Abstract
Experimental methods for wettability research are reviewed. A novel method for quantitative wettability study at nanoscale is presented. It is based on measuring transmitted electrons through nanodroplets using wet scanning transmission electron microscope (wet-STEM) detector in environmental scanning electron microscope (ESEM). The quantitative information of the nanodroplet shape and contact angle is obtained by fitting Monte Carlo simulation results for transmitted electrons with experimental results. Dynamic in situ imaging has showed that irregularities at the water film boundaries constituted nucleation sites for both dropwise and filmwise condensation. The initial stages of nucleation, growth, and coalescence have been studied as well as the growth power law dependence.
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Abbreviations
- 2D:
-
Two dimensional
- 3D:
-
Three dimensional
- AFM:
-
Atomic force microscope
- BF:
-
Bright field
- EM:
-
Electron microscope
- ESEM:
-
Environmental scanning electron microscope
- ETEM:
-
Environmental TEM
- FEG:
-
Field emission gun
- MC:
-
Monte Carlo
- MEMS and NEMS:
-
Micro/nano electromechanical systems
- RH:
-
Relative humidity
- RTD:
-
Resistive temperature device
- SEM:
-
Scanning electron microscope
- TEM:
-
Transmitted electron microscope
- Wet-STEM:
-
Wet scanning transmission electron microscope
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Acknowledgments
The author thanks the “Center of Nanoscience and Nanotechnology” and the “Wolfson Applied Materials Research Center” at Tel-Aviv University for the ESEM facility.
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Barkay, Z. (2013). Dynamic Study of Nanodroplet Nucleation and Growth Using Transmitted Electrons in ESEM. In: Wang, Z. (eds) Nanodroplets. Lecture Notes in Nanoscale Science and Technology, vol 18. Springer, New York, NY. https://doi.org/10.1007/978-1-4614-9472-0_3
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DOI: https://doi.org/10.1007/978-1-4614-9472-0_3
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