Abstract
The production of highly perfect crystals is of considerable scientific and technical importance, and there has been increasing interest in methods of examining crystal perfection. X-ray topographic methods provide abundant information on lattice defects of various scales. A major area of development in recent years has been the determination of crystal perfection by the direct observation of growth defects. X-ray topography here has considerable advantages over electron microscopy and optical methods. The sensitivity is high, while it is possible to examine the bulk distribution of various kinds of defects in comparatively large specimens. Here we consider methods that allow one to examine macroscopic defects (block structure) and microscopic ones (dislocations, inhomogeneous impurity distributions, inclusions, and so on), and results are given from these methods applied to crystals grown under various conditions.
Access this chapter
Tax calculation will be finalised at checkout
Purchases are for personal use only
Preview
Unable to display preview. Download preview PDF.
Literature Cited
T. Fujiwara, Memoirs Defense Acad. Japan, 2: 127 (1963).
T. Fujiwara, K. Koizume, and M. Hirose, Memoirs Defense Acad. Japan, 4: 361 (1965).
B. M. Rovinskii and E. P. Kostyukova, Kristallografiya, 13: 302 (1968).
E. P. Kostyukova, Kristallografiya, 15: 769 (1970).
B. M. Rovinskii, E. P. Kostyukova, and V. G. Lyuttsau, In: X-radiography of Metals, edited by Ya. S. Umanskii [in Russian], Metallurgiya, Moscow (1967), p. 8.
L. G. Schulz, Trans. AIME, 200: 1082 (1954).
V. A. Sazonova and A. A. Kralina, Fiz. Met. Metalloved., 26: 1021 (1968).
H. Berger, J. Bohm, and H. Wadewitz, Kristall und Technik, 2: 129 (1967).
K. Kranjc, J. Appl. Crystallogr., 1: 227 (1968).
C. S. Barrett, Trans. AIME, 161: 15 (1945).
C. Bosquet, M. Lambert, et al., Acta Crystallogr., 16: 989 (1963).
R. J. Towner and J. A. Berger, Trans. Met. Soc. AIME, 218: 339 (1960).
B. M. Rovinskii, Izv. AN SSSR, Ser. Fiz., 17: 333 (1953).
H. Barth, Z. Naturforsch., 13a: 680 (1958).
H. Wadewitz, In: Growth of Crystals, vol. 5 [in Russian], Nauka, Moscow (1965), p. 309. [English translation: Consultants Bureau, New York (1968), p. 257]
J. Auleitner, Postepy Fizyki, 1: 77 (1959).
V. P. Makarov and B. V. Molotilov, Zavod. Lab., 36: 187 (1970).
A. R. Lang, J. Appl. Phys., 30:1749 (1959); Brit. J. Appl. Phys., 14: 904 (1963).
S. B. Austerman and J. B. Newkirk, In: Advances in X-Ray Analysis, vol. 10, Plenum, New York (1967), p. 134.
Yu. M. Fishman, Apparatus and Methods for X-Ray Analysis, issue 6 [in Russian] (1970), p. 16.
