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Morphology, Chemical Composition, and Magnetic Properties of Arc Discharge Fe–C Soot

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Part of the book series: Springer Proceedings in Physics ((SPPHY,volume 186))

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Abstract

The present research aims of elaborating a new manufacturing technology of magnetic nanoparticles for ferrofluid applications. Composite Fe–C anode sputtering in a low-pressure arc discharge has been used to produce Fe-containing nanoparticles on a carbon matrix. The chemical composition and size distribution function of iron containing nanoparticles have been measured. The sizes of Fe-containing nanoparticles are of 3–12 nm: chemical composition includes iron and iron carbide. It was shown that the powder is a superparamagnetic material. The stable ferrofluid, based on synthesised magnetic nanoparticles on a carbon matrix in water with nonoxynol-9 as surfactant, has been manufactured. The value of saturation magnetization on the level of 30 KA/m has been obtained.

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References

  1. Kratschmer, W., Lamb, L.D., Fostiopoulos, K., Hoffman, D.R.: Solid C-60—a new form of carbon. Nature 348, 354–358 (1990)

    Article  ADS  Google Scholar 

  2. Yannoni, C.S., Hoinkis, M., de Vries, M.S., et al.: Scandium clusters in fullerene cages. Science 256, 1191–1192 (1992)

    Article  ADS  Google Scholar 

  3. Majetich, S.A., Artman, J.O., McHenry, M.E., et al.: Preparation and properties of carbon coated magnetic nanoparticles. Phys. Rev. B. 48, 16845–16848 (1993)

    Article  ADS  Google Scholar 

  4. Brunsman, E.M., Sutton, R., Bortz, E., et al.: Magnetic properties of carbon coated, ferromagnetic nanoparticles produced by carbon-arc method. J. Appl. Phys. 75, 5882–5884 (1994)

    Google Scholar 

  5. Maltsev, V.A., Novopashin, S.A., Nerushev, O.A., Cakhapov, C.Z., Smovzh, D.V.: Synthesis of metal nanoparticles on a carbon matrix. Nanotechnol. Russ. 2(5, 6), 85–89 (2007)

    Google Scholar 

  6. Gulyaev, R.V., Slavinskaya, E.M., Novopashin, S.A., Smovzh, D.V., Zaikovskii, A.V., Osadchii, DYu., Bulavchenko, O.A., Korenev, S.V., Boronin, A.I.: Highly active PdCeOx composite catalysts for low-temperature CO oxidation, prepared by plasma-arc synthesis. Appl. Catal. B 147, 132–143 (2014)

    Article  Google Scholar 

  7. Faraji, Y.Y., Rezaee, M.: Magnetic nanoparticles: synthesis, stabilization, functionalization, characterization, and applications. J. Iran. Chem. Soc. 7(1), 1–37 (2010)

    Google Scholar 

  8. Filatov, EYu., Novopashin, S.A., Korenev, S.V.: Co–Pt and Fe–Pt bimetallic nanoparticles in a carbon matrix are prepared by a plasma arc process. Russ. J. Inorg. Chem. 58(1), 78–83 (2013)

    Article  Google Scholar 

  9. Gegechkori, T., Mamniashvili, G., Kutelia, E., et al.: Technology for production of magnetic carbon nanopowders doped with iron and cobalt nanoclusters. J. Magn. Magn. Mater. 373, 200–206 (2015)

    Article  ADS  Google Scholar 

  10. Chaitoglou, S., Reza Sanaee, M., Aguiló-Aguayo, N., Bertran, E.: Arc-discharge synthesis of iron encapsulated in carbon nanoparticles for biomedical applications. J. Nanomater. Article ID 178524, 8 p (2014)

    Google Scholar 

  11. Macková, H., Horák, D., Donchenko, G.V., et al.: Colloidally stable surface-modified iron oxide nanoparticles: Preparation, characterization and anti-tumor activity. J. Magn. Magn. Mater. 380, 125–131 (2015)

    Article  ADS  Google Scholar 

  12. Sharifi, I., Shokrollahi, H., Amiri, S.: Ferrite-based magnetic nanofluids used in hyperthermia applications. J. Magn. Magn. Mater. 373, 903–915 (2012)

    Article  ADS  Google Scholar 

  13. Odenbach, S.: Colloidal Magnetic Fluids. Springer, Berlin (2009)

    Google Scholar 

  14. Cornell, R.M., Schertmann, U.: The Iron Oxides: Structure, Properties, Reactions, Occurrence and Uses. VCH, Weinheim (1996)

    Google Scholar 

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Acknowledgments

This research was funded by Russian Scientific Foundation, Project No №14-19-01379

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Correspondence to Sergey A. Novopashin .

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Novopashin, S.A., Serebryakova, M.A., Zaikovskii, A.V. (2017). Morphology, Chemical Composition, and Magnetic Properties of Arc Discharge Fe–C Soot. In: Oral, A., Bahsi Oral, Z. (eds) 3rd International Multidisciplinary Microscopy and Microanalysis Congress (InterM). Springer Proceedings in Physics, vol 186. Springer, Cham. https://doi.org/10.1007/978-3-319-46601-9_18

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