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The Parameters of NMR Spectroscopy

  • Chapter
Multinuclear NMR

Abstract

Many nuclei have spin angular momentum, since protons and neutrons have this property, although the nucleons couple to produce nuclei without spin when an even number of each kind is present, as in 12C, 16O, 28Si, 32S, etc. The nuclear angular momentum has an associated magnetic field, comparable to the magnetic field produced by an electric current in a loop. A nuclear spin thus behaves as a magnetic dipole, which tends to align with an applied magnetic field and to interact with neighboring dipoles. The magnetic moment µ, which determines the potential energy E of the nuclear magnetic dipole in a magnetic field of strength (or flux density) B 0, is defined by

$$ E = - \mu \cdot{\text{B}}_{\text{0}} $$
(1)

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References

  1. Fuller, G. H. J. Phys. Chem. Ref. Data, 1976, 5, 835–864.

    CAS  Google Scholar 

  2. Lederer, C. M.; Shirley, V. S. Table of Isotopes, 7th ed., Wiley: New York, 1978; Appendix VII.

    Google Scholar 

  3. Abragam, A. “The Principles of Nuclear Magnetism,” corrected reprint, Oxford, 1978.

    Google Scholar 

  4. Pure Appl Chem. 1972, 29, 627; 1976, 45, 217–219.

    Google Scholar 

  5. Buckingham, A. D.; Pople, J. A. Trans. Faraday Soc. 1963, 59, 2421–2430.

    Google Scholar 

  6. Buckingham, A. D.; Malm, S. M. Mol. Phys. 1971, 22, 1127–1130.

    CAS  Google Scholar 

  7. Raynes, W. T. NMR Spec. Per. Rep. C.S. 1978, 7, 1–25.

    CAS  Google Scholar 

  8. Mehring, M. NMR Basic Princ. Prog. 1976, 11, 1–243.

    Google Scholar 

  9. Pines, A.; Gibby, M. G.; Waugh, J. S. Chem. Phys. Lett. 1972, 15, 373–376.

    CAS  Google Scholar 

  10. Wasylishen, R. E., personal communication; Gleeson, J. W.; Vaughan, R. W. J. Chem. Phys. 1983, 78, 5384–5392; Klose, G.; Trahms, L.; Möps, A. Chem. Phys. Lett. 1985, 122, 545–549.

    Google Scholar 

  11. Lynden-Bell, R. M.; Harris, R. K. NMR Spectroscopy, Nelson: London, 1969.

    Google Scholar 

  12. Venanzi, T. J. Chem. Educ. 1982, 59, 144.

    CAS  Google Scholar 

  13. Abraham, R. J. The Analysis of High Resolution NMR Spectra, Elsevier: Amsterdam, 1971.

    Google Scholar 

  14. Emsley, J. W.; Feeney, J.; Sutcliffe, L. H. High Resolution NMR Spectroscopy, Pergamon: Oxford, 1965; Volumes I and II.

