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Texture Weakening and Grain Refinement by High Speed Rolling and Annealing of an AZ31 Magnesium Alloy

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Magnesium Technology 2017

Part of the book series: The Minerals, Metals & Materials Series ((MMMS))

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Abstract

High-speed rolling of 1000 m/min has been used to produce Mg AZ31 alloy sheets at an initial temperature of 100 °C with increasing reductions to generate different as-rolled microstructures. After a reduction of 30%, a heavily twinned and shear-banded microstructure was seen, while after a reduction of 49%, a partially dynamically recrystallized (DRXed) and twinned microstructure was observed. The as-rolled specimens were then annealed at temperatures from 200 to 500 °C. Texture weakening and grain refinement were achieved at both reductions during annealing by static recrystallization (SRX). However, the 49% reduction specimen showed a much higher kinetics of SRX and a higher rate of texture weakening, comparing to the 30% reduction specimen. The weakest texture achieved in the former was slightly lower than that in the latter, which indicates that texture weakening is more effective in the specimen with heavily twinned and shear-banded microstructure than that with partially DRXed and twinned microstructure. Nevertheless, the average size of the SRXed grains at the full recrystallization condition of the specimen after the reduction of 49% was only half of that after 30%.

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References

  1. A.A. Luo, Applications: aerospace, automotive and other structural applications of magnesium, in Fundamentals of Magnesium Alloy Metallurgy, ed. by M.O. Pekguleryuz, K.U. Kainer, A.A. Kaya (Woodhead Publishing Limited, 2013), pp. 266–316

    Google Scholar 

  2. A.A. Luo, A.K. Sachdev, Applications of magnesium alloys in automotive engineering, in Advances in Wrought Magnesium Alloys Fundamentals of Processing, Properties and Applications, ed. by C. Bettles, M. Barnett (Woodhead Publishing Limited, 2012)

    Google Scholar 

  3. A.I. Taub et al., The evolution of technology for materials processing over the last 50 years: the automotive example. J. Met. 59(2), 48–57 (2007)

    Google Scholar 

  4. M.O. Pekguleryuz, Current developments in wrought magnesium alloys, in Advances in Wrought Magnesium Alloys Fundamentals of Processing, Properties and Applications, ed. by C. Bettles, M. Barnett (Woodhead Publishing Limited, 2012)

    Google Scholar 

  5. S.R. Agnew, M.H. Yoo, C.N. Tomé, Application of texture simulation to understanding mechanical behavior of Mg and solid solution alloys containing Li or Y. Acta Mater. 49, 4277–4289 (2001)

    Article  Google Scholar 

  6. A. Styczynski et al., Cold rolling textures in AZ31 wrought magnesium alloy. Scr. Mater. 50, 943–947 (2004)

    Article  Google Scholar 

  7. T. Mukai et al., Effect of grain refinement on tensile ductility in ZK60 magnesium alloy under dynamic loading. Mater. Trans. 42(7), 1177–1181 (2001)

    Article  Google Scholar 

  8. D.L. Atwell, M.R. Barnett, W.B. Hutchinson, The effect of initial grain size and temperature on the tensile properties of magnesium alloy AZ31 sheet. Mater. Sci. Eng. A 549, 1–6 (2012)

    Article  Google Scholar 

  9. I. Basu, T. Al-Samman, Triggering rare earth texture modification in magnesium alloys by addition of zinc and zirconium. Acta Mater. 67, 116–133 (2014)

    Article  Google Scholar 

  10. T. Mukai et al., Ductility enhancement in AZ31 magnesium alloy by controlling its grain structure. Scr. Mater. 45, 89–94 (2001)

    Article  Google Scholar 

  11. H. Wang, P.D. Wu, M.A. Gharghouri, Effects of basal texture on mechanical behaviour of magnesium alloy AZ31B sheet. Mater. Sci. Eng. A 527, 3588–3594 (2010)