H. Barth and R. Hosemann, Z. Naturforsch., 13a: 782 (1958).
G. Dionne, J. Appl. Phys., 38: 4094 (1967).
B. K. Tanner and C. J. Humphreys, J. Phys. (D): Appl. Phys., 3: 1144 (1970).
S. Hosoya, Japan J. Appl. Phys., 7: 1 (1968).
V. G. Lyuttsau and Yu. M. Fishman, Kristallografiya, 14: 835 (1969).
P. Penning and D. Polder, Philips Res. Repts., 16: 419 (1961).
N. Kato, J. Phys. Soc. Japan, 18:1785 (1963); 19: 67, 971 (1964).
S. Takagi, Acta Crystallogr., 15:1371 (1962); J. Phys. Soc. Japan, 26: 1239 (1969).
V. L. Indenbom and F. N. Chukhovskii, Usp. Fiz. Nauk, 107: 229 (1972).
A. Authier, In: Advances in X-Ray Analysis, vol. 10, Plenum Press, New York (1967), p. 9.
A. R. Lang and M. Polcarova, Proc. Roy Soc., A285: 297 (1965).
A. R. Lang, Z. Naturforsch., 20a: 636 (1965).
V. F. Miuskov and L. S. Milevskii, Neorgan. Mat., 1: 1267 (1966).
L. N. Danil’chuk, Fiz. Tverd. Tela, 11: 3085 (1969).
C. A. Wallace and E. A. D. White, Crystal Growth, Pergamon Press, New York (1967), p. 431.
A. R. Lang, Appl. Phys. Letters, 7: 168 (1965).
A. C. McLaren and P. P. Phakey, Phys. Stat. Sol., 31: 723 (1969).
P. P. Phakey, Phys. Stat. Sol., 34: 105 (1969).
W. J. Takei and M. H. Francombe, Brit. J. Appl. Phys., 18: 1589 (1967).
C. A. Wallace, Z. Kristallogr., 126: 444 (1968).
N. Kato, K. Usami, and T. Katagawa, In: Advances in X-Ray Analysis, vol. 10, Plenum Press, New York (1967), p. 46.
A. Authier, Phys. Stat. Sol., 27: 77 (1968).
M. Sauvage and C. Malgrange, Phys. Stat. Sol., 37: 759 (1970).
K. Kohra and M. Yoshimatsu, J. Phys. Soc. Japan, 17: 1041 (1962).
J. Chikawa and S. B. Austerman, J. Appl. Crystallogr., 1: 165 (1968).
A. R. Lang, Z. Naturforsch., 27a: 461 (1972).
Yu. M. Fishman and V. G. Lutsau, Phys. Stat. Sol. (a), 3: 829 (1970).
Yu. M. Fishman and V. G. Lutsau, Acta Crystallogr., A28: S226 (1972).
A. R. Lang, Crystal Growth, Pergamon Press, New York (1967), p. 833.
K. Furusho, Japan. J. Appl. Phys., 3: 203 (1964).
J. Chikawa, In: Advances in X-Ray Analysis, vol. 10, Plenum Press, New York (1967), p. 153.
S. S. Gorelik, V. A. Mironenko, et al., Kristallografiya, 15: 1089 (1970).
U. Bertocci, C. Bertocci, and F. W. Young, J. Appl. Phys., 40: 1674 (1969).
T. I. Ol’khovnikova, I. L. Shul’pina, et al., Fiz. Tverd. Tela, 13: 609 (1971).
G. H. Schwuttke, J. Appl. Phys., 53: 2760 (1962).
N. Kato and Y. Ando, J. Phys. Soc. Japan, 21: 964 (1966).
A. Authier and A. R. Lang, J. Appl. Phys., 35: 1956 (1964).
N. Kato and J. R. Patel, Appl. Phys. Letters, 13: 42 (1968).
V. O. Esin, Fiz. Met. Metalloved., 15: 917 (1963).
I. Sosina and L. I. Meleshko, In: Growth and Imperfection of Metal Crystals [in Russian], Kiev (1966), p. 211.
G. V. Indenbaum, V. B. Zernov, and Yu. M. Fishman, Fiz. Met. Metalloved., 24:107 (1967)
E. P. Kostyukova, B. K. Kazurov, V. G. Lyuttsau, and V. I. Sidenko, In: Growth of Crystal vol. 7 [in Russian], Nauka, Moscow (1967), p. 147. [English translation: Consultants Bureau, New York (1969), p. 124]
V. M. Koltygin, E. P. Kostyukova, and M. V. Pikunov, Abstracts for the Sixth All-Union Conference on Production, Structure, Physical Parameters, and Applications of Single Crystals of Refractory and Rare Metals [in Russian], Moscow (1967).
