Skip to main content

Quantity and Quality of the Nb3Sn Intermetallics Formed by the Internal Tin Process

  • Chapter
Advances in Cryogenic Engineering Materials

Part of the book series: Advances in Cryogenic Engineering ((ACRE,volume 42))

Abstract

This paper considers rather usual methods for investigating the microstructure of the Nb3Sn superconducting phase. These techniques deal with the quality and volume fraction of the Al 5 compound. Microhardness testing show very suitable in order to monotor a fabrication process. The metallurgical effects of each step of a conventional HT schedule are also studied with various designs of composites in an attempt of optimization.

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Chapter
USD 29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD 259.00
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
USD 329.99
Price excludes VAT (USA)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info
Hardcover Book
USD 329.99
Price excludes VAT (USA)
  • Durable hardcover edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

References

  1. S. Okuda, M. Suenaga, and R.L. Sabatini, “Influence of metallurgical on superconducting current densities in “bronze-processed” Nb3Sn multifilamentary wires”, J. Appl. Phys. 54: 289 (1983).

    Article  CAS  Google Scholar 

  2. D.R. Dietderich, W.V. Hassenzahl, and J.W. Morris Jr., “The Relationship between critical current and microstructure of internal tin wire”, in: “Advances in Cryogenic Engineering, Materials” 32 (1985), P. 881.

    Google Scholar 

  3. K.R. Marken, J.J. Kwon, P.L. Lee, and D.C. Larbalestier, “Characterization studies of a fully reacted high bronze niobium ration filamentary Nb3Sn composite”, in: “Advances in Cryogenic Engineering, Materials” 32 (1985), P. 967.

    Google Scholar 

  4. D. Dew-Hughes “Is Jc in Nb3Sn limited by grain-boundary flux-shear?”, IEEE Trans Mag mag-23: 1172 (1987).

    Article  Google Scholar 

  5. W. Schauer, and W. Schelb,“Improvement of Nb3Sn high field critical current by two stages reaction”, IEEE Trans. Mag. mag-17: 374 (1981).

    Article  Google Scholar 

  6. K. Osamura, “Composite Superconducting”, Dekker Publication, New York (1993), p 85.

    Google Scholar 

  7. L.M. Di, P.I. Loef, and H. Bakker, “Atomic disorder in intermetallic compound by mechanical attrition”, Mat. Sci. Eng. A134: 1323 (1991).

    Article  Google Scholar 

  8. K. Togano, and K. Tachikawa, “Textures in diffusion-processed superconducting Nb3Sn and V3Ga layers”, J Appl Phys 50(5): 3495 (1979).

    Article  CAS  Google Scholar 

  9. N. Saunders and A.P. Miodownik, Bull. Alloy Phase Diag.: 11 (1990), p. 278.

    Article  CAS  Google Scholar 

  10. R. Taillard, and C. Verwaerde “Phases transformations during the manufacturing process of Nb3Sn superconducting composites”, Proceeding. Euromat 95, VENISE (1995), p.471.

    Google Scholar 

  11. R. Flückiger, W. Goldacker, and R. Isernhagen, “Characterization of Bulk and Multifilamentary Nb3Sn and Nb3Al by Diffractometric and Resistive Measurements”, in: “Advances in Cryogenic Engineering, Materials” 32 (1985), P. 925.

    Google Scholar 

  12. R.M. Scalan, W. A. Frietz, and E.F. Koch, “Flux pinning centers in superconducting Nb3Sn”, J. Appl. Phys. 46: 2244 (1975).

    Article  Google Scholar 

  13. A.W. West, and R.D. Rawling, “transmission electron microscopy investigation of filamentary superconducting composites”, J. Mat. Sci. 12: 1862 (1977).

    Article  CAS  Google Scholar 

  14. W. Schelb, “Electron microscopy examination of multifilamentary bronze processed”, J. Mat. Sci. 16: 2575 (1981).

    Article  CAS  Google Scholar 

  15. J.R. Cave and C.A.F. Weir, IEEE Trans. Mag. mag-19: 1120 (1983).

    Article  Google Scholar 

  16. E.R. Wallach, and J.E. Evetts, “The Development in multifilamentary bronze route A 15 composites”, in: “Advances in Cryogenic Engineering, Materials” 32 (1985), P.911.

    Google Scholar 

  17. P. Gruzin, Yu Bychkov, J. Evstyukhina, V. Kruglov, and L. Alekseev, “Struktura i Svoistva Sverkhprovodyashchikh Materialov”, Moskova (1974), p 29.

    Google Scholar 

  18. De Cox and Ar Sweedler, “Comments on Móssbauer effect étudies on 2 Mev proton-irradiated Nb3Sn”, Phys. Rev. B 19: 1664 (1979.

    Article  CAS  Google Scholar 

  19. H.H. Farell, G.H. Gilmer and M. Suenaga, “Grain boundary diffusion and growth of intermetallic layers”, J. Appl. Phys A5: 4025 (1974).

    Article  Google Scholar 

  20. B.V. Reddi, V. Raghavan, S. Ray, and A.V. Narlikar,“Growth kinetics of monofilamentary Nb3Sn and V3Ga synthesized by solid-state diffusion”, J. Mat. Sci. 18: 1165 (1983).

    Article  CAS  Google Scholar 

  21. A. M. Gusak, and M.V. Yarmolenko, “A simple way describing the diffusion phase growth cylindrical and spheridrical samples”, J. Appl. Phys. 73(10): 4881 (1993).

    Article  CAS  Google Scholar 

  22. P.K. Ghosh, S. Ray, and R.C. Agarwal, “Reaction annaeling of copper-tin-copper-niobium composite”, J. Appl. Mat. Sci. Letters 3: 370 (1984).

    Article  CAS  Google Scholar 

  23. R. Roberge, H. Lehuy, and S. Foner, “X-ray observations of the low temperature phase transformation of Nb3Sn. E fleets of added elements ans strain”, Phys. B 108: 1245 (1981).

    Article  CAS  Google Scholar 

  24. C.E. Bruzek, P. Suiten, D Mocaer, S. Peltier et al., “Development of Superconducting wires for Fusion Application”, this conference.

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Editor information

Editors and Affiliations

Rights and permissions

Reprints and permissions

Copyright information

© 1996 Springer Science+Business Media New York

About this chapter

Cite this chapter

Verwaerde, C., Taillard, R., Bruzek, C.E., Hoang-Gia-Ky (1996). Quantity and Quality of the Nb3Sn Intermetallics Formed by the Internal Tin Process. In: Summers, L.T. (eds) Advances in Cryogenic Engineering Materials . Advances in Cryogenic Engineering Materials , vol 42. Springer, Boston, MA. https://doi.org/10.1007/978-1-4757-9059-7_178

Download citation

  • DOI: https://doi.org/10.1007/978-1-4757-9059-7_178

  • Publisher Name: Springer, Boston, MA

  • Print ISBN: 978-1-4757-9061-0

  • Online ISBN: 978-1-4757-9059-7

  • eBook Packages: Springer Book Archive

Publish with us

Policies and ethics