Abstract
A solution of 57.3 g (0.3 mole) of 5-bromo-2-furoic acid (see Vol. 1 of this work, p. 11),m.p. 182–183°, in 150 ml of dry benzene was prepared in a 300-ml round-bottomed flask fitted with reflux condenser protected by a calcium chloride tube, and 42.8 g (0.36 mole) of freshly distilled thionyl chloride was added.
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L. C. Raiford and W. G. Huey, J. Org. Chem. 6, 858 (1941)
I. R. Willard and C. S. Hamilton, J. Am. Chem. Soc. 75, 2370 (1953).
A. L. Mndzhoian, Zh. obshchei khim. (J. Gen. Chem.) 16, 751 (1946).
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Mndzhoian, A.L. (1959). 5-Bromo-2-Furoyl Chloride. In: Mndzhoian, A.L. (eds) Syntheses of Heterocyclic Compounds. Springer, Boston, MA. https://doi.org/10.1007/978-1-4757-6658-5_57
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DOI: https://doi.org/10.1007/978-1-4757-6658-5_57
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