Skip to main content

Selection of Lubricants and Thread Compounds for Oxygen Missile Systems

  • Conference paper
Book cover Advances in Cryogenic Engineering

Part of the book series: Advances in Cryogenic Engineering ((ACRE,volume 6))

Abstract

The missile industry has been concerned from the beginning about the presence of lubricants in oxygen systems because the use of some of these compounds may lead to burnouts and to disastrous explosions. Although lubrication of oxygen equipment is discouraged by the oxygen industry, as well as by the missile designers, it is essential in the operation of some types of equipment such as compressors, pumps and valves. Furthermore, in the pipefitting and plumbing trades, it is a standard and necessary practice to lubricate the joints and threads of pipe, tubing and related fittings to reduce friction and seizing and to assure a tight connection, In the installation of the complex propellant systems of liquid oxygen-kerosene—powered missiles, these compounds have assumed extraordinary importance because most of them are easily oxidized and thus their use can constitute a potential hazard, This brief study aims to analyze the reasons behind the special role played by these compounds in missile oxygen systems and to find means of reducing the hazards resulting from their usage by evolving criteria for selecting safe compounds.

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Chapter
USD 29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD 84.99
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
USD 109.99
Price excludes VAT (USA)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

References

  1. W.E. Tournay, F.M. Bower, and.F.W. Brown, “Safety and Performance Characteristics of Liquid Oxygen Explosives,” Bulletin No. 472, Bureau of Mines, U. S. Government Printing Office, Washington, D.C. (1949).

    Google Scholar 

  2. Military Procurement Specification, QPL 5542–6, “Thread Compound, Anti-Seize and Sealing, Oxygen Systems,” U.S. Government Printing Office (July 12, 1954).

    Google Scholar 

  3. Military Specification, Mil-T-5542B (ASG), “Thread Compound, Anti-Seize and Sealing, Oxygen Systems,” U.S. Government Printing Office (July 12, 1954).

    Google Scholar 

  4. Rocketdyne, Division of North American Aviation, “Sealing Compound, Threads and Gaskets for Liquid Oxygen Service,” Materials Specification No, NA2–20502B, Canoga Park, California (June 13, 1957).

    Google Scholar 

  5. Broadview Research Corporation, “Explosive Hazards of Lubricants and Sensitivity of JP4-LOX Mixtures,” Report No. BRD-57–5A1,” Burlingame, California (April, 1957).

    Google Scholar 

  6. Douglas Aircraft Company, “Impact Sensitivity of Materials with Oxygen,” Laboratory Reports: MP 10.792 (August 2, 1957);

    Google Scholar 

  7. Douglas Aircraft Company, “Impact Sensitivity of Materials with Oxygen,” Laboratory Reports: MP 11,076 (May 8, 1958);

    Google Scholar 

  8. Douglas Aircraft Company, “Impact Sensitivity of Materials with Oxygen,” Laboratory Reports: MP 11.215 (September 30, 1958);

    Google Scholar 

  9. Douglas Aircraft Company, “Impact Sensitivity of Materials with Oxygen,” Laboratory Reports: MP 11.272 (December 5, 1958);

    Google Scholar 

  10. Douglas Aircraft Company, “Impact Sensitivity of Materials with Oxygen,” Laboratory Reports: MP 11.303 (January 21, 1959);

    Google Scholar 

  11. Douglas Aircraft Company, “Impact Sensitivity of Materials with Oxygen,” Laboratory Reports: MP 11.303A (August 17, 1959);

    Google Scholar 

  12. Douglas Aircraft Company, “Impact Sensitivity of Materials with Oxygen,” Laboratory Reports: MP 11.3031 (April 19, 1960); Santa Monica, California.

    Google Scholar 

  13. H. M. Peckham and R. L. Bauser, “Compatibility of Materials with Liquid Oxygen,” Advances in Cryogenic Engineering, Vol. 4, K.D. Timmerhaus (ed.), Plenum Press, Inc., New York (1960).

    Google Scholar 

  14. C.H. Reynales, “Compatibility of Materials with Oxygen,” Propulsion Report No. D81–444, Douglas Aircraft Company, Long Beach, California (October 1, 1958).

    Google Scholar 

  15. Rocketdyne, Division of North American Aviation, “Lubricants, Anti-Seize Compounds, and Gasketing Type Sealing Compounds for Rocket Engines,” Process Specification No. RA 01 12–002, Canoga Park, California (November 12, 1958).

    Google Scholar 

  16. W. Seals, “Tabulation of Impact Sensitivity Data,” Laboratory Report EMI. 1997, Reaction Motors Division, Thiokol Chemical Corporation, Denville, New Jersey (March 4, 1959).

    Google Scholar 

  17. F.J. Walker, “Liquid Oxygen Detonation Tests,” Flight Propulsion Laboratory Report, General Electric Company, Malta Test Station, New York (February 27, 1957).

    Google Scholar 

  18. International Acetylene Association, “Recommendations on Anti-Friction Compounds for Use with Gaseous Oxygen,” New York (February 1, 1956).

    Google Scholar 

  19. Ramo-Woolridge Corporation, “Minutes of Meeting of Lox-Lubricants Standards-Committee,” GM 67.6–10 (August 13, 1957).

    Google Scholar 

  20. T.J. Carter, “Procedure for Testing Materials in Liquid Oxygen, “ Technical Note 1–30, Army Ballistic Missile Agency, Huntville, Alabama (March 24, 1956).

