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Recent Advances in the Synthesis and Applications of Organoborane Polymers

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Book cover Synthesis and Application of Organoboron Compounds

Part of the book series: Topics in Organometallic Chemistry ((TOPORGAN,volume 49))

Abstract

Recent advances in the synthesis of organoborane polymers are reviewed in this chapter. The last decade has witnessed new approaches for the direct polymerization of functional borane monomers as well as the use of innovative polymer modification techniques. Powerful new methods that allow for positioning of functional borane moieties at well-defined positions in the polymer chain have also been developed. The resulting organoborane polymers have been investigated as luminescent and electro-active materials, electrolytes for batteries, supported Lewis acid catalysts, sensors for anions and biologically relevant molecules, building blocks of stimuli-responsive and dynamic (supramolecular) materials, and for biomedical applications.

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Abbreviations

9-BBN:

9-Borabicyclononane

AIBN:

Azobisisobutyronitrile

Alq3 :

Aluminum tris(8-hydroxyquinolate)

Ar:

Aryl

ATRP:

Atom transfer radical polymerization

COD:

1,5-Cyclooctadiene

Cp:

Cyclopentadienyl

Cp*:

Pentamethylcyclopentadienyl

CTA:

Chain transfer agent

DLS:

Dynamic light scattering

dppb:

Bis(diphenylphosphino)butane

dppp:

Bis(diphenylphosphino)propane

dtbpy:

4,4′-Di-t-butyl-2,2′-bipyridine

Fc:

Ferrocenyl or ferrocenediyl

Hex:

n-Hexyl

LCST:

Lower critical solution temperature

LLDPE:

Linear low-density polyethylene

Mes:

Mesityl (2,4,6-trimethylphenyl)

NIR:

Near infrared

NMP:

Nitroxide-mediated polymerization

OLED:

Organic light emitting device

PCL:

Poly(ε-caprolactone)

PDMA:

Poly(N,N-dimethylacrylamide)

PEG:

Polyethylene glycol

PEO:

Polyethylene oxide

pin:

Pinacolato

PLA:

Poly(lactic acid)

PMDETA:

N,N,N′,N″,N″-Pentamethyldiethylenetriamine

PNIPAM:

Poly(N-isopropylacrylamide)

PS:

Polystyrene

PSBA:

Polystyrene boronic acid

R:

Organic substituent

RAFT:

Reversible addition–fragmentation chain transfer

ROMP:

Ring-opening metathesis polymerization

St:

Styrene or styryl

TEM:

Transmission electron microscopy

T g :

Glass transition temperature

Tip:

Tripyl (2,4,6-tri-iso-propylphenyl)

TMS:

Trimethylsilyl

UCST:

Upper critical solution temperature

UV:

Ultraviolet

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Acknowledgments

The author thanks the National Science Foundation (NSF CHE-0956655, 1112195, 1308517, and 1362460) for the generous financial support. He is also indebted to all of his students and collaborators for their contributions to the work discussed in here.

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    Frieder Jäkle

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Correspondence to Frieder Jäkle .

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  1. Universitat Rovira i Virgili Directora TECAT, Tarragona, Spain

    Elena Fernández

  2. Department of Chemistry, Centre for Sustainable Chemical Processes, Durham, United Kingdom

    Andrew Whiting

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Jäkle, F. (2015). Recent Advances in the Synthesis and Applications of Organoborane Polymers. In: Fernández, E., Whiting, A. (eds) Synthesis and Application of Organoboron Compounds. Topics in Organometallic Chemistry, vol 49. Springer, Cham. https://doi.org/10.1007/978-3-319-13054-5_10

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