Methyl 5-(Butylthiomethyl)-2-Furoate

  • A. L. Mndzhoian

Abstract

Sodium freed from encrustation (5.75 g, i.e. 0.25 g-atom) was added to 100 ml of dry toluene (Note 1) contained in a 250-ml three-necked round-bottomed flask fitted with stirrer, dropping funnel, and reflux condenser protected by a calcium chloride tube. The mixture was heated until the sodium melted, and the stirrer was then set into motion and the application of heat was stopped; vigorous stirring was continued for 10–15 minutes, during which the temperature of the mixture fell to 40–50°. Gentle stirring of the toluene suspension of finely granulated sodium was continued at this temperature while 30 g (0.33 mole) of freshly distilled 1-butanethiol (Note 2) was added dropwise; the mixture was allowed to stand for several hours.

Keywords

Ethyl Ester Heterocyclic Compound Reflux Condenser Colorless Liquid Unpleasant Odor 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

Literature Cited

  1. 1.
    A. L. Mndzhoian and N. M. Divanian, Doklady Akad. Nauk Arm. SSR (Proc. Acad. Sci. Armenian SSR) 17, 164 (1953).Google Scholar

Copyright information

© Springer Science+Business Media New York 1959

Authors and Affiliations

  • A. L. Mndzhoian

There are no affiliations available

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