    Article  Google Scholar 

  12. N. Stanford, D. Atwell, M.R. Barnett, The effect of Gd on the recrystallisation, texture and deformation behaviour of magnesium-based alloys. Acta Mater. 58, 6773–6783 (2010)

    Article  Google Scholar 

  13. N. Stanford, M. Barnett, Effect of composition on the texture and deformation behaviour of wrought Mg alloys. Scr. Mater. 58, 179–182 (2008)

    Article  Google Scholar 

  14. Y. Chinoa, M. Mabuchi, Enhanced stretch formability of Mg–Al–Zn alloy sheets rolled at high temperature (723 K). Scripta Mater. 60, 447–450 (2009)

    Article  Google Scholar 

  15. G. Manna, J.R. Griffiths, C.H. Cáceres, Hall-Petch parameters in tension and compression in cast Mg–2Zn alloys. J. Alloy. Compd. 378, 188–191 (2004)

    Article  Google Scholar 

  16. J. Bohlen et al., The texture and anisotropy of magnesium–zinc–rare earth alloy sheets. Acta Mater. 55, 2101–2112 (2007)

    Google Scholar 

  17. R. Li et al., Effect of Li addition on the mechanical behavior and texture of the as-extruded AZ31 magnesium alloy. Mater. Sci. Eng. A 562, 33–38 (2013)

    Article  Google Scholar 

  18. Muraoka A. et al., Improvement in rolling workability of Fe3Al by high-speed rolling, in Journal of Physics: Conference Series (IOP Publishing Ltd. 2012)

    Google Scholar 

  19. H. Koh et al., Deformation and texture evolution during high-speed rolling of AZ31 magnesium sheets. Mater. Trans. 48(8), 2023–2027 (2007)

    Article  Google Scholar 

  20. M. Sanjari et al., Promotion of texture weakening in magnesium by alloying and thermomechanical processing-II high speed rolling. J. Mater. Sci. 49, 1426–1436 (2014)

    Article  Google Scholar 

  21. H. Li et al., Deformation mechanism and texture and microstructure evolution during high-speed rolling of AZ31B Mg sheets. J. Mater. Sci. 43, 7148–7156 (2008)

    Article  Google Scholar 

  22. S.Q. Zhu et al., Effect of twinning and dynamic recrystallization on the high strain rate rolling process. Scr. Mater. 63, 985–988 (2010)

    Article  Google Scholar 

  23. T. Sakai, Y. Watanabe, H. Utsunomiya, Microstructure and texture of AZ31 magnesium alloy sheet rolled by high speed warm rolling. Mater. Sci. Forum 618–619, 483–486 (2009)

    Google Scholar 

  24. J. Su et al., Characteristics of magnesium AZ31 alloys subjected to high speed rolling. Mater. Sci. Eng. A 636, 582–592 (2015)

    Article  Google Scholar 

  25. B. Beausir et al., Analysis of texture evolution in magnesium during equal channel angular extrusion. Acta Mater. 56, 200–214 (2008)

    Article  Google Scholar 

  26. M. Kohzu et al., Texture randomization of AZ31 magnesium alloy sheets for improving the cold formability by a combination of rolling and high-temperature annealing. Mater. Trans. 51(4), 749–755 (2010)

    Google Scholar 

  27. A. Levinson et al., Influence of deformation twinning on static annealing of AZ31 Mg alloy. Acta Mater. 61, 5966–5978 (2013)

    Article  Google Scholar 

  28. X. Li et al., Orientational analysis of static recrystallization at compression twins in a magnesium alloy AZ31. Mater. Sci. Eng. A 517, 160–169 (2009)

    Article  Google Scholar 

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Su, J., Yue, S. (2017). Texture Weakening and Grain Refinement by High Speed Rolling and Annealing of an AZ31 Magnesium Alloy. In: Solanki, K., Orlov, D., Singh, A., Neelameggham, N. (eds) Magnesium Technology 2017. The Minerals, Metals & Materials Series. Springer, Cham. https://doi.org/10.1007/978-3-319-52392-7_76

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