    Google Scholar 

  15. Hoffman, R. A.; Forsen, S.; Gestblom, B. NMR Basic Princ. and Prog. 1971, 5, 1–165.

    Google Scholar 

  16. Siddall, T. H.; Flurry, R. L. Jr. J. Magn. Reson. 1980, 39, 487–497.

    CAS  Google Scholar 

  17. Siddall, T. H.; Flurry, R. L. Jr. J. Magn. Reson. 1981, 43, 357–372.

    CAS  Google Scholar 

  18. Siddall, T. H. J. Phys. Chem. 1982, 86, 91–96.

    CAS  Google Scholar 

  19. Crocker, C. Ph.D. thesis, University of Bristol, 1978.

    Google Scholar 

  20. Haigh, C. W. Annu. Rep. NMR Spectrosc. 1971, 4, 311–362.

    CAS  Google Scholar 

  21. Diehl, P.; Kellerhals, H.; Lustig, E. NMR Basic Princ. and Prog. 1972, 6, 1–96.

    Google Scholar 

  22. Edmonds, D. T. Int. Rev. Phys. Chem. 1982, 2, 103–126.

    CAS  Google Scholar 

  23. Sears, R. E. J. Phys. Rev. Ser. B 1980, 22, 1135–1140.

    CAS  Google Scholar 

  24. Wolff, E. K.; Griffin, R. G.; Watson, C. J. Chem. Phys. 1977, 66, 5433–5438.

    CAS  Google Scholar 

  25. Gorter, C. J. Physica 1936, 3, 995–998; Gorter, C. J.; Broer, L. F. J. Physica 1942, 9, 591–596.

    CAS  Google Scholar 

  26. Bloch, F. Phys. Rev. 1946, 70, 46–474; 1956, 102, 104–135.

    Google Scholar 

  27. Pople, J. A.; Schneider, W. G.; Bernstein, H. J. High-Resolution NMR; McGraw-Hill: New York, 1959.

    Google Scholar 

  28. Martin, M. L.; Delpuech, J. J.; Martin, G. J. Practical NMR Spectroscopy; Heyden: London, 1980, 492 pp.

    Google Scholar 

  29. Doddrell, D. M.; Barron, P. F.; Clegg, D. E.; Bowie, C. J. Chem. Soc., Chem. Commun. 1982, 575–576.

    Google Scholar 

  30. Akitt, J. W. J. Magn. Reson. 1970, 3, 411–414.

    CAS  Google Scholar 

  31. Wehrli, F. W. J. Magn. Reson. 1978, 30, 193–209.

    CAS  Google Scholar 

  32. Shaw, D. Fourier Transform NMR Spectroscopy, 2nd Ed.; Elsevier: Amsterdam, 1984, 304 pp.

    Google Scholar 

  33. Farrar, T. C.; Becker, E. D. Pulse and Fourier Transform NMR, Academic Press; New York, 1973, 115 pp.; Fukushima, E.; Roeder, S. B. Experimental Pulse NMR: A Nuts and Bolts Approach, Addison-Wesley: Reading, 1981, 539 pp.

    Google Scholar 

  34. Gibby, M.; Pines, A.; Waugh, J. S. J. Am. Chem. Soc. 1972, 94, 6231–6232.

    CAS  Google Scholar 

  35. Laue, E. D.; Skilling, J.; Staunton, J.; Sibisi, S.; Brereton, R. G. J. Magn. Reson. 1985, 62, 437–452.

    CAS  Google Scholar 

  36. Ernst, R. R. J. Magn. Reson. 1970, 3, 10–27; Bluemich, B.; Kaiser, R. J. Magn. Reson. 1983, 54, 486–501.

    CAS  Google Scholar 

  37. Belton, P. S.; Cox, I. J.; Harris, R. K. J. Chem. Soc., Faraday Trans. 2 1985, 81, 63–75; Morris, G. A.; Toohey, M.J. J. Magn. Reson. 1985, 63, 629–633; Canet, D.; Brondeau,J.; Marchai, J. P.; Robin-Lherbier, B. Org. Magn. Reson. 1982, 20, 51–53; Lambert, J. B.; Riddell, F. G. Eds.; The Multinuclear Approach to NMR Spectroscopy, NATO ASI Series, Reidel; Dordrecht, 1983, p. 22 (Brévard, C); p. 310 (Drakenberg, T.; Forsen, S.; Ellis, P. D.).

    CAS  Google Scholar 

  38. Morris, G. A. J. Am. Chem. Soc. 1980, 102, 428–429.

    CAS  Google Scholar 

  39. Doddrell, D. M.; Pegg, D. T. J. Am. Chem. Soc. 1980, 102, 6388–6390.

    CAS  Google Scholar 

  40. Hahn, E. L. Phys. Rev. 1950, 80, 580–584.

    Google Scholar 

  41. Carr, H. Y.; Purcell, E. M. Phys. Rev. 1954, 94, 630–638.

    CAS  Google Scholar 

  42. Freeman, R.; Hill, H. D. W. In Dynamic NMR Spectroscopy, Jackman, L. M.; Cotton, F. A., Ed.; Academic Press: New York, 1975; pp. 131–162.

    Google Scholar 

  43. Freeman, R.; Morris, G. A. Bull. Magn. Reson. 1979, 1, 5–26.

    CAS  Google Scholar 

  44. Freeman, R. Proc. R. Soc. London, Ser. A 1980, 373, 149–178.

    CAS  Google Scholar 

  45. Morris, G. A. Magn. Reson. Chem. 1986, 24, 371–403; Top. 13C NMR Spectrosc. 1984, 4, 179–196; Benn, R.; Günther, J. Angew. Chem. Int. Ed. Engl. 1983, 22, 350–380; Turner, C. J. Prog. NMR Spectrosc. 1985, 16, 311–358; Sanders, J. K. M.; Hunter, B. K. Modern NMR Spectroscopy, Oxford, 1987.

