Abstract
With stirring and cooling with ice water, 146 g (2 moles) of diethylamine was added over a period of 2.5–3 hours to 108 g (2 moles) of 85% formic acid contained in a 750-ml three-necked round-bottomed flask fitted with mercury-sealed stirrer, dropping funnel, and reflux condenser (Note 1). The reflux condenser was replaced by one set for distillation, and liquid distilling below 135° was removed from the reaction mixture. The contents of the flask were allowed to cool to room temperature, the condenser was replaced by one set for reflux, and 38.4 g (0.4 mole) of freshly distilled 2-furaldehyde, b.p. 159–161°/680 mm, was added from the dropping funnel.
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Literature Cited
E. A. Weilmuenster and C. N. Jordan, J. Am. Chem. Soc. 67, 415 (1945).
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© 1959 Springer Science+Business Media New York
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Mndzhoian, A.L. (1959). N,N-Diethylfurfurylamine. In: Mndzhoian, A.L. (eds) Syntheses of Heterocyclic Compounds. Springer, Boston, MA. https://doi.org/10.1007/978-1-4757-6658-5_54
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DOI: https://doi.org/10.1007/978-1-4757-6658-5_54
Publisher Name: Springer, Boston, MA
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