Abstract
Two types of specimen-heating holder were developed which allow one to observe, at near atomic resolution, phenomena or reactions taking place at very high temperatures such as 1500°C. The performance of the heating holders was described. Some typical examples of results obtained using these holders were given. These include formation of SiC through reaction between Si and C, growth of SiC, formation of a void at a grain boundary in SiC during sintering and surface reconstruction of Au-deposited Si.
Access this chapter
Tax calculation will be finalised at checkout
Purchases are for personal use only
Preview
Unable to display preview. Download preview PDF.
References
Butler,E.P., and Hale,K.F., Dynamic Experiments in the Electron Microscope. Amsterdam:North-Holland,1982.
Loretto.M.H., and Smallman, R.E.,Materi.Sci.Engg.,28(1977),1–32.
Fujita,H.,In situ Experiments with High Voltage Electron Microscopes, Osaka: Research Center for Ultra-High Voltage Electron Microscopy.Osaka Univ.1985.
Louchet,F., and Saka,H.,French-Japanese Seminar on In Situ Electron Microscopy. Microsc.Microanal.Microstr.,1993;4:101–346.
Sharma,R.,Gai,P.L.,Gajdardziska-Josifovska,M.,Sinclair,R.Whitman,L.J.,In Situ Electrton and Tunneling Microscopy of Dynamic Processes.MRS Symp.,Vol.404, Pittsburgh:Materials Reseach Society,1996
Kamino,T., and Saka, H.,Microsc.Microanal.Microstruct,4(1993),127–135.
Mori,H., Yasuda,H, and Kaimno,T.,Phil.Mag.Lett.,69(1994),279–283.
Kamino,T.,Yaguchi,T., and Saka,H., J.Electron Microsco.,43(1994)104–110.
Kamino,T.,Yaguchi,T.,Ukiana,M.,Yasutomi,Y., and Saka,H.,Materi.TransJIM., 6(1995),73–75.
Kamino,T.,Yaguchi,T., and Saka,H.,Phil.Mag.A., in printing.
Author information
Authors and Affiliations
Editor information
Editors and Affiliations
Rights and permissions
Copyright information
© 1997 Springer Science+Business Media New York
About this chapter
Cite this chapter
Kamino, T., Saka, H. (1997). HREM In-Situ Experiment at Very High Temperatures. In: Gai, P.L. (eds) In-Situ Microscopy in Materials Research. Springer, Boston, MA. https://doi.org/10.1007/978-1-4615-6215-3_8
Download citation
DOI: https://doi.org/10.1007/978-1-4615-6215-3_8
Publisher Name: Springer, Boston, MA
Print ISBN: 978-0-7923-9989-6
Online ISBN: 978-1-4615-6215-3
eBook Packages: Springer Book Archive