    CAS  Google Scholar 

  46. Bax, A. Two-Dimensional NMR Spectroscopy in Liquids, Reidel: Hingham, 1982; Top. 13C NMR Spectrosc. 1984, 4, 197–238; Ernst, R. R.; Bodenhausen, G.; Wokaun, A. Principles of NMR in One and Two Dimensions; Clarendon Press: Oxford, 1986; Derome, A. E. Modern NMR Techniques for Chemistry Research, Pergamon: Oxford, 1987.

    Google Scholar 

  47. Drobny, G.; Pines, A.; Sinton, S.; Weitekamp, D. P.; Wemmer, D. Faraday Symp. C. S. (Pulsed NMR in Solids), 1978, 13, 49–55.

    Google Scholar 

  48. Drobny, G.; Pines, A.; Sinton, S.; Warren, W. S.; Weitekamp, D. P. Phil. Trans. R. Soc. London, Ser. A 1981, 299, 585–592; Munowitz, M.; Pines, A. Science 1986, 233, 525–531.

    CAS  Google Scholar 

  49. Turner, D. L. J. Magn. Reson. 1982, 49, 175–178.

    CAS  Google Scholar 

  50. Bax, A.; Freeman, R.; Frenkiel, T. A.; Levitt, M. H. J. Magn. Reson. 1981, 43, 478–483.

    CAS  Google Scholar 

  51. Bax, A.; Freeman, R.; Frenkiel, T. A. J. Am. Chem. Soc. 1981, 103, 2102–2104.

    CAS  Google Scholar 

  52. Warren, W. S.; Pines, A. J. Am. Chem. Soc. 1981, 103, 1613–1617.

    CAS  Google Scholar 

  53. Bodenhausen, G. Prog. NMR Spectrosc. 1981, 14, 137–173.

    Google Scholar 

  54. Hoffman, R. A.; Forsen, S. Prog. NMR Spectrosc. 1966, 1, 15–204.

    Google Scholar 

  55. McFarlane, W. Annu. Rep. NMR Spectrosc. 1972, 5a, 353–393; Annu. Rep. NMR Spectrosc. 1979, 9, 319–414.

    CAS  Google Scholar 

  56. McFarlane, W.; Rycroft, D. S. Annu. Rep. NMR Spectrosc. 1985, 16, 293–364.

    CAS  Google Scholar 

  57. McFarlane, W. and others, annual chapters. NMR Spec. Per. Rep. C. S. 1977–1986, 6–15.

    Google Scholar 

  58. Baker, E. B. J. Chem. Phys. 1962, 37, 911–912.

    CAS  Google Scholar 

  59. Freeman, R.; Anderson, W. A. J. Chem. Phys. 1962, 37, 2053–2073.

    CAS  Google Scholar 

  60. Levitt, M. H.; Freeman, R.; Frenkiel, T. J. Magn. Reson. 1982, 50, 157–160; Waugh, J. S. J. Magn. Reson. 1982, 49, 517–521.

