Methyl 4-(Chloromethyl)-5-Methyl-2-Furoate

  • A. L. Mndzhoian


A mixture of 14 g (0.1 mole) of methyl 5-methyl-2-furoate (see Vol. 1 of this work, p. 23), b.p. 97–99°/12 mm, 80 ml of dry chloroform (Note 1), 4.5 g of paraformaldehyde (0.15 mole, calculated as formaldehyde) and 3.4 g (0.025 mole) of anhydrous zinc chloride was prepared in a 250-ml four-necked round-bottomed flask fitted with stirrer, bent glass tube passing to the bottom of the flask and serving for the introduction of hydrogen chloride, gas-outlet tube, and thermometer.


Concentrate Hydrochloric Acid Hydrogen Chloride Colorless Needle Potassium Cyanide Reach Room Temperature 
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Literature Cited

  1. A. L. Mndzhoian, V. G. Afrikian, M. T. Grigorian, and E. A. Markarian, Doklady Akad. Nauk Arm. SSR (Proc. Acad. Sci. Armenian SSR) 25, 277 (1957).Google Scholar

Copyright information

© Springer Science+Business Media New York 1959

Authors and Affiliations

  • A. L. Mndzhoian

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