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The Role of Microwaves in the Extraction of Fats and Oils

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Part of the book series: Food Engineering Series ((FSES))

Abstract

The microwave-assisted extraction (MAE) of fats and oils at laboratory and industrial scales, the most common raw materials from which they are extracted, and the extractant required in each case are reviewed. The extractors used for this purpose, which range from conventional household devices to sophisticated commercial equipment, and their use at pilot and industrial plants, are discussed. Selected applications of MAE are compared with those of other energy-assisted extraction techniques (e.g., ultrasound-assisted extraction and superheated liquid extraction) and with conventional extraction to highlight its advantages and disadvantages. Finally, potential trends in the broad field of fat and oil extraction are outlined.

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References

  1. AOAC 920.39 official method, extraction of fat from bakery products

    Google Scholar 

  2. Hara M, Radin NS (1978) Anal Biochem 90:420

    Article  CAS  Google Scholar 

  3. Freyburger G, Heape A, Gin H, Boisseau M, Cassagne C (1988) Anal Biochem 171:213

    Article  CAS  Google Scholar 

  4. Erickson MC (1993) J Food Sci 58:84

    Article  CAS  Google Scholar 

  5. Gunnlangdottir K, Ackman RG (1993) J Sci Food Agric 61:235

    Article  Google Scholar 

  6. Nelson GJ (1991) In: Perkins EG (ed) Analysis of fats, oils and lipoproteins. American Oil Chemists’ Society, Champaign

    Google Scholar 

  7. Eller FJ (1999) J AOAC Int 82:766

    CAS  Google Scholar 

  8. Boselli E, Velazco V, Caboni MF, Lercker G (2001) J Chromatogr A 917:239

    Article  CAS  Google Scholar 

  9. Ruiz-Jiménez J, Luque de Castro MD (2004) Anal Chim Acta 502:75

    Article  Google Scholar 

  10. Priego-López E, Velasco J, Dobarganes MC, Ramis-Ramos G, Luque de Castro MD (2003) Food Chem 83:143

    Article  Google Scholar 

  11. Tavella M, Peterson G, Espeche M, Cavallero E, Cipolla L, Perego L, Caballero B (2000) Food Chem 69:209

    Article  CAS  Google Scholar 

  12. Ruiz Jiménez J, Priego Capote F, Luque de Castro MD (2006) Anal Bioanal Chem 385:1532

    Article  Google Scholar 

  13. Priego Capote F, Ruiz Jiménez J, García Olmo J, Luque de Castro MD (2004) Anal Chim Acta 517:13

    Article  CAS  Google Scholar 

  14. Ruiz Jiménez J, Priego Capote F, García Olmo J, Luque de Castro MD (2004) Anal Chim Acta 525:159

    Article  Google Scholar 

  15. Jiménez-Carmona MM, Ubera JL, Luque de Castro MD (1999) J Chromatogr A 855:625

    Article  Google Scholar 

  16. Priego Capote F, Ruiz Jiménez J, Luque de Castro MD (2007) Food Chem 100:859

    Article  CAS  Google Scholar 

  17. Ruiz Jiménez J, Priego Capote F, Luque de Castro MD (2004) J Chromatogr A 1045:203

    Article  Google Scholar 

  18. Sánchez-Ávila N, Priego Capote F, Ruiz-Jiménez J, Luque de Castro MD (2009) Talanta 78:40

    Article  Google Scholar 

  19. Nazari F, Ebrahimi SN, Talebi M, Rassouli A, Bijanzadeh HR (2007) Phytochem Anal 18:333

    Article  CAS  Google Scholar 

  20. National Academy of Sciences (1990) Nutritional labeling: issues and directions for the 1990s. Report of the Committee on the Nutrition Components of Food Labeling, Food and Nutrition Board, Institute of Medicine, National Research Council. National Academy Press, Washington, DC

