Skip to main content

New Perspectives for the Application of High-Resolution Benchtop X-Ray MicroCT for Quantifying Void, Solid and Liquid Phases in Soils

  • Chapter
  • First Online:
Application of Soil Physics in Environmental Analyses

Part of the book series: Progress in Soil Science ((PROSOIL))

Abstract

Recent technological advances of imaging techniques such as X-ray computed tomography (CT) provide powerful means for visualization of the soil interior to evaluate pore topological properties and structure and study dynamic processes in a noninvasive way. The objective of this chapter is to present new opportunities for the application of advanced benchtop X-ray MicroCT scanners in soil science and vadose zone research and to discuss advantages and limitations associated with the MicroCT technique. Instrumentation, spatial resolution, image contrast and other aspects that directly affect the ability to discriminate and quantify various soil phases are discussed. Analysis of nearly 400 published papers regarding the application of computed tomography in soil and porous media research indicate a surge of applications of benchtop MicroCT systems over the last few years. These instruments are becoming more affordable and popular and have great potential to significantly enhance the ability to characterize and better understand dynamic processes in soils and provide important insights for the development of advanced mathematical pore network and fluid dynamics models. New advanced benchtop MicroCT systems are very flexible in terms of sample size and image spatial resolution and provide high quality images, comparable to advanced synchrotron systems. Results of soil samples scanned at different spatial resolutions are presented and their air phase (porosity) and solid phase are evaluated and quantified. Examples of liquid phase quantification using sodium iodide as dopant are also presented for glass bead and undisturbed soil samples.

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Chapter
USD 29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD 129.00
Price excludes VAT (USA)
  • Available as EPUB and PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
USD 169.99
Price excludes VAT (USA)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info
Hardcover Book
USD 169.99
Price excludes VAT (USA)
  • Durable hardcover edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

References

  • Anderson SH, Peyton RL, Wigger JW, Gantzer CJ (1992) Influence of aggregate size on solute transport as measured using computed-tomography. Geoderma 53(3–4):387–398

    Article  Google Scholar 

  • Bailey VL, McCue LA, Fansler SJ, Boyanov MI, DeCarlo F, Kemner KM, Konopka A (2013) Micrometer-scale physical structure and microbial composition of soil macroaggregates. Soil Biol Biochem 65:60–68

    Article  CAS  Google Scholar 

  • Bellato D, Simonini P, Coste AD (2013) Microstructural and mineralogical evaluation of the effectiveness of mixing treatments in stabilized clays. Geotech Test J 36(5):742–754

    Article  Google Scholar 

  • Cameron KC, Buchan GD (2006) Porosity and pore size distribution. In: Lal R (ed) Encyclopedia of soil science. CRC Press, Boca Raton, pp 1350–1353

    Google Scholar 

  • Capowiez Y, Pierret A, Daniel O, Monestiez P, Kretzschmar A (1998) 3D skeleton reconstructions of natural earthworm burrow systems using CAT scan images of soil cores. Biol Fert Soils 27(1):51–59

    Article  Google Scholar 

  • Clausnitzer V, Hopmans JW (1999) Determination of phase-volume fractions from tomographic measurements in two-phase systems. Adv Water Resour 22(6):577–584

    Article  Google Scholar 

  • Cnudde V, Boone MN (2013) High-resolution X-ray computed tomography in geosciences: a review of the current technology and applications. Earth-Sci Rev 123:1–17

    Article  Google Scholar 

  • Costa ACS, Almeida VC, Lenzi E, Nozaki J (2002) Determination of copper, aluminum and iron in basaltic soils by sequential extractions. Quim Nova 25:548–552

    Article  Google Scholar 

  • Crestana S, Mascarenhas S, Pozzi-Mucelli RS (1985) Static and dynamic 3-dimensional studies of water in soil using computed tomographic scanning. Soil Sci 140(5):326–332

    Article  Google Scholar 

  • Crestana S, Cesareo R, Mascarenhas S (1986) Using a computed-tomography miniscanner in soil science. Soil Sci 142(1):56–61

    Article  Google Scholar 

  • Cruvinel PE, Cesareo R, Crestana S, Mascarenhas S (1990) X-rays and gamma-ray computerized minitomograph scanner for soil Science. IEEE T Instrum Meas 39(5):745–750

    Article  Google Scholar 

  • Hainsworth JM, Aylmore LAG (1983) The use of computer-assisted tomography to determine spatial-distribution of soil-water content. Aust J Soil Res 21(4):435–443

    Article  Google Scholar 

  • Heijs AWJ, Ritsema CJ, Dekker LW (1996) Three-dimensional visualization of preferential flow patterns in two soils. Geoderma 70(2–4):101–116

    Article  Google Scholar 

  • Heinemann S (1978) Computerized axial tomography-application to archeological material. Anthropol J Canada 16(3):13–16

    Google Scholar 

  • Helliwell JR, Sturrock CJ, Grayling KM, Tracy SR, Flavel RJ, Young IM, Whalley WR, Mooney SJ (2013) Applications of X-ray computed tomography for examining biophysical interactions and structural development in soil systems: a review. Eur J Soil Sci 64(3):279–297

    Article  CAS  Google Scholar 

  • Hounsfield GN (1973) Computerized transverse axial scanning (tomography) 1. Description of system. Brit J Radiol 46(552):1016–1022

