Abstract
In this study, the objective was to develop, manufacture, and test hybrid nano/microcomposites with a nanoparticle reinforced matrix and demonstrate enhancements to damage tolerance properties in the form of fracture toughness and fatigue life. The material employed was a woven carbon fiber/epoxy composite, with multi-wall carbon nanotubes (CNT) as a nano-scale reinforcement to the epoxy matrix. A direct-mixing process, aided by a block copolymer dispersant and sonication, was employed to produce the nanoparticle-filled epoxy matrix. Initial tests were performed on cast epoxy sheets (neat and with nanotubes) to determine effects of nanotubes on the matrix alone. Specimens were tested in Mode I three point bend, showing a 20 % increase in critical stress intensity factor K for nanotube-filled epoxy over neat resin. Woven carbon fiber performs were then infused with epoxy (neat and with nanotubes) by a wet layup process to produce flat composite plates. Composite specimens cut from these plates were subjected to Mode I double cantilever beam (DCB) tests (straight and tapered) showing nearly a 200 % increase in Mode-I fracture toughness G for nano-reinforced composite over reference composite. Fatigue tests were then performed on the woven carbon fiber composite in the form of cyclic short-beam three point bend to produce interlaminar shear fatigue. Stress-life curves obtained from cyclic short-bearm three point bend showed an increase of more than an order of magnitude in cyclic life at a given cyclic load between reference and nano-reinforced composite. Fatigue-fracture tests were performed on interlaminar Mode-I tapered double cantilever beams to produce Mode-I interlaminar fatigue-crack growth. The results of cyclic interlaminar Mode-I testing showed a much lower crack growth rate for nano-reinforced composite than for reference material. SEM micrographs of failed specimens also showed significant differences in fracture surface morphology between nano-reinforced and reference composite.
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Acknowledgment
This work was supported in part by ISEN (Initiative for Sustainability and Energy at Northwestern) and the Office of Naval Research with Dr. Y. D. S. Rajapakse as Program Manager.
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© 2014 The Society for Experimental Mechanics, Inc.
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Fenner, J.S., Daniel, I.M. (2014). Fracture Toughness and Fatigue Behavior of Nanoreinforced Carbon/Epoxy Composites. In: Tandon, G., Tekalur, S., Ralph, C., Sottos, N., Blaiszik, B. (eds) Experimental Mechanics of Composite, Hybrid, and Multifunctional Materials, Volume 6. Conference Proceedings of the Society for Experimental Mechanics Series. Springer, Cham. https://doi.org/10.1007/978-3-319-00873-8_6
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DOI: https://doi.org/10.1007/978-3-319-00873-8_6
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