Abstract
The need for highly purified solvents for use in pesticide residue analysis has become increasingly apparent, particularly with the relatively recent introduction of new and more highly sensitive detection systems. With this increase in the need for pure solvents, several commercial firms are now supplying “high-purity” solvents produced by careful distillation of the technical grade.1 Table I lists these firms through the year 1965.
This is a preview of subscription content, log in via an institution.
Buying options
Tax calculation will be finalised at checkout
Purchases are for personal use only
Learn about institutional subscriptionsPreview
Unable to display preview. Download preview PDF.
References
Anderson, C. A.: Personal communication (Chemagro Corp., Kansas City, Mo. 1965).
Ashmore, S. A.: Preparation of cyclohexane for spectroscopic work. Analyst 72, 206 (1947).
Association of Official Agricultural Chemists: Sulphenone (p-chlorophenyl phenyl sulfone)—official final action. In: Official methods of analysis, 10th ed., Washington, D.C. (1965).
Atlas Chemical Industries, Inc.: Measuring adsorptive capacity of activated carbons for liquid purification. Bull. D-87. Wilmington 99, Delaware 1966.
Beckman, H., and W. O. Gauer: Solvent purification for residue analysis by non- distillation methods. Presented meeting Amer. Chem. Soc., Phoenix, Ariz. (Jan. 16–21, 1966).
Blinn, R. C., F. A. Gunther, and M. J. Kolbezen: Microdetermination of the acaricide ethyl p,p’-dichlorobenzilate (Chlorobenzilate). J. Agr. Food Chem. 2, 1080 (1954).
Brierley, E., and H. J. Smith: Changes occurring in active alumina on storage. J. Chromatog., 14, 499 (1964).
Bruce, R. B., J. W. Howard, and J. b. Zink: Determination of diphenylamine residues on apples. J. Agr. Food Chem. 6, 597 (1958).
Dasler, W., and C. D. Bauer: Removal of peroxides from organic solvents. Ind. Eng. Chem., anal. ed. 18, 52 (1946).
Emmett, P. H. ed.: Catalysis, vol. VII, p. 140. New York: Reinhold (1960).
Gordon, C. F., L. D. Haines, and A. L. Wolfe: A procedure for the microdetermination of l-butoxy-2-(2-thiocyanoethoxy)-ethane (Lethane 384) with applications for determination of residues in milk and animal tissues. J. Agr. Food Chem. 9, 478 (1961).
Gordon, C. F., L. D. Haines, and I. Rosenthal: Analytical method for determining 1, l-dichloro-2, 2- bis(p-ethyl phenyl) ethane in rat fat and cow’s milk. J. Agr. Food Chem 10, 380 (1962).
Mair, B. J.: Separation of hydrocarbons with silica gel. J. Research National Bur. Standards 15, 51 (1935).
Mair, B. J.: Separation of hydrocarbons by adsorption. J. Research National Bur. Standards 34, 435 (1945).
Mair, B. J., and A. F. Forziah: Analytical determination of aromatic hydrocarbons. J. Research National Bur. Standards 32, 151 (1944 a).
Mair, B. J., and A. F. Forziah.,: Separation and recovery of aromatic hydrocarbons from paraffins and naphthenes by adsorption. J. Research National Bur. Standards 32, 165 (1944 b).
Mair, B. J., and M. Shamaiengar: Fractionation of certain aromatic hydrocarbons with molecular sieve adsorbants. Anal. Chem. 30, 276 (1958).
Murphy, R. T., and W. F. Barthel: Determination of heptachlor and heptachlor epoxide in soil. J. Agr. Food Chem. 6, 442 (1960).
Nakanishi, K.: Infrared absorption spectroscopy. San Francisco: Holden-Day (1964).
Ordas, E. P., V. C. Smith, and C. F. Meyer: Spectrophotometric determination of heptachlor and technical chlordan on food and forage crops. J. Agr. Food Chem. 4, 444 (1956).
Pittsburgh Activated Ccvrbon Co.: Basic concepts of adsorption of activated carbon. Pittsburgh, Pa., 1966.
Rosenthal, I., C. F. Gordon, and E. L. Stanley: Microdetermination of TDE in spray residues. J. Agr. Food Chem. 7, 486 (1959).
Rosenthal, I., C. F. Gordon, and E. L. Stanley, and M. H. Perlman: Microdetermination of the fungicide dinitro- caprylphenylcrotonate in food crops and animal tissues. J. Agr. Food Chem. 5, 914 (1957).
Snyder, L. R.: Linear elution adsorption chromatography. II. Compound separability with alumina as adsorbant. J. Chromatog. 6, 22 (1961).
Strain, H. H.: Chromatographic adsorption analysis. Ind. Eng. Chem., anal, ed. 14, 245 (1942).
Strohmeyer, F.: Personal communication (Alupharm Chemicals, New Orleans, La., 1966).
Thornburg, W.: Preparation and extraction of samples prior to pesticide residue analysis. J. Assoc. Official Agr. Chemists 48, 1023 (1965).
U.S. Food and Drug Administration: Combustion product gas. In: Food additives analytical manual, vol. I. U.S. Dept. of Health, Education, and Welfare, Food and Drug Administration (1965 a).
U.S. Food and Drug Administration: Ethoxyquin. Ibid. (1965 b).
U.S. Food and Drug Administration: Metaldehyde. Ibid. (1965 c).
U.S. Food and Drug Administration: Monoglyceride Citrate.Ibid. (1965 d).
U.S. Food and Drug Administration: Petrolaum. Ibid. (1965 e).
U.S. Public Health Service: Arsenic in air by diethyldithiocarbamate method. In: The analysis of pesticide residues, vol. II., US. Dept. of Health, Education, and Welfare, Public Health Service (1965).
Waldron, A. C, N. R. Pasarela, M. H. Woolford, and J. H. Ware: Improved colorimetric determination of phorate residues in plant tissues. J. Agr. Food Chem. 11, 241 (1963).
Weissberger, A., E. S. Proskauer, J. A. Riddick, and E. E. Toops, Jr.: Organic solvents, 2nd ed. New York-London: Interscience (1955).
White, R. G.: Handbook of industrial infrared analysis, pl08. New York: Plenum Press (1964).
Woelm Publication: AL10 (M. Woelm Eschwege). Thin-layer chromatography with Woelm adsorbants. Germany 1961.
Woelm Publication: Bull. AL-11 (M. Woelm Eschwege), p. 12. Germany 1966.
Wohlleben, G: Zur Wasseraufnahme von aktiven Aluminiumoxyd. J. Chromatog. 1,271 (1958).
Author information
Authors and Affiliations
Editor information
Editors and Affiliations
Rights and permissions
Copyright information
© 1967 Springer-Verlag New York Inc.
About this paper
Cite this paper
Beckman, H., Gauer, W.O. (1967). Solvent purification for residue analysis by non-distillation methods. In: Gunther, F.A. (eds) Residue Reviews / Rückstands-Berichte. Residue Reviews / Rückstandsberichte, vol 18. Springer, New York, NY. https://doi.org/10.1007/978-1-4615-8422-3_1
Download citation
DOI: https://doi.org/10.1007/978-1-4615-8422-3_1
Publisher Name: Springer, New York, NY
Print ISBN: 978-1-4615-8424-7
Online ISBN: 978-1-4615-8422-3
eBook Packages: Springer Book Archive