A. A. Kralina, L. V. Smirnov, et al., Fiz. Met. Metalloved., 33: 113 (1972).
D. Jaffrey and G. A. Chadwick, Phil. Mag., 18: 573 (1968).
D. A. Curits and J. S. Thorp, Brit. J. Appl. Phys., 16: 734 (1965).
V. O. Esin and A. A. Kralina, Fiz. Met. Metalloved., 13: 577 (1962).
I. K. Zasimchuk and D. E. Ovsienko, Ukr. Fiz. Zh., 9: 10 (1964).
R. L. Barns, Metall. Adv. Electron Mater. (1963), p. 337.
E. N. Sosina and D. E. Ovsienko, Fiz. Met. Metalloved., 3: 527 (1956).
A. E. Jenkinson and A. R. Lang, Direct Observation of Imperfections in Crystals, New York (1962), p. 471.
J. F. Petroff and A. Authier, Phys. Stat. Sol., 13: 373 (1966).
A. S. T. Badrick and E. Puttick, Phil. Mag., 23: 585 (1971).
V. F. Miuskov and A. R. Lang, Kristallografiya, 8: 672 (1963).
A. R. Lang and V. F. Miuscov, Phil. Mag., 10: 263 (1964).
L A. Blech and E. S. Meieran, Phil. Mag., 14: 275 (1966).
G. M. McManus, R. H. Hopkins, and W. J. Takei, J. Appl. Phys., 40: 180 (1969).
J. L. Caslaysky, C. P. Gazzara, and R. M. Middleton, Phil. Mag., 95: 35 (1972).
M. Oguro and H. Higashi, Phil. Mag., 24: 713 (1971).
C. A. May and J. S. Shah, J. Mater. Sci., 4: 179 (1969).
A. Authier and M. Sauvage, Rev. Intern. Hautes Temp. et Refract., 7: 94 (1970).
C. C. Wang and S. H. McFarlane, J. Cryst. Growth, 3 /4: 485 (1968).
F. W. Young, Crystal Growth, Pergamon Press, New York (1967), p. 789.
S. H. McFarlane and C. Elbaum, J. Appl. Phys., 39: 2024 (1967).
Z. Ishii, T. Furuoya, et al., J. Phys. Soc. Japan, 15: 206 (1960).
V. T. Bublik, S. S. Gorelik, and M. A. Khatsernov, Elektronnaya Tekhnika, Ser. 12, No. 1 (7), 23 (1971).
W. W. Webb and C. E. Hayes, Phil. Mag., 16: 309 (1967).
S. Ikeno, H. Maruyama, and N. Kato, J. Cryst. Growth, 3 /4: 683 (1968).
S. H. Emara, B. R. Lawn, and A. R. Lang, Phil. Mag., 19: 7 (1969).
V. G. Lutsau, Yu. M. Fishman, and I. S. Res, Kristall und Technik, 5: 445 (1970).
Yu. M. Fishman, Kristallografiya, 17: 607 (1972).
