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General Introduction to Sample-Controlled Thermal Analysis (SCTA)

  • J. Rouquerol
  • O. Toft Sorensen
Part of the Hot Topics in Thermal Analysis and Calorimetry book series (HTTC, volume 3)

Abstract

For a majority of technical applications, it is of upmost importance to know the behaviour of materials as they are heated or cooled. This is the objective of thermal analysis. In the beginning (say, one century ago) the sample was simply submitted to the heating from a gas burner and, later, from an electrical furnace, operated at ca constant power (as it was the case with the “micro-DTA” equipment marketed in the early sixties). This meant a certain lack of control on the heating rate and on the total duration of the experiment. It was therefore considered as a great improvement to impose a temperature programme to the sample, most often with a constant heating rate, i.e. with a constant dT/dt (where T is the sample or furnace temperature and where t is the time): the great majority of thermal analysis equipments are, nowadays, operated in this way.

Keywords

Thermal Analysis Early Sixty Upmost Importance Thermal Preparation Constant Rate Thermal Analysis 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

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References

  1. 1.
    C.S. Smith, Trans. A.I.M.E. (Metal Division) 137 (1940) 236.Google Scholar
  2. 2.
    F.H. Hayes, UMIST, Manchester, UK, personal communication.Google Scholar
  3. 3.
    L. Erdey, F. Paulik and J. Paulik, Hungarian Patent No. 152197, registered 31 October 1962, published 1 December 1965.Google Scholar
  4. 4.
    J. Rouquerol, Thesis, Faculty of Sciences of Paris University, 19 November 1964 (Série A, No. 4348, No. d’ordre 5199).Google Scholar
  5. 5.
    J. Rouquerol, Bull. Soc. Chim. Fr. (1964) 31.Google Scholar
  6. 6.
    J. Mayet, J. Rouquerol, J. Fraissard and B. Imelik, Bull. Soc. Chim. Fr. (1966) 2805.Google Scholar
  7. 7.
    A. Baumer and M. Ganteaume, C.R. Acad. Sci. 266 (1968) 120.Google Scholar
  8. 8.
    J. Rouquerolin Thermal Analysis, in Thermal Analysis, Academic Press, New York 1 (1969) 281.Google Scholar
  9. 9.
    G. Chottard, J. Fraissard and B. Imelik, Bull. Soc. Chim. Fr. (1967) 4331.Google Scholar
  10. 10.
    J. Kermarec, J. Fraissard, J. Elston and B. Imelik, J. Chim. Phys. 65 (1968) 920.Google Scholar
  11. 11.
    J. Rouquerol, J. Therm. Anal. 2 (1970) 123.CrossRefGoogle Scholar
  12. 12.
    J. Paulik and F. Paulik, Anal. Chim. Acta 56 (1971) 328.CrossRefGoogle Scholar
  13. 13.
    J. Paulik and F. Paulik in G. Svehla (Eds.) Comprehensive Analytical Chemistry, Elsevier, Amsterdam, Vol. XII, Part A (1981) 48.Google Scholar
  14. 14.
    F. Rouquerol and J. Rouquerol in H.G. Widemann (Eds.) Thermal Analysis, Vol. 1, Birkhäuser, Basel (1972) 373.Google Scholar
  15. 15.
    F. Paulik and J. Paulik, Anal. Chim. Acta 67 (1973) 437.CrossRefGoogle Scholar
  16. 16.
    J. Paulik and F. Paulik Thermal Analysis, Proc. 5th ICTA Conference, Kyoto, Heyden and Sons, London (1977).Google Scholar
  17. 17.
    O.T. Sorensen, J. Therm. Anal. 13 (1978) 429.CrossRefGoogle Scholar
  18. 18.
    O.T. Sorensen, Thermochim. Acta 50 (1980) 163.CrossRefGoogle Scholar
  19. 19.
    O.T. Sorensen in Proc. 5th Meeting of AICAT, AICAT, Trieste (1983) 25.Google Scholar
  20. 20.
    M.H. Stacey, Anal. Proc. 22 (1985) 242.Google Scholar
  21. 21.
    M. Reading, in “Thermal Analysis, Techniques and Applications” E.L. Charsley and S.B. Warrington (Eds.), Royal Society of Chemistry, Cambridge (1992) 126.Google Scholar
  22. 22.
    P.S. Gill, S.R. Sauerbrunn and B.S. Crowe, J. Thermal Analysis, 38 (1992) 255.CrossRefGoogle Scholar
  23. 23.
    A. Ortega, L.A. Pérez-Maquéda and J.M. Criado, J. Thermal Anal. 42 (1994) 551.CrossRefGoogle Scholar
  24. 24.
    P.A. Barnes, G.M.B. Parkes and E.L. Charsley, Anal. Chemistry, 66 (1994) 2226.CrossRefGoogle Scholar
  25. 25.
    P.A. Barnes, G.M.B. Parkes, D.R. Brown and E.L. Charsley, Thermochimica Acta, 269/270 (1995) 665.CrossRefGoogle Scholar
  26. 26.
    J. Rouquerol and J.M. Fulconis, ICTAC 11 Book of Abstracts, P. Gallagher (Ed.), Philadelphia (1996) 272.Google Scholar
  27. 27.
    R.L. Blaine, Proceedings of NATAS Meeting, R.J. Morgan (Ed.) (1997) 485Google Scholar
  28. 28.
    M. Reading in: M.E. Brown (Ed.), Handbook of Thermal Analysis and Calorimetry, Elsevier, 1998 (Chapter 8).Google Scholar
  29. 29.
    G.M.B. Parkes, P.A. Barnes, E.L. Charsley, M. Reading and I. Abrahams, Thermochimica Acta, 354 (2000) 39.CrossRefGoogle Scholar

Copyright information

© Springer Science+Business Media Dordrecht 2003

Authors and Affiliations

  • J. Rouquerol
    • 1
  • O. Toft Sorensen
    • 2
  1. 1.Madirel LaboratoryCNRS-Université de ProvenceMarseilleFrance
  2. 2.Risoe National LaboratoryRoskildeDenmark

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