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Heteroepitaxial Recrystallization, a New Recrystallization Mechanism in Sub-Solvus Forged γ-γ’ Nickel-Based Superalloys with Low Lattice Mismatch

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Proceedings of the 6th International Conference on Recrystallization and Grain Growth (ReX&GG 2016)

Abstract

A new dynamic recrystallization mechanism has recently been reported in γ-γ′ Nickel-based superalloys after hot-forging in the sub-solvus domain. The mechanism leads to recrystallized grains encompassing a primary γ′ precipitate having the same crystallographic orientation. The nucleation of those grains actually occurs before deformation by inverse precipitation of coherent γ phase at the rim of the primary γ′ precipitates. This makes the specificity of that recrystallization process. Once the matrix starts being deformed, the coherent γ phase particles grow under the conventional stored-energy-consumption driving force. A detailed study of this new mechanism in the René65™ alloy has recently been published by the authors. Heteroepitaxially recristallized grains grow first, at low strain levels; then discontinuous dynamic recrystallization takes place, through classical necklace nucleation. Contrary to the usual trends for dynamic recrystallization kinetics, heteroepitaxial recrystallization goes faster with increasing strain rate and at lower temperatures. In the present paper, hot-forging experiments have been designed to demonstrate that the same mechanism can be triggered in other γ-γ′ nickel base superalloys (Udimet 720 and RR1000).

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References

  1. G. Shen, S.L. Semiatin, R. Shivpuri, Modeling microstructural development during the forging of Waspaloy, Metall. Mater. Trans. A. 26 (1995) 1795–1803. doi:10.1007/BF02670767

    Article  Google Scholar 

  2. S.. Medeiros, Y.V.R.. Prasad, W.. Frazier, R. Srinivasan, Microstructural modeling of metadynamic recrystallization in hot working of IN 718 superalloy, Mater. Sci. Eng. A. 293 (2000) 198–207. doi:10.1016/S0921–5093(00)01053–4.

    Article  Google Scholar 

  3. Q. Guo, D. Li, S. Guo, H. Peng, J. Hu, The effect of deformation temperature on the microstructure evolution of Inconel 625 superalloy, J. Nucl. Mater. 414 (2011) 440–450. doi:10.1016/j.jnucmat.2011.05.029

    Article  Google Scholar 

  4. S. Mitsche, C. Sommitsch, D. Huber, M. Stockinger, P. Poelt, Assessment of dynamic softening mechanisms in Allvac® 718Plus™ by EBSD analysis, Mater. Sci. Eng. A. 528 (2011) 3754–3760. doi:10.1016/j.msea.2011.01.044

    Article  Google Scholar 

  5. B. Lindsley, X. Pierron, Sub-solvus recrystallization mechanisms in UDIMET (R) alloy 720LI, SUPERALLOYS 2000. (2000) 59–68.

    Google Scholar 

  6. H. Zhang, K. Zhang, S. Jiang, H. Zhou, C. Zhao, X. Yang, Dynamic recrystallization behavior of a γ′-hardened nickelbased superalloy during hot deformation, J. Alloys Compd. 623 (2015) 374–385. doi:10.1016/j.jallcom.2014.11.056

    Article  Google Scholar 

  7. Y.C. Lin, X.-Y. Wu, X.-M. Chen, J. Chen, D.-X. Wen, J.-L. Zhang, et al., EBSD study of a hot deformed nickel-based superalloy, J. Alloys Compd. 640 (2015) 101–113. doi:10.1016/j.jallcom.2015.04.008

    Article  Google Scholar 

  8. M. ASHBY, J. HARPER, J. LEWIS, INTERACTION OF CRYSTAL BOUNDARIES WITH SECOND-PHASE PARTICLES, Trans. Metall. Soc. AIME. 245 (1969) 413–&.

    Google Scholar 

  9. C.S. Smith, Zener pinning, Trans. Met. Soc. AIME. 175 (1948) 15–51.

    Google Scholar 

  10. M.-A. Charpagne, T. Billot, J.-M. Franchet, N. Bozzolo, Hereroepitaxial recrystallization: a new mechanism simultaneous to conventional discontinuous dynamic recrystallizaton, discovered in a polycristalline γ-γ′ nickel-based superalloy, Submitted. (2016).

    Google Scholar 

  11. M.-A. Charpagne, T. Billot, J.-M. Franchet, N. Bozzolo, Heteroepitaxial recrystallization observed in René 65 and Udimet 720: a new recrystallization mechanism possibly occuring also in other low lattice mismatch γ/γ′ Nickel-based superalloys, in: Submitt. to Superalloys 2016, TMS, 2016.

    Google Scholar 

  12. M.-A. Charpagne, P. Vennéguès, T. Billot, J.-M. Franchet, N. Bozzolo, Evidence of multimicrometric coherent γ′ precipitates in a γ-γ’ Nickel-based superalloy, J. Microsc. (2016). http://onlinelibrary.wiley.com/doi/10.1111/jmi.12380/full.

  13. B.M.B. Grant, E. Knoche, M. Preuss, J. Quinta da Fonseca, M.R. Daymond, The Effect of Lattice Misfit on Deformation Mechanisms at High Temperature, Adv. Mater. Res. 278 (2011) 144–149. doi:10.4028/www.scientific.net/AMR.278.144.

    Article  Google Scholar 

  14. R.A. Ricks, A.J. Porter, R.C. Ecob, The growth of γ′ precipitates in nickel-base superalloys, Acta Metall. 31 (1983) 43–53. doi:10.1016/0001–6160(83)90062–7.

    Article  Google Scholar 

  15. F.E. Sczerzenie, G.E. Maurer, Development of Udimet 720 for High Strength Disk Applications, (1984) 573–580.

    Google Scholar 

  16. A. Day, Developments in the EBSP technique and their application to grain imaging, Ph. D. dissertation, University of Bristol, 1993.

    Google Scholar 

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© 2016 TMS (The Minerals, Metals & Materials Society)

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Charpagne, MA., Billot, T., Franchet, JM., Bozzolo, N. (2016). Heteroepitaxial Recrystallization, a New Recrystallization Mechanism in Sub-Solvus Forged γ-γ’ Nickel-Based Superalloys with Low Lattice Mismatch. In: Holm, E.A., et al. Proceedings of the 6th International Conference on Recrystallization and Grain Growth (ReX&GG 2016). Springer, Cham. https://doi.org/10.1007/978-3-319-48770-0_38

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