    CAS  Google Scholar 

  61. Pachler, K. G. R.; Wessels, P. L. J. Magn. Reson. 1973, 12, 337–339.

    CAS  Google Scholar 

  62. Chalmers, A. A.; Pachler, K. G. R.; Wessels, P. L. J. Magn. Reson. 1974, 15, 415–419.

    CAS  Google Scholar 

  63. Sorensen, S.; Hansen, R. S.; Jakobsen, H. J. J. Magn. Reson. 1974, 14, 243–245.

    Google Scholar 

  64. Anderson, W. A. Phys. Rev. 1956, 102, 151–167.

    CAS  Google Scholar 

  65. Bloch, F. Phys. Rev. 1954, 93, 944.

    Google Scholar 

  66. Solomon, I.; Bloembergen, N. J. Chem. Phys. 1956, 25, 261–266.

    CAS  Google Scholar 

  67. Kaiser, R. J. Chem. Phys. 1963, 39, 2435–2442.

    CAS  Google Scholar 

  68. Feeney, J.; Shaw, D.; Pauwells, P. J. S. J. Chem. Soc., Chem. Commun. 1970, 554–555.

    Google Scholar 

  69. Freeman, R.; Hill, H. D. W. J. Magn. Reson. 1971, 5, 278–280.

    CAS  Google Scholar 

  70. Freeman, R.; Hill, H. D. W.; Kaptein, R. J. Magn. Reson. 1972, 7, 327–329.

    CAS  Google Scholar 

  71. Ernst, R. R. J. Chem. Phys. 1966, 45, 3845–3861.

    CAS  Google Scholar 

  72. DeMilou, M. E.; Kowalewski, V. J. J. Magn. Reson. 1982, 46, 54–60.

    CAS  Google Scholar 

  73. Kessler, H.; Krack, G.; Zimmermann, G. J. Magn. Reson. 1981, 44, 208–211.

    CAS  Google Scholar 

  74. Noggle, J. H.; Schirmer, R. E. The Nuclear Overhauser Effect: Chemical Applications, Academic Press: New York, 1971, 259 pp.

    Google Scholar 

  75. Freeman, R.; Pachler, K. G. R.; LaMar, G. D. J. Chem. Phys. 1971, 55, 4586–4593.

    CAS  Google Scholar 

  76. McFarlane, W. Annu. Rep. NMR Spectrosc. 1968, 1, 135–163.

    CAS  Google Scholar 

  77. Sorensen, O. W.; Bildsoe, H.; Jakobsen, H. J. J. Magn. Reson. 1981, 45, 325–336.

    Google Scholar 

  78. Kuhlmann, K. F.; Grant, D. M. J. Am. Chem. Soc. 1968, 90, 7355–7357.

    CAS  Google Scholar 

  79. Hartmann, S. R.; Hahn, E. L. Phys. Rev. 1962, 128, 2042–2053.

    CAS  Google Scholar 

  80. Pines, A.; Gibby, M. G.; Waugh, J. S. J. Chem. Phys. 1972, 56, 1776–1777; J. Chem. Phys. 1973, 59, 569–590.

    CAS  Google Scholar 

  81. Bertrand, R. D.; Moniz, W. B.; Garroway, A. N.; Chingas, G. C. J. Am. Chem. Soc. 1978, 100, 5227–5229.

    CAS  Google Scholar 

  82. Bertrand, R. D.; Moniz, W. B.; Garroway, A. N.; Chingas, G. C. J. Magn. Reson. 1978, 32, 465–467.

    CAS  Google Scholar 

  83. Chingas, G. C.; Garroway, A. N.; Moniz, W. B.; Bertrand, R. D., J. Am. Chem. Soc. 1980, 102, 2526–2528.

    CAS  Google Scholar 

  84. Doddrell, D. M.; Pegg, D. T.; Bendall, M. R. J. Magn. Reson. 1982, 49, 181–196.

    CAS  Google Scholar 

  85. Morris, G. A.; Freeman, R. J. Am. Chem. Soc. 1979, 101, 760–762.

    CAS  Google Scholar 

  86. Maudsley, A. A.; Muller, L.; Ernst, R. R. J. Magn. Reson. 1977, 28, 463–469.

    CAS  Google Scholar 

  87. Burum, D. T.; Ernst, R. R. J. Magn. R.son. 1980, 39, 163–168; Bolton, P. H. Magn. Reson. 1980, 41, 287–292.

    CAS  Google Scholar 

  88. Jakobsen, H. J.; Linde, S. A.; Sorensen, S. J. Magn. Reson. 1974, 15, 385–388.

    CAS  Google Scholar 

  89. Becker, E. D.; Ferretti, J. A.; Farrar, T. C. J. Am. Chem. Soc. 1969, 91, 7784–7785.

    PubMed  CAS  Google Scholar 

  90. Allerhand, A.; Cochran, D. W. J. Am. Chem. Soc. 1970, 92, 4482–484.

    CAS  Google Scholar 

  91. Maudsley, A. A.; Ernst, R. R. Chem. Phys. Lett. 1977, 50, 368–372.

    CAS  Google Scholar 

  92. Doddrell, D. M.; Pegg, D. T.; Bendall, M. R. J. Magn. Reson. 1982, 48, 323–327.

    CAS  Google Scholar 

  93. Martineau, H.; Trierweiler, M.; Martin, M. L. Org. Magn. Reson. 1981, 17, 182–185; Sarkar, S. K.; Bax, A. Magn. Reson. 1985, 62, 109–112.