    Google Scholar 

  21. Saccomandi V (1990) Off J Eur Comm 276:40

    Google Scholar 

  22. Sheppard J (1992) Lipid manual: methodology suitable for fatty acid-cholesterol analysis. Brown, Dubuque

    Google Scholar 

  23. Federal Register 58 (1993) 631

    Google Scholar 

  24. López-Ávila VJ (1999) J Assoc Off Anal Chem 82:217

    Google Scholar 

  25. Vetter W, Weichbrodt M, Hummert K, Glotz D, Luckas B (1998) Chemosphere 37:2425

    Article  Google Scholar 

  26. Weast RC (1988–1989) Handbook of chemistry and physics, 69th edn. CRC Press, Cleveland

    Google Scholar 

  27. Hummert K, Vetter W, Luckas B (1996) Chromatographia 42:300

    Article  CAS  Google Scholar 

  28. Kingston HM, Haswell SJ (1997) Microwave-enhanced chemistry. Professional reference book series. American Chemical Society, Washington, DC

    Google Scholar 

  29. Leray C, Grcic T, Gutbier G, Bnouham M (1995) Analusis 23:65

    CAS  Google Scholar 

  30. Bligh EG, Dyer WJ (1959) Biochem Physiol 37:911

    Article  CAS  Google Scholar 

  31. Ewald G, Bremle G, Karlsson A (1998) Mar Pollut Bull 36:222

    Article  CAS  Google Scholar 

  32. Renaud SM, Thinh LV, Parry LD (1999) Aquaculture 170:147

    Article  CAS  Google Scholar 

  33. Virot M, Tomao V, Ginies C, Visinoni F, Chemat F (2008) J Chromatogr A 1196:147

    Google Scholar 

  34. Luque de Castro MD, García Ayuso LE (1998) Dispositif et installation d’extractions sous microondas de composes organiques d’un echantillon. PCT/FR97/00883

    Google Scholar 

  35. Chemat F, Tomao V, Visinoni F (2010) Microwave integrated Soxhlet. US2010/0022788 A1, United States

    Google Scholar 

  36. Luque de Castro MD, Priego-Capote F (2011) Focused microwave-assisted Soxhlet extraction. In: Microwaves: theoretical aspects and practical applications in chemistry. Transworld Research Network, Kerala, India p 227

    Google Scholar 

  37. Luque de Castro MD, Priego Capote F (2010) J Chromatogr A 1217:2383

    Article  Google Scholar 

  38. Fernández-Pérez V, García-Ayuso LE, Luque de Castro MD (2000) Analyst 125:317

    Article  Google Scholar 

  39. García-Ayuso LE, Luque-García JL, Luque de Castro MD (2000) Anal Chem 72:3627

    Article  Google Scholar 

  40. García-Ayuso LE, Sánchez M, Fernández de Alba A, Luque de Castro MD (1998) Anal Chem 70:2426

    Article  Google Scholar 

  41. Luque-García JL, Luque de Castro MD (2001) Anal Chem 73:5903

    Article  Google Scholar 

  42. Luque-García JL, Luque de Castro MD (2003) J Chromatogr A 998:21

    Article  Google Scholar 

  43. Virot M, Tomao V, Colnagui G, Visinoni F, Chemat F (2007) J Chromatogr A 1174:138–144

    Article  CAS  Google Scholar 

  44. Abu-Samra A, Morris JS, Koirtyohann SR (1975) Anal Chem 47:1475

    Article  CAS  Google Scholar 

  45. Mahesar SA, Sherazi STH, Kamran Abroa, Aftab Kandhro, Bhanger MI, van de Voort FR, Sedmanb J (2008) Talanta 75:1240

    Google Scholar 

  46. Bhattacharya M, Basak T (2006) Food Res Int 39(10):1046

    Article  Google Scholar 

  47. Baxendale IR, Hayward JJ, Ley SV (2007) Combinatorial Chem High Throughput Screening 10(10):802

    Article  CAS  Google Scholar 

  48. Contreras Flores VH (2010) Extracción de Aceite de Orégano Mediante Radiación de Microondas. Doctoral thesis, Instituto Tecnológico de Durango, Mexico

