-2-0182.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Todd C. Henry .

Editor information

Editors and Affiliations

Rights and permissions

Reprints and permissions

Copyright information

© 2018 The Society for Experimental Mechanics, Inc.

About this paper

Cite this paper

Henry, T.C., Cole, D.P., Gardea, F., Haynes, R.A. (2018). Interphase Mechanics in Fatigued Carbon Fiber Composite Materials. In: Starman, L., Hay, J. (eds) Micro and Nanomechanics, Volume 5. Conference Proceedings of the Society for Experimental Mechanics Series. Springer, Cham. https://doi.org/10.1007/978-3-319-63405-0_5

Download citation

  • DOI: https://doi.org/10.1007/978-3-319-63405-0_5

  • Published:

  • Publisher Name: Springer, Cham

  • Print ISBN: 978-3-319-63404-3

  • Online ISBN: 978-3-319-63405-0

  • eBook Packages: EngineeringEngineering (R0)

Publish with us

Policies and ethics