    CAS  Google Scholar 

  94. Voigt, J.; Jakobsen, J. P. J. Magn. Reson. 1981, 45, 510–513.

    CAS  Google Scholar 

  95. Pachler, K. G. R.; Wessels, P. L. J. Magn. Reson. 1977, 28, 53–61.

    CAS  Google Scholar 

  96. Brevard, C.; Van Stein, G. C.; Van Koten, G. J. Am. Chem. Soc. 1981, 103, 6746–6748.

    CAS  Google Scholar 

  97. Staedeli, W.; Bigler, P.; Von Philipsborn, W. Org. Magn. Reson. 1981, 16, 170–172.

    CAS  Google Scholar 

  98. Doddrell, D. M.; Pegg, D. T.; Brooks, W.; Bendall, M. R. J. Am. Chem. Soc. 1981, 103, 727–728.

    CAS  Google Scholar 

  99. Brevard, C.; Schimpf, R. J. Magn. Reson. 1982, 47, 528–534.

    CAS  Google Scholar 

  100. Holmes, B. S.; Chingas, G. G; Moniz, W. B.; Ferguson, R. C. Macromol. 1981, 14, 1785–1787.

    CAS  Google Scholar 

  101. Bolton, P. H.; Bodenhausen, G. J. Magn. Reson. 1981, 43, 339–342.

    CAS  Google Scholar 

  102. Morris, G. A.; Hall, L. D. J. Am. Chem. Soc. 1981, 103, 4703–4711.

    CAS  Google Scholar 

  103. Van Divender, J. M.; Hutton, W. C. J. Magn. Reson. 1982, 48, 272–279.

    Google Scholar 

  104. Finster, D. C.; Hutton, W. C.; Grimes, R. N. J. Am. Chem. Soc. 1980, 102, 400–401.

    CAS  Google Scholar 

  105. Sorensen, O. W.; Freeman, R.; Frenkiel, T.; Mareci, T. H.; Schuck, R. J. Magn. Reson. 1982, 46, 180–184.

    CAS  Google Scholar 

  106. Bax, A.; Freeman, R.; Morris, G. A. J. Magn. Reson. 1981, 42, 164–168.

    CAS  Google Scholar 

  107. Bolton, P. H.; Bodenhausen, G. J. Am. Chem. Soc. 1979, 101, 1080–1084.

    CAS  Google Scholar 

  108. Bolton, P. H. J. Magn. Reson. 1982, 48, 336–340; Bax, A. J. Magn. Reson. 1983, 53, 149–153; Bax, A.; Drobny, G. J. Magn. Reson. 1985,61, 306–320.

    CAS  Google Scholar 

  109. Nagayama, K.; Wüthrich, K.; Ernst, R. R. Biochem. Biophys. Res. Commun. 1979, 90, 305–311.

    PubMed  CAS  Google Scholar 

  110. Freeman, R.; Morris, G. A. J. Magn. Reson. 1978, 29, 173–176; Morris, G. A.; Nayler, G. L.; Shaka, A. J.; Keeler, J.; Freeman, R. J. Magn. Reson. 1984, 58, 155–160, 161–166.

    CAS  Google Scholar 

  111. Opella, S. J.; Cross, T. A. J. Magn. Reson. 1980, 37, 171–175.

    CAS  Google Scholar 

  112. Bendall, M. R.; Doddrell, D. M.; Pegg, D. T. J. Am. Chem. Soc. 1981, 103, 4603–4605.

    CAS  Google Scholar 

  113. Brown, D. W.; Nakashima, T. T.; Rabenstein, D. L. J. Magn. Reson. 1981, 45, 302–314.

    CAS  Google Scholar 

  114. Bolton, P. H. J. Magn. Reson. 1981, 45, 418–421.

    CAS  Google Scholar 

  115. Nagayama, K.; Wüthrich, K. Eur. J. Biochem. 1981, 114, 365–374.

    PubMed  CAS  Google Scholar 

  116. Wagner, G.; Kumar, A.; Wuthrich, K. Eur. J. Biochem. 1981, 114, 375–384; Wuthrich, K. NMR of Proteins and Nucleic Acids, Wiley: New York, 1986, 432 pp.