    Google Scholar 

  21. A. Africano, “Maximum Rate Theory of Impact Sensitivity,” Advances in Cryogenic Engineering, Vol. 5, K.D. Timmerhaus (ed.), Plenum Press, Inc., New York (1960).

    Google Scholar 

  22. W.M. Orr, “Results of Lox-Lubricant Impact Sensitivity Cooperative Test Program,” Technical Note No. 58–344, Wright Air Development Center, Dayton, Ohio (November, 1958).

    Google Scholar 

  23. R. C. Kopituk, “A Method for Determining the Impact Sensitivity Characteristics of Materials with Highly Reactive Oxidizers,” Eeaction Motors Division, Thikol Chemical Corporation, Proceedings of the Annual Meeting of the A.S.T.M., Atlantic City. (June 26-July 1, 1960).

    Google Scholar 

  24. Aerospace Industries Association, “Minutes’ of Meeting of Aircraft Research and Testing Committee Project 18–58, Liquid Oxygen Systems Cleanliness, ” Los Angeles (April 30, 1959; October 20, 1959; January 18, 1960; July 18, 1960).

    Google Scholar 

  25. W. Seals, “Impact Sensitivity of Halocarbon 411-V and Ucon LB-65 Blends with Liquid Oxygen Using Different Plummet Heights,” Laboratory Report No, EML 1385A, Reaction Motors, Division, Thiokol Chemical Corporation, Denville, New Jersey (September 2, 1959).

    Google Scholar 

  26. W. Seals, “Liquid Oxygen Impact Sensitivity of ARTC Project 18–58 Test Samples,” Laboratory Report No. 1416, Reaction Motors Division, Thiokol Chemical Corporation, Denville, New Jersey (October 13, 1959).

    Google Scholar 

  27. Convair-Astronautics, “Lubrication of Threaded Fittings,” Manufacturing Procese Specification No. 24–05A, San Diego, California (November 13, 1957).

    Google Scholar 

  28. Convair-Astronautics, “Thread Compounds Anti-Seize and Sealing, Gaseous and Liquid Oxygen Systems,” Report No. 0.73.001, San Diego, California (January 12, 1957).

    Google Scholar 

  29. Douglas Aircraft Company, “Anti-Seize Lubricants for Mating Parts,” Process Specification No. 1.22, Santa Monica, California (March 27, 1958).

    Google Scholar 

  30. Douglas Aircraft Company, “Oxygen-Safe Dry Film Lubricants for Mating Parts,” Process Specification No, 3.75, Santa Monica, California (August 27, 1959).

    Google Scholar 

  31. C. H. Reynales, “Safety Aspects in the Design and Operation of Oxygen Systems,” Engineering Paper No. 713, Douglas Aircraft Company, Long Beach. California (January 21. 1959).

    Google Scholar 

  32. Halocarbon Corporation, “Halocarbon Oils and Greases,” Technical Data Bulletin, Hackensack, New Jersey (1959).

    Google Scholar 

  33. Hooker Chemical Company, “Fluorolubes,” Technical Bulletin No. 30, Niagara Falls, New York (1952).

    Google Scholar 

  34. Hooker Chemical Company, “Pluorolube Greases,” Technical Bulletin No. 41, Niagara Palls, New York (1955).

    Google Scholar 

  35. Hooker Chemical Company, “Safe Lubricants for Oxygen Systems,” Technical Bulletin No. 472, Niagara Palls, New York (1953).

    Google Scholar 

  36. J.V. Milewski and W. Fishgrund, “Pluorocarbon Materials in the X-15 and Other Rocket Engines,” Reaction Motors Division, Thiokol Chemical Corporation, Proceedings of the Fluorine Symposium, American Chemical Society, Atlantic City (September 14–18, 1959).

    Google Scholar 

  37. Minnesota Mining and Manufacturing Company, “Kel-F Halofluorocarbon Oils, Waxes, Greases, and Alkanes,” Technical Data Bulletin, St. Paul, Minnesota (1958).

    Google Scholar 

  38. Anonymous, “Fluorocarbons,” Special Report, Chem. Eng. News, Vol. 38, No. 29, p. 92 (July 18, 1960).

    Google Scholar 

  39. Ehrenfeld, “Polychlorotrifluoroethylene Oils as Industrial Lubricants,” Ind. Eng. Chem., Vol. 52, No. 2.p. 65A (February, 1960).

    Google Scholar 

  40. Convair-Astronautics, “Fluorolube-Aluminum Detonation Point,” Report 7E-1500, San Diego, California (May 12, 1958).

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Editor information

Editors and Affiliations

Rights and permissions

Reprints and permissions

Copyright information

© 1961 Springer Science+Business Media New York

About this paper

Cite this paper

Reynales, C.H. (1961). Selection of Lubricants and Thread Compounds for Oxygen Missile Systems. In: Timmerhaus, K.D. (eds) Advances in Cryogenic Engineering. Advances in Cryogenic Engineering, vol 6. Springer, Boston, MA. https://doi.org/10.1007/978-1-4757-0534-8_11

Download citation

  • DOI: https://doi.org/10.1007/978-1-4757-0534-8_11

  • Publisher Name: Springer, Boston, MA

  • Print ISBN: 978-1-4757-0536-2

  • Online ISBN: 978-1-4757-0534-8

  • eBook Packages: Springer Book Archive

Publish with us

Policies and ethics