Abstract
The reaction was carried out in a 200-ml round-bottom flask fitted with reflux condenser protected by a calcium chloride tube. In order to trap the gases liberated during the reaction, the end of the calcium chloride tube was connected to a Tishchenko vessel containing a solution of caustic alkali. A solution of 20.2 g (0.1 mole) of 5-benzyl-2-furoic acid (see p. 7), m.p. 104–105°, in 50 ml of dry benzene was introduced into the flask, and a solution of 14.5 g (0.12 mole) of freshly distilled thionyl chloride in 30 ml of benzene was added.
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A. L. Mndzhoian, V. G. Afrikian, and A. A. Dokhikian, Doklady Akad. Nauk Arm. SSR (Proc. Acad. Sci. Armenian SSR) 17, 169 (1953).
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Mndzhoian, A.L. (1959). 5-Benzyl-2-Furoyl Chloride. In: Mndzhoian, A.L. (eds) Syntheses of Heterocyclic Compounds. Springer, Boston, MA. https://doi.org/10.1007/978-1-4757-6658-5_24
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DOI: https://doi.org/10.1007/978-1-4757-6658-5_24
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