Advertisement

Ethyl (2-Furoyl) Acetate (Ethyl α-Oxo-2-Furanpropionate)

  • A. L. Mndzhoian

Abstract

A 300-ml four-necked round-bottomed flask fitted with mercury-sealed stirrer, dropping funnel, and reflux condenser protected by a calcium chloride tube was charged with 24.8 g (0.177 mole) of freshly distilled ethyl 2-furoate, m.p. 33–34°. The stirrer was set in motion, and the flask was heated in a water bath at a bath temperature of 75–80°. At this temperature 2 g of sodium wire was added (Note 1), and 8.8 g (9.8 ml) of ethyl acetate was added gradually from the dropping funnel (Note 2).

Keywords

Ethyl Acetate Bath Temperature Potassium Carbonate Ethyl Acetoacetate Dilute Hydrochloric Acid 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

Literature Cited

  1. 1.
    E. E. Royals, I. C. Hoppe, A. D. Jordan, and A. G. Robinson, J. Am. Chem. Soc. 73, 5857 (1951).CrossRefGoogle Scholar
  2. 2.
    D. S. Breslow, E. Baumgarten, and C. R. Hauser, J. Am. Chem. Soc. 66, 1286 (1944).CrossRefGoogle Scholar
  3. 3.
    S. S. Sanderlin, Ber. 33, 492, 1176 (1900).Google Scholar
  4. 4.
    G. Barger, R. Robinson, and L. H. Smith, J. Chem. Soc. 718 (1937).Google Scholar

Copyright information

© Springer Science+Business Media New York 1959

Authors and Affiliations

  • A. L. Mndzhoian

There are no affiliations available

Personalised recommendations