Abstract
An apparatus which has been employed for the measurement of the optical transmission and mass changes in metal films is described. The stoichiometry of the metal film is inferred from measurements carried out with an automated bakeable vacuum microbalance. The optical transmission of the film is measured for monochromatic light from 4000 to 8000 A. The experimental difficulties encountered in this study are discussed in detail.
Results obtained with this apparatus during the stepwise evaporation of a copper film are presented and briefly discussed.
Some pertinent comments concerning the design and use of pivot-type microbalances are included in an appendix.
Access this chapter
Tax calculation will be finalised at checkout
Purchases are for personal use only
Preview
Unable to display preview. Download preview PDF.
References
F. Blaha, Mikrochemie ver. Mikrochim. Acta 39, 339 (1952).
S. P. Wolsky and E. J. Zdanuk, Vacuum Microbalance Techniques, Vol. 1, Plenum Press, New York, 1961, p. 35.
H. Wieder and A. W. Czanderna, J. Phys. Chem., in press, March, 1962.
A. W. Czanderna and J. M. Honig, Anal. Chem. 29, 1206 (1957).
J. M. Honig, Vacuum Microbalance Techniques, Vol. 1, Plenum Press, New York, 1961, p. 55.
A. W. Czanderna, Vacuum Microbalance Techniques, Vol. 1, Plenum Press, New York, 1961, p. 129.
C. N. Cochran, Vacuum Microbalance Techniques, Vol. 1, Plenum Press, New York, 1961, p. 23.
H. Wieder and A. W. Czanderna, J. Chem. Physics, Vol. 35, No. 6, p. 2259, Dec. 1961.
O. S. Heavens, Optical Properties of Thin Solid Films, Butterworths, 1955.
Editor information
Editors and Affiliations
Rights and permissions
Copyright information
© 1962 Springer Science+Business Media New York
About this paper
Cite this paper
Czanderna, A.W., Wieder, H. (1962). An Apparatus for the Simultaneous Measurement of the Optical Transmission and Mass Changes in Thin Films. In: Walker, R.F. (eds) Vacuum Microbalance Techniques. Springer, Boston, MA. https://doi.org/10.1007/978-1-4899-6285-0_11
Download citation
DOI: https://doi.org/10.1007/978-1-4899-6285-0_11
Publisher Name: Springer, Boston, MA
Print ISBN: 978-1-4899-6155-6
Online ISBN: 978-1-4899-6285-0
eBook Packages: Springer Book Archive