Abstract
Because of ever increasing demanded of Magnesium alloys in various industries, high temperature deformation of Mg-Al-Zn alloys (AZ31) at constant stress (i.e. creep) were studied at a wide range of stresses and temperatures to characterize underlying deformation mechanism and dynamic recrystallization (DRX) Various microstructures (e.g. grain growth & DRX) are noted during steady-state creep mechanisms such as grain boundary sliding (GBS), dislocation glide creep (DGC) and dislocation climb creep (DCC). Although a combination of DRX and grain growth is characteristic of low stacking fault energy materials like Mg alloys at elevated temperatures, observation reveals grain growth at low strain-rates (GBS region) along with dynamic recovery (DRV) mechanism. Scanning Electron Microscopic (SEM) characterization of the fracture surface reveals more inter-granular fracture for large grains (i.e. GBS region with DRV process) and more dimple shape fracture for small grains (i.e. DGC & DCC region with DRX).
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References
S. W. Chung, H. Watanabe, W.-J. Kim, and K. Higashi, “Creep Deformation Mechanisms in Coarse-Grained Solid Solution Mg Alloys,” Mater. Trans., vol. 45, no. 4, pp. 1266–1271, 2004.
R. Korla and A. H. Chokshi, “A Constitutive Equation for Grain Boundary Sliding: An Experimental Approach,” Metall. Mater. Trans. A, vol. 45, no. 2, pp. 698–708, Oct. 2013.
R. B. Figueiredo and T. G. Langdon, “Developing superplasticity in a magnesium AZ31 alloy by ECAP,” J. Mater. Sci., vol. 43, no. 23–24, pp. 7366–7371, Jul. 2008.
S. Spigarelli, M. El Mehtedi, D. Ciccarelli, and M. Regev, “Effect of grain size on high temperature deformation of AZ31 alloy,” Mater. Sci. Eng. A, vol. 528, no. 22–23, pp. 6919–6926, Aug. 2011.
S. Spigarelli, M. El Mehtedi, M. Cabibbo, E. Evangelista, J. Kaneko, A. Jäger, and V. Gartnerova, “Analysis of high-temperature deformation and microstructure of an AZ31 magnesium alloy,” Mater. Sci. Eng. A, vol. 462, no. 1–2, pp. 197–201, Jul. 2007.
H. Somekawa, K. Hirai, H. Watanabe, Y. Takigawa, and K. Higashi, “Dislocation creep behavior in Mg-Al-Zn alloys,” Mater. Sci. Eng. A, vol. 407, no. 1–2, pp. 53–61, Oct. 2005.
K. Ishikawa, H. Watanabe, and T. Mukai, “High temperature compressive properties over a wide range of strain rates in an AZ31 magnesium alloy,” J. Mater. Sci., vol. 40, no. 7, pp. 1577–1582, Apr. 2005.
A. G. Beer and M. R. Barnett, “Influence of initial microstructure on the hot working flow stress of Mg-3A1–1Zn,” Mater. Sci. Eng. A, vol. 423, no. 1–2, pp. 292–299, May 2006.
S.-H. Choi, J. K. Kim, B. J. Kim, and Y. B. Park, “The effect of grain size distribution on the shape of flow stress curves of Mg-3Al-lZn under uniaxial compression,” Mater. Sci. Eng. A, vol. 488, no. 1–2, pp. 458–467, Aug. 2008.
H.-K. Kim and W.-J. Kim, “Creep behavior of AZ31 magnesium alloy in low temperature range between 423 K and 473 K,” J. Mater. Sci., vol. 42, no. 15, pp. 6171–6176, Apr. 2007.
J. A. D. E. L. Valle and O. A. Ruano, “Deformation Mechanisms Responsible for the High Ductility in a Mg AZ31 Alloy Analyzed by Electron Backscattered Diffraction,” Metallurgical and Material Trans A., vol. 36, no. June, pp. 1427–1438, 2005.
S. W. Chung, C. S. Chung, and D. Kum, “Super plasticity in thin Magnesium alloy sheets and deformation mechanism maps for magnesium.,” Acta Mater., vol. 49, pp. 3337–3345, 2001.
K. Kitazono, E. Sato, and K. Kuribayashi, “Internal stress superplasticity in polycrystalline AZ31 magnesium alloy,” Scr. Mater., vol. 44, no. 12, pp. 2695–2702, Jun. 2001.
P. Shahbeigi Roodposhti, A. Sarkar, and K. L. Murty, “A review of the influence of production methods and intermetallic phase on the creep properties of AZ91,” Magnes. Technol., pp. 59–64, 2014.
K. L. Murty, “Grain boundary sliding and viscous glide mechanisms of high temperature creep in Pb-6% Sn,” Scr. Metall., vol. 7, pp. 1083–1088, 1973.
T. G. Langdon, “A unified approach to grain boundary sliding in creep and superplasticity,” Acta Metall., vol. 42, no. 7, pp. 2437–2443, 1994.
H. Somekawa, H. Watanabe, and T. Mukai, “Effect of solute atoms on grain boundary sliding in magnesium alloys,” Philos. Mag., vol. 94, no. 12, pp. 1345–1360, Apr. 2014.
S. Ansary, R. Mahmudi, and M. J. Esfandyarpour, “Creep of AZ31 Mg alloy: A comparison of impression and tensile behavior,” Mater. Sci. Eng. A, vol. 556, pp. 9–14, Oct. 2012.
