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Supporting Information

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Development of New Radical Cascades and Multi-Component Reactions

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Abstract

Reactions were carried out under argon, with magnetic stirring and redistilled solvents. THF and Et2O were distilled from sodium/benzophenone. CH2Cl2, acetonitrile, DMSO, NEt3 and t-BuOH were distilled from CaH2. Thin layer chromatography (TLC) was performed on Merck 60 F254 silica gel. Merck Geduran SI 60 Å silica gel (35−70 mm) was used for column chromatography. The melting points reported were measured with a Reichert hot stage apparatus and are uncorrected. IR spectra were recorded with a Bruker Tensor 27 ATR diamant PIKE spectrometer.

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Notes

  1. 1.

    (3-butyl-1-tosylaziridin-2-yl)(phenyl)methanone was synthesized in one step from (E)-1-phenylhept-2-en-1-one. Spectral data are in accordance with those described in the literature: [32].

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Authors and Affiliations

  1. Stockwell laboratory, Department of Biological Sciences, Columbia University, 550 West 120th Street, New York, NY, 10027, USA

    Marie-Hélène Larraufie

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  1. Marie-Hélène Larraufie
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Correspondence to Marie-Hélène Larraufie .

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Larraufie, MH. (2014). Supporting Information. In: Development of New Radical Cascades and Multi-Component Reactions. Springer Theses. Springer, Cham. https://doi.org/10.1007/978-3-319-01324-4_6

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