    Google Scholar 

  49. Terigar BG (2009) Advanced microwave technology for biodiesel feedstock processing. A thesis submitted to the Graduate Faculty of the Louisiana State University and Agricultural and Mechanical College, Baton Rouge

    Google Scholar 

  50. Ching-Lung C, Shang-Lien L, Wen-Hui K, Ching-Hong H (2005) J Hazard Mater B 123:256

    Article  Google Scholar 

  51. Paré JR (1995) Microwave-assisted extraction from materials containing organic matter. Patent 5,458,897, USA

    Google Scholar 

  52. Paré JR, Bélanger MR (1994) Trends Anal Chem 13(4):176

    Article  Google Scholar 

  53. Cocchi M, Durante C, Marchetti A, Li Vigni M, Baschieri C, Bertacchini L, Siguinolfi S, Tassi L, Totaro S (2011) Optimization of microwave assisted digestion procedure by means of chemometric tools. In: Microwaves: Theoretical Aspects and Practical Applications in Chemistry, Transworld Research Network, Kerala, India, p. 203

    Google Scholar 

  54. Zhang H, Xue M, Lu Y, Dai Z, Wang H (2010) J Sep Sci 33:235

    Article  CAS  Google Scholar 

  55. Smythe MC, Wakeman RJ (2000) Ultrasonics 38:657

    Article  CAS  Google Scholar 

  56. Bermejo-Barrera P, Moreda-Piñeiro A, Bermejo-Barrera A (2001) Talanta 57:969

    Article  Google Scholar 

  57. Luchini LC, Peres TB, Andrea MM (2000) J Environ Sci Health 35:51

    Article  CAS  Google Scholar 

  58. Wang T, Jia X, Wu J (2003) J Pharm Biomed Anal 33:639

    Article  CAS  Google Scholar 

  59. Ruiz-Jiménez J, Luque García JL, Luque de Castro MD (2003) Anal Chim Acta 480:231

    Article  Google Scholar 

  60. Pérez Serradilla JA, Priego Capote F, Luque de Castro MD (2007) Anal Chem 79:6767

    Article  Google Scholar 

  61. Luque de Castro MD, Priego Capote F (2007) Analytical applications of ultrasound. Elsevier, Amsterdam

    Google Scholar 

  62. Luque de Castro MD, Jiménez-Carmona MM (1998) Trends Anal Chem 17:441

    Article  Google Scholar 

  63. Canals Hernández A, Hidalgo Nuñez MM, Domini CE, Cravotto G (2008) Method and apparatus for direct irradiation of a liquid or solid sample with microwave or ultrasound irradiation simultaneously, consecutively or alternating Universidad de Alicante, Patent No. ES 2304839, España, 2008

    Google Scholar 

  64. Zhang L, Liu Z (2008) Ultrason Sonochem 15:731

    Article  CAS  Google Scholar 

  65. Cravotto G, Boffa L, Mantegna S, Perego P, Avogadro M, Cintas P (2008) Ultrason Sonochem 15:898

    Article  CAS  Google Scholar 

  66. Chen Y, Gu X, Huang S, Li J, Wang X, Tang J (2010) Int J Biol Macromol 46

    Google Scholar 

  67. Richter BE, Jones BA, Ezzell JL, Porter NL (1996) Anal Chem 68:1033

    Article  CAS  Google Scholar 

  68. Hawthorne SB, Yang Y, Miller DJ (1994) Anal Chem 66:2912

    Article  CAS  Google Scholar 

  69. Luque de Castro MD, Luque García JL (2002) Acceleration and automation of solid sample treatment. Elsevier, Amsterdam

    Google Scholar 

  70. Bjoërklund E, von Holst C, Anklam E (2002) TrAC, 21(1):40–52

    Google Scholar 

  71. Keller JM, Swarthout RF, Carlson BKR, Yordy J, Guichard A, Schantz MM, Kucklick JR (2009) Anal Bioanal Chem 393:747–760

