Abstract
The response of silicon nitride to an aging treatment of 165 h at 800°C is studied with the help of four different material conditions: as received, aged, indentation pre-cracked + aged and pre-cracked + flexure-loaded + aged.
The aging treatment results in surface confined material changes that lead to high fracture toughness values and R-curve behaviour. The bulk-fracture toughness and strength are reduced. Pre-cracks heal by the formation of oxides that fill the cracks. Complete strength recovery is obtained for samll pre-cracks. Flexure-loaded pre-cracks expirience pronounced healing. In combination with possible crack closure effects this leads to an enhanced room-temperature strength of such specimens compared to the as received condition.
Access this chapter
Tax calculation will be finalised at checkout
Purchases are for personal use only
Preview
Unable to display preview. Download preview PDF.
References
T.E. Easler, R.C. Bradt, R.E. Tressler, Effects of oxidation and oxidation under load on strength distributions of Si3N4, J. Amer. Ceram. Soc., 65, 317–320 (1982).
K. Jakus, J.E. Ritter, Jr., W.P. Rogers, Strength of hot-pressed silicon nitride after high temperature exposure, J. Amer. Ceram. Soc., 67, 471–475 (1984).
S.R. Choi, V. Tikare, R. Pawlik, Crack healing in silicon nitride due to oxidation, Ceram. Eng. Sci. Proc., 12, 2190–2202 (1991).
R.J. Damani, C. Schuster, R. Danzer, Polished notch modification of SENB-S fracture toughness testing, J. Eur. Ceram. Soc., 17, 1685–1689 (1997).
J. Kübler, Fracture toughness of ceramics using the SENVB method: first results of a joint VAMAS/ESIS round robin, Ceram. Eng. Sci. Proc., to be published (1999).
J.B. Wachtman, Mechanical Properties of Ceramics, John Wiley Sons Inc., New York (1996).
G.R. Anstis, P. Chantikul, B.R. Lawn, D.B. Marshall, A critical evaluation of indentation techniques for measuring fracture toughness: I, direct crack measurements, J. Am. Ceram. Soc., 64, 533–538 (1981).
P. Chantikul, G.R. Anstis, B.R. Lawn, D.B. Marshall, A critical evaluation of indentation techniques for measuring fracture toughness: II, strength method, J. Am. Ceram. Soc., 64, 539–543 (1981).
P. Pancheri, P. Bosetti, R. Dal Maschio, V.M. Sglavo, Production of sharp cracks in ceramic materials by three-point bending of sandwiched specimens, Eng. Fract. Mech., 59, 447–456 (1998).
V.M. Sglavo: personal communication (1999).
B.R. Lawn, Fracture of Brittle Solids, Cambridge University Press, Cambridge (1993).
W. Bolse, S.D. Peteves, Indentation characterization of silicon nitride, J. Test. and Eval., 23, 27–32 (1995).
R.F. Krause, Rising fracture toughness from bending strength of indented alumina bars, J. Am. Ceram. Soc., 71, 338–343 (1988).
L.M. Braun, S.J. Bennison, B.R. Lawn, Objective evaluation of short-crack toughness curves using indentation flaws: case study on alumina-based ceramics, J. Am. Ceram. Soc., 75, 3049–3057 (1992).
M. Mitomo, T. Nishimura, M. Tsutsumi, Crack healing in silicon nitride and alumina ceramics, J. Mater. Sci. Lett., 15, 1976–1978 (1996).
S. Suresh, G.F. Zamiski, R.O. Ritchie, Oxide-induced crack closure: an explanation for near —threshold corrosion fatigue crack growth behaviour, Metall. Trans., 12A, 1435–1443 (1981).
S. Suresh, R.O. Ritchie, On the influence of environment on the load ratio dependence of fracture thresholds in pressure vessel steels, Engng. Fract. Mech., 18, 785–792 (1983).
Author information
Authors and Affiliations
Editor information
Editors and Affiliations
Rights and permissions
Copyright information
© 2002 Springer Science+Business Media New York
About this chapter
Cite this chapter
Lube, T. (2002). Improvement of the Strength of Silicon Nitride by Aging. In: Bradt, R.C., Munz, D., Sakai, M., Shevchenko, V.Y., White, K. (eds) Fracture Mechanics of Ceramics. Springer, Boston, MA. https://doi.org/10.1007/978-1-4757-4019-6_11
Download citation
DOI: https://doi.org/10.1007/978-1-4757-4019-6_11
Publisher Name: Springer, Boston, MA
Print ISBN: 978-1-4419-3370-6
Online ISBN: 978-1-4757-4019-6
eBook Packages: Springer Book Archive