Abstract
A sample is pyrolyzed in the presence of carbon to quantitatively convert oxygen to carbon monoxide. Helium elutes the pyrolysis products through a molecular sieve column for separation of the carbon monoxide and through a katharometer for quantitative measurement. Analysis time is 15 — 30 min, detectability is 30 ppm, no blank is involved, and less than 50 mg of sample is used.
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References
J.T. Gilmore and D.E. Hull, Anal. Chem. 35: 1623 (1963).
R. A. Stallwood, W.E. Mott, and D.T. Finale, Anal. Chem. 35: 6 (1963).
R.R. Suchanec, doctoral thesis, University of Pittsburgh (1961). [Available from University Microfilms, Inc., Ann Arbor, Michigan (1962).]
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© 1965 Chicago Section of the Society for Applied Spectroscopy
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Boys, F.L., Dworak, D.D. (1965). Gas Chromatographic Determination of Total Oxygen in Organic Materials. In: Davis, E.N. (eds) Developments in Applied Spectroscopy. Developments in Applied Spectroscopy, vol 4. Springer, Boston, MA. https://doi.org/10.1007/978-1-4684-8691-9_31
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DOI: https://doi.org/10.1007/978-1-4684-8691-9_31
Publisher Name: Springer, Boston, MA
Print ISBN: 978-1-4684-8693-3
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