Skip to main content

Differential Scanning Calorimetry: Simultaneous Temperature and Calorimetric Calibration

  • Chapter
Analytical Calorimetry

Abstract

With computer equipped DSC instruments it is possible to measure temperatures and enthalpies with one and the same run. For the practical application of this possibility, standards are needed which allow the simultaneous calibration for both types of measurements. Based on numerous T and ΔH measurements a set of 12 standards is proposed in this paper.

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

eBook
USD 16.99
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
USD 54.99
Price excludes VAT (USA)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

References

  1. K.-H. Breuer and W. Eysel, The calorimetric calibration of differential scanning calorimetry cells, Thermochimica Acta 57, 317–329 (1982).

    Article  CAS  Google Scholar 

  2. K.-H. Breuer, W. Eysel and G.W.H. Höhne, Enthalpy standards for heat flux calorimeters, Paper presented at the 5. Ulmer Kalorimetrietage, Ulm, Germany (1983).

    Google Scholar 

  3. NBS Circ. 500 (1952).

    Google Scholar 

  4. S. Allard,ed., Int. Tables of selected constants 16, Pergamon Press, Oxford, N.Y., Paris, Braunschweig (1969).

    Google Scholar 

  5. A.P. Gray, The calorimetry of the NBS-ICTA temperature standards, inThermal Analysis, Proceedings Fourth ICTA, J. Buzas, ed., Akademiai Kiado, Budapest, Vol.3, 991–1003, (1975).

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Editor information

Editors and Affiliations

Rights and permissions

Reprints and permissions

Copyright information

© 1984 Plenum Press, New York

About this chapter

Cite this chapter

Eysel, W., Breuer, KH. (1984). Differential Scanning Calorimetry: Simultaneous Temperature and Calorimetric Calibration. In: Johnson, J.F., Gill, P.S. (eds) Analytical Calorimetry. Springer, Boston, MA. https://doi.org/10.1007/978-1-4613-2699-1_7

Download citation

  • DOI: https://doi.org/10.1007/978-1-4613-2699-1_7

  • Publisher Name: Springer, Boston, MA

  • Print ISBN: 978-1-4612-9677-5

  • Online ISBN: 978-1-4613-2699-1

  • eBook Packages: Springer Book Archive

Publish with us

Policies and ethics