N,N-Diethylfurfurylamine

  • A. L. Mndzhoian

Abstract

With stirring and cooling with ice water, 146 g (2 moles) of diethylamine was added over a period of 2.5–3 hours to 108 g (2 moles) of 85% formic acid contained in a 750-ml three-necked round-bottomed flask fitted with mercury-sealed stirrer, dropping funnel, and reflux condenser (Note 1). The reflux condenser was replaced by one set for distillation, and liquid distilling below 135° was removed from the reaction mixture. The contents of the flask were allowed to cool to room temperature, the condenser was replaced by one set for reflux, and 38.4 g (0.4 mole) of freshly distilled 2-furaldehyde, b.p. 159–161°/680 mm, was added from the dropping funnel.

Keywords

Formic Acid Water Cool Sodium Hydroxide Heterocyclic Compound Aqueous Layer 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

Literature Cited

  1. 1.
    E. A. Weilmuenster and C. N. Jordan, J. Am. Chem. Soc. 67, 415 (1945).CrossRefGoogle Scholar

Copyright information

© Springer Science+Business Media New York 1959

Authors and Affiliations

  • A. L. Mndzhoian

There are no affiliations available

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