    Google Scholar 

  117. Haeberlen, U . Adv. Magn. Reson. 1976; Suppl. 1, 1–186.

    Google Scholar 

  118. Andrew, E. R. Prog. NMR Spectrosc. 1971, 8, 1–39.

    CAS  Google Scholar 

  119. Andrew, E. R. Phil. Trans. R. Soc. London Ser. A 1981, 299, 505–520; Int. Rev. Phys. Chem. 1981, 1, 195–224.

    CAS  Google Scholar 

  120. Andrew, E. R.; Farnell, L. F.; Gledhill, T. D. Phys. Rev. Lett. 1967, 19, 6–7.

    CAS  Google Scholar 

  121. Herzfeld, J.; Berger, A. E. J. Chem. Phys. 1980, 73, 6021–6030.

    CAS  Google Scholar 

  122. Maricq, M. M.; Waugh, J. S. J. Chem. Phys. 1979, 70, 3300–3316.

    CAS  Google Scholar 

  123. Waugh, J. S.; Huber, L. M.; Haeberlen, U. Phys. Rev. Lett. 1968, 20, 180–182.

    CAS  Google Scholar 

  124. Rhim, W. K.; Burum, D. P.; Elleman, D. D. J. Chem. Phys. 1979, 71, 3139–3141.

    CAS  Google Scholar 

  125. Sarles, L. R.; Cotts, R. M. Phys. Rev. 1958, 111, 853–859.

    CAS  Google Scholar 

  126. Mehring, M.; Pines, A.; Rhim, W.-K.; Waugh, J. S. J. Chem. Phys. 1971, 54, 3239–3240.

    CAS  Google Scholar 

  127. Schaefer, J.; Stejskal, E. O. J. Am. Chem. Soc. 1976, 98, 1030–1032.

    Google Scholar 

  128. Earl, W. L.; VanderHart, D. L. J. Magn. Reson. 1982, 48, 35–54.

    CAS  Google Scholar 

  129. Phil. Trans. R. Soc. London, Ser. A 1981, 299, (especially pages 593–663).

    Google Scholar 

  130. Wasylishen, R. E.; Fyfe, C. A. Annu. Rep. NMR Spectrosc. 1982, 12, 1–80.

    CAS  Google Scholar 

  131. Fyfe, C. A. Solid State NMR for Chemists, CFC Press: Guelph, Ontario, Canada, 1983.

    Google Scholar 

  132. Lippmaa, E. T.; Alia, M. A.; Pehk, T. J.; Engelhardt, G. J. Am. Chem. Soc. 1978, 100, 1929–1931.

    CAS  Google Scholar 

  133. Oldfield, E.; Schramm, S.; Meadows, M. D.; Smith, K. A.; Kinsey, R. A.; Ackerman, J. J. Am. Chem. Soc. 1982, 104, 919–920; Ganapathy, S.; Schramm, S.; Oldfield, E. J. Chem. Phys. 1982, 77, 4360–4365; Meadows, M. D.; Smith, K. A.; Kinsey, R. A.; Rothgeb, T. M.; Scarjune, R. P.; Oldfield, E. Proc. Natl. Acad. Sci. USA 1982, 79, 1351–1355; Schramm, S.; Oldfield, E. Am. Chem. Soc. 1984, 106, 2502–2506; Oldfield, E.; Timken, H. K. C.; Montez, B.; Ramachandran, R.Nature 1985, 318, 163–165;

    CAS  Google Scholar 

  134. Lippmaa, E.; Samoson, A.; Mägi, M. J. Am. Chem. Soc. 1986, 108, 1730–1735.

    CAS  Google Scholar 

  135. Opella, S. J. Annu. Rev. Phys. Chem. 1982, 33, 533–562.

    CAS  Google Scholar 

  136. Landolt-Börnstein, Zahlenwerte und Funktionen aus Naturwissenschaften und Technik, New Series, Group II; Springer-Verlag: Berlin, 1974; Vol. 6, pp. 2–383 to 2–434.

