Abstract
The x-ray signals obtained from the SEM-EPMA are most often used either to identify the elements present in a sample or to measure the relative or actual amounts of these elements in localized areas of the sample. The methods for determining the presence of a given element by the wavelength-or energy-dispersive method have been described in previous chapters. Similarly, the methods of scanning x-ray analysis and quantitative analysis have been discussed in some detail (Chapters IX–XI).
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References
T. Shiraiwa, N. Fujino, and J. Murayama, in Proceedings of the Sixth International Conference on X-Ray Optics and Microanalysis (G. Shinoda, K. Kohra, and T. Ichinokawa, eds.), University of Tokyo Press (1972), p. 213.
G. L. Fisher and G. D. Farningham, Quantitative Carbon Analysis of Nickel Steels with the Electron Probe Microanalyzer, ASM Materials Engineering Congress, Cleveland, Ohio, October (1972).
P. Duncumb and D. A. Melford, in X-Ray Optics and Microanalysis, Fourth International Conference on X-Ray Optics and Microanalysis (R. Castaing, P. Deschamps, and J. Philibert, eds.), Hermann, Paris (1966), p. 240.
D. W. Fisher and W. L. Baun, Norelco Reporter, 14, 92 (1967).
J. E. Holliday, Norelco Reporter, 14, 84 (1967).
R. Castaing, in Advances in Electronics and Electron Physics, (L. Marton, ed.), p. 317, Academic Press, New York (1960).
R. Castaing and J. Deschamps, Compt. Rend., 238, 1506 (1954).
J. S. Duerr and R. E. Ogilvie, Anal. Chem., 44, 2361 (1972).
G. W. Bruno and S. H. Moll, Second National Microprobe Conference, Boston, Massachusetts (1967), Paper 57.
R. Theisen, Quantitative Electron Microprobe Analysis, Springer, Berlin (1965).
V. E. Kohlhaas and F. Scheiding, Arch. Eisenhüttenwessen, 40, 1 (1969).
R. H. Barkalow, R. W. Kraft, and J. I. Goldstein, Met. Trans., 3, 919 (1972).
B. L. Henke and E. S. Ebisu, in Advances in X-Ray Analysis, Vol. 17, Plenum Press, New York (1974), p. 150.
H. A. Liebhafsky, H. G. Pfeiffer, and P. D. Zemany, Anal. Chem. 27, 1257 (1955).
T. O. Ziebold, Anal. Chem., 39, 858 (1967).
H. Yakowitz, C. E. Fiori, and R. E. Michaelis, NBS Special Publication 260–22 (1971).
F. Kunz, E. Eichen, and A. Varshneya, in Proceedings of the Sixth National Conference on Electron Probe Analysis EPASA, Pittsburgh (1971), Paper 20.
R. E. Michaelis, H. Yakowitz, and G. A. Moore, J. Res. NBS, A68, 343 (1964).
H. Yakowitz, D. L. Vieth, K. F. J. Heinrich, and R. E. Michaelis, NBS Special Publication 260–10 (1965).
J. I. Goldstein, F. J. Majeske, and H. Yakowitz, in Applications of X-Ray Analysis, Vol. 10 (J. B. Newkirk and G. R. Mallett, eds.), Plenum Press, New York (1967), p. 431.
P. R. Buseck and J. I. Goldstein, Geol. Soc. Am. Bull, 80, 2141 (1969).
H. Yakowitz, A. W. Ruff, and R. E. Michaelis, NBS Special Publication 260–43 (1972).
E. L. Bauer, A Statistical Manual for Chemists, 2nd ed., Academic Press, New York (1971), p. 189.
H. A. Liebhafsky, H. G. Pfeiffer, and P. D. Zemany, in X-Ray Microscopy and X-Ray Microanalysis (A. Engstrom, V. Cosslett, and H. Pattee, eds.), Elsevier, Amsterdam (1960), p. 321.
R. H. Hewins and J. I. Goldstein, “Metal-Olivine Associations and Ni-Co Contents in Apollo 12 Mare Basalts,” Earth and Planet. Sci. Lett. 24, 59 (1974).
