Abstract
Mg-1.58Zn-0.52Gd (wt%) alloy was indirectly extruded at different temperatures and the resulting microstructure , texture and mechanical properties were investigated. The alloy extruded at 350 °C exhibited a typical bimodal microstructure, consisting of fine dynamically recrystallized (DRXed) grains of ~3.1 μm and coarse unDRXed grains elongated along the ED with many fine spherical Mg3Zn3Gd2 phase, and a strong \( \left[ {10\bar{1}0} \right] \) fiber texture, thereby resulting in high yield strength of 283 MPa and low elongation of 10.0%. With increasing extrusion temperature, the yield strength gradually decreased mainly due to increased DRXed grain size from the Hall-Petch relation, and the elongation increased due to the weakened extrusion texture and increased DRX fraction, suppressing crack initiation at twins in coarse unDRXed grains. As a result, the alloy extruded at 400 °C showed yield strength of 161 MPa and elongation of 24.7%.
References
H. Yan, R.S. Chen, E.H. Han, Room-temperature ductility and anisotropy of two rolled Mg–Zn–Gd alloys. Mater. Sci. Eng. A 527, 3317–3322 (2010)
D. Wu et al., Influence of texture and grain size on the room-temperature ductility and tensile behavior in a Mg-Gd-Zn alloy processed by rolling and forging. Mater. Des. 41, 306–313 (2012)
H. Yan et al., Effects of trace Gd concentration on texture and mechanical properties of hot-rolled Mg-2Zn-xGd sheets. J. Magnes. Alloys 1, 23–30 (2013)
J. Luo et al., Effects of Gd concentration on microstructure, texture and tensile properties of Mg-Zn-Gd alloys subjected to large strain hot rolling. Mater. Sci. Eng. A 614, 88–95 (2014)
M.G. Jiang et al., Rare earth texture and improved ductility in a Mg-Zn-Gd alloy after high-speed extrusion. Mater. Sci. Eng. A 667, 233–239 (2016)
Y. Liu et al., Stable icosahedral phase in Mg-Zn-Gd alloy. Scripta Mater. 55, 919–922 (2006)
A. Rollett et al., Recrystallization and Related Annealing Phenomena (Elsevier, Amsterdam, 2004)
T. Laser et al., The influence of calcium and cerium mischmetal on the microstructural evolution of Mg-3Al-1Zn during extrusion and resulting mechanical properties. Acta Mater. 56, 2791–2798 (2008)
S. Yi, H.-G. Brokmeier, D. Letzig, Microstructural evolution during the annealing of an extruded AZ31 magnesium alloy. J. Alloy. Compd. 506, 364–371 (2010)
S. Agnew, M. Yoo, C. Tome, Application of texture simulation to understanding mechanical behavior of Mg and solid solution alloys containing Li or Y. Acta Mater. 49, 4277–4289 (2001)
J. Del Valle, F. Carreño, O.A. Ruano, Influence of texture and grain size on work hardening and ductility in magnesium-based alloys processed by ECAP and rolling. Acta Mater. 54, 4247–4259 (2006)
S.H. Choi, E.J. Shin, B.S. Seong, Simulation of deformation twins and deformation texture in an AZ31 Mg alloy under uniaxial compression. Acta Mater. 55, 4181–4192 (2007)
H. Yu et al., Effects of extrusion speed on the microstructure and mechanical properties of ZK60 alloys with and without 1 wt% cerium addition. Mater. Sci. Eng. A 583, 25–35 (2013)
S.W. Xu et al., Dynamic microstructural changes during hot extrusion and mechanical properties of a Mg-5.0 Zn-0.9 Y-0.16 Zr (wt.%) alloy. Mater. Sci. Eng. A 528, 4055–4067 (2011)
S.H. Park, B.S. You, Effect of homogenization temperature on the microstructure and mechanical properties of extruded Mg-7Sn-1Al-1Zn alloy. J. Alloy. Compd. 637, 332–338 (2015)
M.R. Barnett, Twinning and the ductility of magnesium alloys Part II. “Contraction” twins. Mater. Sci. Eng. A 464, 8–16 (2007)
P. Cizek, M.R. Barnett, Characteristics of the contraction twins formed close to the fracture surface in Mg-3Al-1Zn alloy deformed in tension. Scripta Mater. 59, 959–962 (2008)
M.R. Barnett et al., Influence of grain size on the compressive deformation of wrought Mg-3Al-1Zn. Acta Mater. 52, 5093–5103 (2004)
Acknowledgements
The authors gratefully acknowledge the financial supports from the State Key Program of National Natural Science of China (No. 51531002), National Natural Science Foundation of China (NSFC, No. 51601193 and 51301173), National Key Research and Development Program of China (No. 2016YFB0301104), National Basic Research Program of China (973 Program, No. 2013CB632202), JST, Advanced Low Carbon Technology Research and Development Program (ALCA, No. 12102886) and JSPS, Grant-in-Aid for Young Scientists (B) (No. 16K18266).
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Jiang, M.G., Chen, J.C., Yan, H., Xu, C., Nakata, T., Kamado, S. (2017). Microstructure and Mechanical Properties of an Extruded Mg-1.58Zn-0.52Gd Alloy. In: Solanki, K., Orlov, D., Singh, A., Neelameggham, N. (eds) Magnesium Technology 2017. The Minerals, Metals & Materials Series. Springer, Cham. https://doi.org/10.1007/978-3-319-52392-7_43
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DOI: https://doi.org/10.1007/978-3-319-52392-7_43
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