    Google Scholar 

  137. Emsley, J. W.; Lindon, J. C. NMR Spectroscopy Using Liquid Crystal Solvents, Pergamon: Oxford, 1975, 367 pp.; Khetrapal, C. L.; Kunwar, A. C. Adv. Liq. Cryst. 1983,6, 173–242.

    Google Scholar 

  138. Saupe, A. Z. Naturforsch. A 1964, 19, 161–171.

    Google Scholar 

  139. Daborn, G. T.; Ferguson, W. I.; Handy, N. C. Chem. Phys. 1980, 50, 255–263.

    CAS  Google Scholar 

  140. Khetrapal, C. L.; Kunwar, A. C. Adv. Magn. Reson. 1977, 9, 302–422.

    Google Scholar 

  141. Khetrapal, C. L.; Kunwar, A. C; Tracey, A. S.; Diehl, P. NMR Basic Princ. Prog. 1975, 9.

    Google Scholar 

  142. Buckingham, A. D.; McLauchlan, K. A. Prog. NMR Spectrosc. 1967, 2, 63–109.

    Google Scholar 

  143. Haeberlen, U.; Waugh, J. S. Phys. Rev. 1968, 175, 453–467.

    CAS  Google Scholar 

  144. Veeman, W. S. Phil. Trans. R. S.c. London, Ser. A 1981, 299, 629–641; Prog. NMR Spectrosc. 1984, 16, 193–235.

    CAS  Google Scholar 

  145. Zilm, K. W.; Beeler, A. J.; Grant, D. M.; Michl, J.; Chou, T.-C.; Allred, E. L. J. Am. Chem. Soc. 1981, 103, 2119–2120.

    CAS  Google Scholar 

  146. Zilm, K. W.; Conlin, R. T.; Grant, D. M.; Michl, J. J. Am. Chem. Soc. 1980, 102, 6672–6676; 1978, 100, 8038–8039.

    Google Scholar 

  147. Facelli, J. C.; Orendt, A. M.; Beeler, A. J.; Solum, M. S.; Depke, G.; Malsch, K. D.; Downing, J. W.; Murthy, P. S.; Grant, D. M.; Michl, J. J. Am. Chem. Soc. 1985, 107, 5649–6754; Beeler, A. J.; Orendt, A. M.; Grant, D. M.; Cutts, P. W.; Michl, J.; Zilm, K. W.; Downing, J. W.; Facelli, J. C; Schindler, M. S.; Kutzelnigg, W. J. Am. Chem. Soc. 1984, 106, 7672–7676; Strub, H.; Beeler, A. J.; Grant, D. M.; Michl, J.; Cutts, P. W.; Zilm, K. W. J. Am. Chem. Soc. 1983, 105, 3333–3334.

    Google Scholar 

  148. Dutasta, J. P.; Robert, J. B.; Wiesenfeld, L. ACS Symp. Ser. 1981, 171, 581–584.

    CAS  Google Scholar 

  149. Robert, J. B.; Wiesenfeld, L. Mol. Phys. 1981, 44, 319–327.

    CAS  Google Scholar 

  150. Bodenhausen, G.; Stark, R. E.; Ruben, D. J.; Griffin, R. G. Chem. Phys. Lett. 1979, 67, 424–427.

    CAS  Google Scholar 

  151. Opella, S. J.; Hexern, J. G.; Frey, M. H.; Cross, T. A. Phil. Trans. R. Soc. London, Ser. A 1981, 299, 665–683; Hexern, J. G.; Frey, M. H.; Opella, S. J. J. Am. Chem. Soc. 1981, 103, 224–226

    CAS  Google Scholar 

  152. Griffin, R. G.; Bodenhausen, G.; Haberkorn, R. A.; Huang, T. H.; Munowitz, M.; Osredkar, R.; Ruben, D. J.; Stark, R. E.; van Willigen, H. Phil. Trans. R. Soc. London,, Ser. A 1981, 299, 547–563.

    CAS  Google Scholar 

  153. Drobny, G. P. Annu. Rev. Phys. Chem. 1985, 36, 451–489.

    CAS  Google Scholar 

  154. Sørensen, O. W.; Ernst R. R. J. Magn. R.son. 1983, 51, 477–489; Sørensen, O. W.; Eich, G.; Levitt, M. H.; Bodenhausen, G.; Ernst, R. R. Prog. NMR Spectrosc. 1983, 16, 163–192.

