Abstract
In this paper, Plackett–Burman design was employed for screening factors influencing phosphate-based geopolymers consolidation time, through comparing the differences between each factor at two levels. This design screens 9 factors through 12 experiments. Considered factors are: Si/P molar ratio, curing temperature, heating time, calcination of used aluminosilicate precursor, mold’s condition, aluminosilicate particle size, chemical composition of aluminosilicate precursor, pH and acidic solution. Results show that curing temperature, calcination of aluminosilicate precursor, mold’s condition and aluminosilicate particle size factors are responsible for 97.79% of the consolidation time variation. The most significant effect is attributed to curing temperature, with a contribution of 73.46%. This factor presents a negative effect. Thus, its increase generates the decrease of consolidation time. This result can be explained by the endothermic character of the geopolymeric reaction. In fact, the increase of the curing temperature activates the reaction which accelerates the kinetics of consolidation. The impact of the other factors like Si/P molar ratio, the heating time, nature of aluminosilicate precursor, pH values and the acidic solution is very small and it can be neglected, in the studied conditions. These factors did not present a kinetics influence and they haven’t a direct effect on the consolidation time.
Access this chapter
Tax calculation will be finalised at checkout
Purchases are for personal use only
References
Amara AA, Salem-Bekhit Mounir M, Alanazi FK (2013) Plackett-Burman randomization method for bacterial ghosts preparation form E. coli JM109. Saudi Pharm J 6(2):1–7
Ahuja SK, Ferreira GM, Moreira AR (2004) Application of Plackett-Burman design and response surface methodology to achieve exponential growth for aggregated shipworm bacterium. Biotechnol Bioeng 85(6):666–675
Bich C (2005) Contribution à l’étude de l’activation thermique du kaolin: évolution de la structure cristallographique et activité pouzzolanique. Doctoral dissertation, Lyon, INSA
Bui DD, Hu J, Stroeven P (2005) Particle size effect on the strength of rice husk ash blended gap-graded portland cement concrete. Cement Concr Compos 27(3):357–366
Buffat P, Borel JP (1976) Size effect on the melting temperature of gold particles. Phys Rev A 13(6):2287
Cao D, Su D, Lu B, Yang Y (2005) synthesis and structure characterization of geopolymeric material based on metakaolinite and phosphoric acid. Chin Ceram J 33
Davidovits J (2008) Geopolymer chemistry and applications, 2nd edn. Inst. Geopolymer, Sain Quentin, France
Davidovits J (2011) Geopolymers-chemistry and applications, 4th edn. Institut géopolymère, Saint-Quentin
Douiri H, Louati S, Baklouti S, Arous M, Fakhfakh Z (2014) Structural, thermal and dielectric properties of phosphoric acid-based geopolymers with different amounts of H3PO4. Mater Lett 116:9–12. https://doi.org/10.1016/j.matlet.2013.10.075
He Y, Liu L, He L, Cui X (2016) Characterization of chemosynthetic H3PO4–Al2O3–2SiO2 geopolymers. Ceram Int 42(9):10908–10912
Khan MI, Azizli K, Sufian S, Siyal AA, Man Z, Ullah H (2014) Sodium silicate free geopolymer as coating material: adhesion to steel. In: 1st International electronic conference on materials, vol 26. Multidisciplinary Digital Publishing Institute
Louati S, Baklouti S, Samet B (2016) Acid based geopolymerization kinetics: effect of clay particle size. Appl Clay Sci 132:571–578
Louati S, Hajjaji W, Baklouti S, Samet B (2014) Structure and properties of new eco material obtained by phosphoric acid attack of natural Tunisian clay. Appl Clay Sci 101:60–67. https://doi.org/10.1016/j.clay.2014.07.015
Murat M, Barchioni A (1982) Corrélation entre l’état d’amorphisation et l’hydraulicité du métakaolin. Bull Minéral 105:543–555
Sadangi JK, Muduli SD, Nayak BD, Mishra BK (2013) Effect of phosphate ions on preparation of fly ash based geopolymer. IOSR J Appl Chem 4:20–26
Stanbury PF, Whitaker A, Hall SJ (1986) Media for industrial fermentations. Principles of fermentation technology. Pergamon, Oxford, pp 93–122
Tchakouté HK, Rüscher CH, Kamseu E, Andreola F, Leonelli C (2017) Influence of the molar concentration of phosphoric acid solution on the properties of metakaolin-phosphate-based geopolymer cements. Appl Clay Sci 147:184–194. https://doi.org/10.1016/j.clay.2017.07.036
Author information
Authors and Affiliations
Corresponding author
Editor information
Editors and Affiliations
Rights and permissions
Copyright information
© 2020 Springer Nature Switzerland AG
About this paper
Cite this paper
Zribi, M., Samet, B., Baklouti, S. (2020). Screening of Factors Influencing Phosphate-Based Geopolymers Consolidation Time, Using Plackett-Burman Design. In: Chaari, F., et al. Advances in Materials, Mechanics and Manufacturing. Lecture Notes in Mechanical Engineering. Springer, Cham. https://doi.org/10.1007/978-3-030-24247-3_13
Download citation
DOI: https://doi.org/10.1007/978-3-030-24247-3_13
Published:
Publisher Name: Springer, Cham
Print ISBN: 978-3-030-24246-6
Online ISBN: 978-3-030-24247-3
eBook Packages: EngineeringEngineering (R0)