V. F. Miuskov, V. P. Konstantinova, and A. I. Gusev, Kristallografiya, 13: 909 (1968).
Z. Malek, M. Polcarova, et al., Phys., Stat. Sol. (a), 11: 195 (1972).
H. Klapper, J. Cryst. Growth, 10: 13 (1971).
J. T. McDermott and P. P. Phakey, Phys. Stat. Sol. (a), 8: 505 (1971).
J. di Persio and B. Escaig., Cryst. Lattice Defects, 3: 55 (1972).
S. B. Austerman, D. K. Smith, and H. W. Newkirk, Crystal Growth, Pergamon Press, New York (1967), p. 813.
Y. Takano, K. Kohn, et al., Japan J. Appl. Phys., 9: 847 (1970).
R. F. Belt, In: Advances in X-Ray Analysis, vol. 10, Plenum Press, New York (1967), p. 159.
R. F. Belt, J. Appl. Phys., 40: 1644 (1969).
W. J. Spencer and K. Haruta, J. Appl. Phys., 37: 549 (1966).
A. R. Lang and V. F. Miuscov, J. Appl. Phys., 39: 2477 (1967).
A. C. McLaren, C. F. Osborne, and L. A. Sanders, Phys. Stat. Sol. (a), 4: 235 (1971).
L. A. Gordienko, V. F. Miuskov, et al., Kristallografiya, 13: 539 (1969).
F. Lefaucheux, J. Cryst. Growth, 13 /14: 272 (1972).
B. R. Lawn, Y. Kamiya, and A. R. Lang, Phil. Mag., 12: 177 (1965).
A. R. Lang, Proc. Roy. Soc., A278: 234 (1964).
W. L. Spencer and W. L. Smith, J. Appl. Phys., 37: 2557 (1966).
A. R. Lang and V. F. Miuskov, In: Growth of Crystals, vol. 7 [in Russian], Izd. Nauka (1967), p. 133. [English translation: Consultants Bureau, New York (1969), p. 112]
V. T. Ushakovskii, L. I. Chernyi, and P. I. Nikitichev, Dokl. AN SSSR, 192: 1040 (1970).
P. P. Phakey and J. R. Leonard, J. Appl. Crystallogr., 3: 38 (1970).
M. Sauvage and A. Authier, Bull. Soc. Franc. Miner. Cryst., 88: 379 (1965).
A. Zarka, Bull. Soc. Franc. Miner. Cryst., 92: 160 (1969).
Yu. M. Fishman, Neorg. Mat>, 8: 2224 (1972).
S. Amelinckz, G. Strunane, and W. W. Webb, J. Appl. Phys., 31: 1359 (1960).
K. Ohta, T. Tornita, and T. Watanabe, Japan. J. Appl. Phys., 4: 652 (1965).
I. N. Frantsevich and V. A. Kravets, In: Silicon Carbide [in Russian], Naukova Dumka, Kiev (1966), pp. 12, 17.
V. M. Al’tshuller, E. A. Belousova, et al., Fiz. Tverd. Tela, 14: 296 (1972).
J. Chikawa and T. Nakayama, J. Appl. Phys., 35: 2493 (1964).
M. Ya. Skorokhova and L. N. Datsenko, Kristallografiya, 11: 300 (1966).
W. Moling, J. Cryst. Growth, 1: 115 (1967).
D. Michell and G. Ogilvie, Phys. Stat. Sol., 15: 83 (1966).
Chr, Nanev and M. Wilkens, Phys. Stat. Sol., 32: 839 (1969).
V. G. Lyuttsau, Yu. M. Fishman, and I. L. Svetlov, Kristallografiya, 10: 845 (1965).
O. Nittono and S. Nagakura, Japan. J. Appl. Phys., 8: 1180 (1969).
M. Tamura and Y. Sugita, Japan. J. Appl. Phys., 9: 368 (1970).
V. M. Al’tshuller, A. S. Fokin, et al., Fiz. Tverd. Tela, 13: 2827 (1971).
Yu. M. Fishman and V. G. Lutsau, Phys. Stat. Sol., (a), 18: 443 (1973).
H. Klapper, J. Cryst. Growth, 15: 281 (1972).
H. Klapper and H. Kuppers, Acta Crystallogr., A29: 495 (1973).
H. Klapper, Z. Naturforsch., 28a: 614 (1973).
F. Lefaucheux, J. Cryst. Growth, 16: 289 (1972).
H. Tabata, H. Okuda, and E. Ishii, Japan. J. Appl. Phys., 12: 7 (1973).
R. W. Bartlett and G. W. Martin, J. Appl. Phys., 39: 2324 (1968).
F. Lefaucheux, M. C. Robert, and J. M. Olson, J. Cryst. Growth, 19: 329 (1973).
H. Klapper, Phys. Stat. Sol. (a), 14: 99, 443 (1972).
H. Klapper, Yu. M. Fishman, and V. G. Lutsau, Phys. Stat. Sol. (a), 21: 115 (1974).
Y. Epelboin, A. Zarka, and H. Klapper, J. Cryst. Growth, 20: 103 (1973).
A. S. Tregubov and I. L. Shul’pina, Fiz. Tverd. Tela, 14: 2670 (1972).
Author information
Authors and Affiliations
Editor information
Editors and Affiliations
Rights and permissions
Copyright information
© 1984 Consultants Bureau, New York
About this chapter
Cite this chapter
Kostyukova, E.P., Lyuttsau, V.G., Fishman, Y.M. (1984). X-ray Diffraction Topography of Growth Defects in Crystals. In: Chernov, A.A. (eds) Рост Кристаллоь / Rost Kristallov / Growth of Crystals. Springer, Boston, MA. https://doi.org/10.1007/978-1-4615-7116-2_42
Download citation
DOI: https://doi.org/10.1007/978-1-4615-7116-2_42
Publisher Name: Springer, Boston, MA
Print ISBN: 978-1-4615-7118-6
Online ISBN: 978-1-4615-7116-2
eBook Packages: Springer Book Archive