T. O. Ziebold and R. E. Ogilvie, Anal. Chem., 36, 322 (1964).
J. I. Goldstein, J. Geophys. Res., 72, 4689 (1967).
S. J. B. Reed and J. V. P. Long, in X-Ray Optics and X-Ray Microanalysis, Academic Press, New York (1963), p. 317.
E. J. Rapperport, in Advances in Electronics and Electron Physics, Supplement 6, Academic Press, New York (1969), p. 117.
J. B. Gilmour, “The Role of Manganese in the Formation of Proeutectoid Ferrite,” Ph.D. Thesis, McMaster University (1970).
P. K. Gupta, J. Phys. D. Appl. Phys., 3, 1919 (1970).
A. S. Norkiewicz, “Dissolution of Phosphides in the Ternary Fe-Ni-P System,” M.S. Thesis, Lehigh University (1972).
J. B. Gilmour, G. R. Purdy, and J. S. Kirkaldy, Met. Trans., 3, 3213 (1972).
G. T. Miyake and J. I. Goldstein, Geochim. et Cosmochim. Acta, 38, 1201 (1974).
D. M. Koffman, Norelco Reporter, 11, 59 (1964).
J. I. Goldstein and R. E. Ogilvie, in X-Ray Optics and Microanalysis, IVth International Congress on X-Ray Optics and Microanalysis (R. Castaing, P. Deschamps, and J. Philibert, eds.), Hermann, Paris (1966), p. 594.
M. J. Henoc, F. Maurice, and A. Zemskoff, in Fifth International Congress on X-Ray Optics and Microanalysis (G. Mollenstedt and K. H. Gaukler, eds.), Springer Verlag, Berlin (1969), p. 187.
E. W. White, in “Tutorial Session,” 7th National Conference on Electron Probe Analysis (1972).
E. W. White, in Microprobe Analysis (C. A. Andersen, ed.), Wiley New York (1973), p. 349.
J. W. Colby, D. R. Wonsiddler, and A. Androshuck, in Proceedings of the 4th National Conference on Electron Probe Analysis, EPASA (1969), p. 26.
A. L. Albee and A. A. Chodos, Am. Mineral, 55, 491 (1970).
J. W. Colby, in Proceedings of the 6th International Conference on X-Ray Optics and Microanalysis (G. Shinoda, K. Kohra, and T. Ichinokawa, eds.), University of Tokyo Press (1972), p. 247.
J. W. Colby, in Advances in X-Ray Analysis, Vol. 11, Plenum Press, New York (1968), p. 287.
J. W. Colby, in Thin Film Dielectrics (F. Vratny, ed.), The Electr. Chem. Soc, New York (1969).
R. R. Warner and J. R. Coleman, Micron, 4, 61 (1973).
Y. Oda and K. Nakajima, J. Jap. Inst. Met., 37, 673 (1973).
V. E. Cosslett and R. N. Thomas, in The Electron Microprobe (T. D. McKinley, K. F. J. Heinrich, and D. B. Wittry, eds.), Wiley, New York (1966), p. 248.
V. E. Cosslett and R. N. Thomas, Brit. J. Appl. Phys., 15, 1283 (1964).
P. Duncumb and P. K. Shields, in The Electron Microprobe (T. D. McKinley, K. F. J. Heinrich, and D. B. Wittry, eds.), Wiley, New York (1966), p. 284.
D. F. Kyser and K. Murata, in Proceedings of the 8th National Conference on Electron Probe Analysis, EPASA (1973), p. 28.
D. F. Kyser and K. Murata, IBM J. Res. Dev., 18, 352 (1974).
M. A. Nicolet, J. Mayer and I. Mitchell, Science, 177, 844 (1972).
G. D. Bergland, IEEE Trans., Audio and Electroacoustics, AU-17, 138 (1969).
G. D. Bergland, IEEE Spectrum, 6, 41 (1969).
R. Bracewell, in The Fourier Transform and Its Applications, McGraw-Hill, New York (1965), p. 108.
J. W. Colby, in “Tutorial Session,” 7th National Conference on Electron Probe Analysis (1972).
J. R. Morrey, Anal Chem., 40, 905 (1968).
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Goldstein, J.I., Colby, J.W. (1975). Special Techniques in the X-Ray Analysis of Samples. In: Goldstein, J.I., Yakowitz, H. (eds) Practical Scanning Electron Microscopy. Springer, Boston, MA. https://doi.org/10.1007/978-1-4613-4422-3_12
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DOI: https://doi.org/10.1007/978-1-4613-4422-3_12
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