    Article  CAS  PubMed  Google Scholar 

  • Iassonov P, Gebrenegus T, Tuller M (2009) Segmentation of X-ray computed tomography images of porous materials: a crucial step for characterization and quantitative analysis of pore structures. Water Resour Res 45(9):W09415

    Article  Google Scholar 

  • Ketcham RA (2005) Three-dimensional grain fabric measurements using high-resolution X-ray computed tomography. J Struct Geol 27:1217–1228

    Article  Google Scholar 

  • Kulkarni R, Tuller M, Fink W, Wildenschild D (2012) Three-dimensional multiphase segmentation of X-ray CT data of porous materials using a Bayesian Markov Random Field framework. Vadose Zone J 11. doi:10.2136/vzj2011.0082

  • Luo L, Lin H (2009) Lacunarity and fractal analyses of soil macropores and preferential transport using micro-X-ray computed tomography. Vadose Zone J 8(1):233–241

    Article  Google Scholar 

  • Macedo A, Crestana S, Vaz CMP (1998) X-ray microtomography to investigate thin layers of soil clod. Soil Tillage Res 49(3):249–253

    Article  Google Scholar 

  • Onoe M, Tsao JW, Yamada H, Nakamura H, Kogure J, Kawamura H, Yoshimatsu M (1983) Computed-tomography for use on live trees. Mater Eval 41(6):748–749

    Google Scholar 

  • Peth S (2010) Applications of microtomography in soils and sediments. Dev Soil Sci 34:73–101

    Article  CAS  Google Scholar 

  • Petrovic AM, Siebert JE, Rieke PE (1982) Soil bulk-density analysis in 3 dimensions by computed tomographic scanning. Soil Sci Soc Am J 46(3):445–450

    Article  Google Scholar 

  • Pires LF, Borges JAR, Bacchi OOS, Reichardt K (2010) Twenty-five years of computed tomography in soil physics: a literature review of the Brazilian contribution. Soil Till Res 110(2):197–210

    Article  Google Scholar 

  • Rozenbaum O, Bruand A, Trong EL (2012) Soil porosity resulting from the assemblage of silt grains with a clay phase: new perspectives related to utilization of X-ray synchrotron computed microtomography. CR Geosci 344(10):516–525

    Article  Google Scholar 

  • Singh K, Niven RK (2013) Non-aqueous phase liquid spills in freezing and thawing soils: critical analysis of pore-scale processes. Crit Rev Env Sci 43(6):551–597

    Article  Google Scholar 

  • Sorensen HO, Hakim SS, Pedersen S, Christiansen BC, Balogh ZI, Hem CP, Pasarin IS, Schmidt S, Olsen UL, Oddershede J, Frandsen C, Feidenhans’L R, Stipp SLS (2012) Non-destructive identification of micrometer-scale minerals and their position within a bulk sample. Can Mineral 50(2):501–509

    Article  Google Scholar 

  • Taina IA, Heck RJ, Elliot TR (2010) Micromorphological and X-ray mu CT study of Orthic Humic Gleysols under different management conditions. Geoderma 158(3–4):110–119

    Article  CAS  Google Scholar 

  • Tuller M, Kulkarni R, Fink W (2013) Segmentation of X-ray CT data of porous materials: a review of global and locally adaptive algorithms. In: Anderson SA, Hopmans JW (eds) Tomography and imaging of soil-water-root processes, 2nd edn, SSSA special publication 61. Soil Science Society of America, Madison, pp 157–182. ISBN 978-0-89118-958-9

    Google Scholar 

  • Vainberg EI, Kazak IA, Kurozaek VP et al (1982) Materials and method of certification of standard specimens for checking computerized X-ray tomographs. Sov J Nondestr Test+ 18(9):672–677

    Google Scholar 

  • Vaz CMP, Crestana S, Mascarenhas S, Cruvinel PE, Reichardt R, Stolf R (1989) Using a computed tomography miniscanner for studying tillage induced soil compaction. Soil Technol 2(3):313–321

    Article  Google Scholar 

  • Vaz CMP, de Maria IC, Lasso PO, Tuller M (2011) Evaluation of an advanced benchtop micro-computed tomography system for quantifying porosities and pore-size distributions of two Brazilian oxisols. Soil Sci Soc Am J 75(3):832–841

    Article  CAS  Google Scholar 

  • Wildenschild D, Sheppard AP (2013) X-ray imaging and analysis techniques for quantifying pore-scale structure and processes in subsurface porous medium systems. Adv Water Resour 51:217–246

    Article  Google Scholar 

  • Wildenschild D, Hopmans JW, Vaz CMP, Rivers ML (2002) Using X-ray computed tomography in hydrology: systems, resolutions, and limitations. J Hydrol 267(3–4):285–297

    Article  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Carlos Manoel Pedro Vaz .

Editor information

Editors and Affiliations

Rights and permissions

Reprints and permissions

Copyright information

© 2014 Springer International Publishing Switzerland

About this chapter

Cite this chapter

Vaz, C.M.P., Tuller, M., Lasso, P.R.O., Crestana, S. (2014). New Perspectives for the Application of High-Resolution Benchtop X-Ray MicroCT for Quantifying Void, Solid and Liquid Phases in Soils. In: Teixeira, W., Ceddia, M., Ottoni, M., Donnagema, G. (eds) Application of Soil Physics in Environmental Analyses. Progress in Soil Science. Springer, Cham. https://doi.org/10.1007/978-3-319-06013-2_12

Download citation

Publish with us

Policies and ethics