J. Koike, R. Ohyama, T. Kobayashi, M. Suzuki, and K. Maruyama, “Grain-Boundary Sliding in AZ31 Magnesium Alloys at Room Temperature to 523 K,” Mater. Trans., vol. 44, no. 4, pp. 445–451,2003.
J. Deng, Y. C. Lin, S. Li, J. Chen, and Y. Ding, “Hot tensile deformation and fracture behaviors of AZ31 magnesium alloy,” Materials & Design, vol. 49, pp. 209–219, 2013.
a. G. Beer and M. R. Barnett, “Microstructural Development during Hot Working of Mg-3Al-1Zn,” Metall. Mater. Trans. A, vol. 38, no. 8, pp. 1856–1867, Jul. 2007.
S. Gourdet and F. Montheillet, “A model of continuous dynamic recrystallization,” Acta Mater., vol. 51, no. 9, pp. 2685–2699, May 2003.
S. Gourdet and F. Montheillet, “Effects of dynamic grain boundary migration during the hot compression of high stacking fault energy metals,” Acta Mater., vol. 50, no. 11, pp. 2801–2812, Jun. 2002.
N. Xiao, C. Zheng, D. Li, and Y. Li, “A simulation of dynamic recrystallization by coupling a cellular automaton method with a topology deformation technique,” Comput. Mater. Sci., vol. 41, no. 3, pp. 366–374, Jan. 2008.
G. Kugler and R. Turk, “Modeling the dynamic recrystallization under multi-stage hot deformation,” Acta Mater., vol. 52, no. 15, pp. 4659–4668, Sep. 2004.
X. LIU, L. LI, F. HE, J. ZHOU, B. ZHU, and L. ZHANG, “Simulation on dynamic recrystallization behavior of AZ31 magnesium alloy using cellular automaton method coupling Laasraoui-Jonas model,” Trans. Nonferrous Met. Soc. China, vol. 23, no. 9, pp. 2692–2699, Sep. 2013.
P. Shahbeigi Roodposhti, “A Review on the Equal Channel Angular Process of Commercially pure Titanium,” Proc. MS&T14, pp. 1559–1566, 2014.
R. Ding and Z. Guo, “Coupled quantitative simulation of microstructural evolution and plastic flow during dynamic recrystallization,” Acta Mater., vol. 49, no. 16, pp. 3163–3175, Sep. 2001.
W. Roberts and B. Ahlblom, “A nucleation criterion for dynamic recrystallization during hot working,” Acta Metall., vol. 26, no. 5, pp. 801–813, May 1978.
H. Watanabe, et al. “Grain size control of commercial wrought Mg-Al-Zn alloys utilizing dynamic recrystallization.pdf” Mater. Trans., Vol. 42, pp. 1200–1205,2001.
Y. C. Lin, M.-S. Chen, and J. Zhong, “Microstructural evolution in 42CrMo steel during compression at elevated temperatures,” Mater. Lett., vol. 62, no. 14, pp. 2132–2135, May 2008.
S. Mandal, a. K. Bhaduri, and V. Subramanya Sarma, “Influence of State of Stress on Dynamic Recrystallization in a Titanium-Modified Austenitic Stainless Steel,” Metall. Mater. Trans. A, vol. 43, no. 2, pp. 410–414, Dec. 2011.
Y. C. Lin, M.-S. Chen, and J. Zhong, “Effect of temperature and strain rate on the compressive deformation behavior of 42CrMo steel,” J. Mater. Process. Technol., vol. 205, no. 1–3, pp. 308–315, Aug. 2008.
F. A. Mohamed and T. G. Langdon, “The transition from dislocation climb to viscous glide in creep of solid solution alloys,” Acta Metall., vol. 22, no. 6, pp. 779–788, Jun. 1974.
K. L. Murty and J. Ravi, “Transitions in creep mechanisms and creep anisotropy in Zr-1Nb-1Sn-0.2Fe sheet,” Nucl. Eng. Des., vol. 156, no. 3, pp. 359–371, Jun. 1995.
Y. Zhou, B. Devarajan, and K. Murty, “Short-term rupture studies of Zircaloy-4 and Nb-modified Zircaloy-4 tubing using closed-end internal pressurization,” Nucl. Eng. Des., vol. 228, no. 1–3, pp. 3–13, Mar. 2004.
K. Linga Murty, “Transitional creep mechanisms in Al-5Mg at high stresses,” Scr. Metall., vol. 7, no. 9, pp. 899–903, Sep. 1973.
S. Spigarelli and M. El Mehtedi, “Creep as an extension of hot working: A unified approach to high temperature deformation of AZ31 alloy,” Mater. Sci. Eng. A, vol. 527, no. 21–22, pp. 5708–5714, Aug. 2010.
A. H. Chokshi, “Cavity nucleation and growth in superplasticity,” Mater. Sci. Eng. A, vol. 410–411, no. May, pp. 95–99, Nov. 2005.
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Roodposhti, P.S., Sarkar, A., Murty, K.L. (2015). Creep Deformation Mechanisms and Related Microstucture Development of AZ31 Magnesium Alloy. In: Manuel, M.V., Singh, A., Alderman, M., Neelameggham, N.R. (eds) Magnesium Technology 2015. Springer, Cham. https://doi.org/10.1007/978-3-319-48185-2_9
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DOI: https://doi.org/10.1007/978-3-319-48185-2_9
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