    Article  CAS  Google Scholar 

  72. García-Ayuso LE, Luque de Castro MD (1999) Anal Chim Acta 382:309

    Article  Google Scholar 

  73. García-Ayuso LE, Velasco J, Dobarganes MC, Luque de Castro MD (2000) Chromatographia 52:103

    Article  Google Scholar 

  74. García-Ayuso LE, Velasco J, Dobarganes MC, Luque de Castro MD (1999) J Agric Food Chem 47:2308

    Article  Google Scholar 

  75. García-Ayuso LE, Velasco J, Dobarganes MC, Luque de Castro MD (1999) Int Dairy J 9:667

    Article  Google Scholar 

  76. Luque-García JL, Velasco J, Dobarganes MC, Luque de Castro MD (2002) Food Chem 76:241

    Article  Google Scholar 

  77. Priego-Capote F, Luque de Castro MD (2005) Talanta 65:81

    CAS  Google Scholar 

  78. Batista A, Vetter W, Luckas B (2001) Eur Food Res Technol 212:377

    Article  CAS  Google Scholar 

  79. Fuentes E, Báez ME, Díaz J (2009) J Chromatogr A 1216:8859

    Article  CAS  Google Scholar 

  80. Pena T, Pensado L, Casais C, Mejuto C, Phan-Tan-Luu R, Cela R (2006) J Chromatogr A 1121:163

    Article  CAS  Google Scholar 

  81. Fuentes E, Báez ME, Quiñones A (2008) J Chromatogr A 1207:38

    Article  CAS  Google Scholar 

  82. Fuentes E, Báez ME, Labra R (2007) J Chromatogr A 1169:40

    Article  CAS  Google Scholar 

  83. Ramalhosa MJ, Paiga P, Morais S, Rui Alves M, Delerue-Matos C, Prior Pinto Oliveira MB (2012) Food Chem 131:328

    Article  CAS  Google Scholar 

  84. Pérez-Serradilla JA, Ortiz MC, Sarabia L, Luque de Castro MD (2007) Anal Bioanal Chem 388:451

    Article  Google Scholar 

  85. Sabliov CM, Xu Z, Boldor D, Lima M, Spanier CN (2011) Spring 2011 issue of Louisiana Agriculture Magazine

    Google Scholar 

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Acknowledgments

The authors are grateful to Spain’s Ministry of Science and Innovation (MICINN), and the FEDER programme, for funding this work through Project CTQ2009-07430.

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Correspondence to M. D. Luque de Castro .

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Abbreviations

ASE

Accelerated solvent extraction

CMAE

Continuous flow microwave-assisted extraction

EFAs

Essential fatty acids

FID

Flame-ionization detection

FMASE

Focused microwave-assisted Soxhlet extractor

FME

Focused microwave-assisted extraction

GC

Gas chromatography

HPSE

High-pressure solvent extraction

LC

Liquid chromatography

LDL

Low-density lipoproteins

LLE

Liquid–liquid extraction

MAE

Microwave-assisted extraction

MASE

Microwave-assisted Soxhlet extraction

MIR

Middle infrared spectrometry

MIS

Microwave integrated Soxhlet

MS

Mass spectrometry

NEFAs

Nonessential fatty acids

NMR

Nuclear magnetic resonance

PFE

Pressurized fluid extraction

PHSE

Pressurized hot solvent extraction

PTFE

Polytetrafluoroethylene

PUFAs

Polyunsaturated fatty acids

SHLE

Superheated liquid extraction

SHSE

Superheated solvent extraction

SPE

Solid-phase extraction

SPME

Solid-phase microextraction

SSE

Subcritical solvent extraction

UMAE

Ultrasound and microwaves for acceleration of extraction

USAE

Ultrasound-assisted extraction

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de Castro, M.D.L., Fernández-Peralbo, M.A., Linares-Zea, B., Linares, J. (2012). The Role of Microwaves in the Extraction of Fats and Oils. In: Chemat, F., Cravotto, G. (eds) Microwave-assisted Extraction for Bioactive Compounds. Food Engineering Series. Springer, Boston, MA. https://doi.org/10.1007/978-1-4614-4830-3_4

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