    Google Scholar 

  155. Sandstrom, J. Dynamic NMR Spectroscopy, Academic Press: New York, 1982, 226 pp.

    Google Scholar 

  156. Steigel, A. In NMR Basic Princ. Prog. 1978, 15, 1–53.

    CAS  Google Scholar 

  157. Mann, B. E. Annu. Rep. NMR Spectrosc. 1982, 12, 263–286; Martin, M. L.; Sun, X. Y.; Martin, G. J. Annu. Rep. NMR Spectrosc. 1985, 16, 187–364.

    CAS  Google Scholar 

  158. Dynamic NMR Spectroscopy, Jackman, L. M.; Cotton, F. A., Ed.; Academic Press: New York, 1975; 660 pp.

    Google Scholar 

  159. Oki, M., Ed.; Applications of Dynamic NMR Spectroscopy to Organic Chemistry, VCH Verlag: Weinheim, 1985, 423 pp.

    Google Scholar 

  160. Forsen, S.; Hoffmann, R. A. J. Chem. Phys. 1964, 40, 1189–1196; 1963, 39, 2892–2901.

    CAS  Google Scholar 

  161. Alger, J. R.; Prestegard, J. H. J. Magn. Reson. 1977, 27, 137–141.

    CAS  Google Scholar 

  162. Campbell, I. D.; Dobson, C. M.; Ratcliffe, R. G.; Williams, R. J. P. J. Magn. Reson. 1978, 29, 397–417.

    CAS  Google Scholar 

  163. Baine, P.; Gerig, J. T.; Stock, A. D. Org. Magn. Reson. 1981, 17, 41–45.

    CAS  Google Scholar 

  164. Jeener, J.; Meier, B. H.; Bachmann, P.; Ernst, R. R. J. Chem. Phys. 1979, 71, 4546–4553.

    CAS  Google Scholar 

  165. Macura, S.; Huang, Y.; Suter, D.; Ernst, R. R. J. Magn. Reson. 1981, 43, 259–281.

    CAS  Google Scholar 

  166. Bodenhausen, G.; Ernst, R. R. J. Am. Chem. Soc. 1982, 104, 1304–1309.

    CAS  Google Scholar 

  167. Bodenhausen G.; Ernst, R. R. J. Magn. Reson. 1981, 45, 367–373.

    CAS  Google Scholar 

  168. Dobson, C. M.; Olejniczak, E. T.; Poulsen, F. M.; Ratcliffe, R. G. J. Magn. Reson. 1982, 48, 97–110.

    CAS  Google Scholar 

  169. Spiess, H. W. NMR Basic Princ. Prog. 1978, 15, 55–214.

    CAS  Google Scholar 

  170. McKnett, C. L.; Dybowski, C. R.; Vaughan, R. W. J. Chem. Phys. 1975, 63, 4578–581.

    CAS  Google Scholar 

  171. Berglund, B.; Tegenfeldt, J. J. Magn. Reson. 1977, 27, 315–323.

    CAS  Google Scholar 

  172. Waugh, J. S. Ann. N. Y. Acad. Sci. 1958, 70, 900–926.

    CAS  Google Scholar 

  173. Reynhardt, E. C. J. Magn. Reson. 1977, 28, 441–458.

    CAS  Google Scholar 

  174. Huntress, W. T. Adv. Magn. Reson. 1970, 4, 1–37.

    CAS  Google Scholar 

  175. Jonas, J. Adv. Magn. Reson. 1973, 6, 73–139.

    Google Scholar 

  176. Batley, M.; Redmond, J. W. J. Magn. Reson. 1982, 49, 172–174.

    CAS  Google Scholar 

  177. Reilly, C. A.; McConnell, H. M.; Meisenheimer, R. G. Phys. Rev. A 1955, 98, 264–265.

    CAS  Google Scholar 

  178. Zimmerman, J. R.; Foster, M. R. J. Phys. Chem. 1957, 61, 282–289.

    CAS  Google Scholar 

  179. Li, N. C; Scruggs, R. L.; Becker, E. D. J. Am. Chem. Soc. 1962, 84, 4650–4654.

    CAS  Google Scholar 

  180. Douglass, D. C.; Fratiello, A. J. Chem. Phys. 1963, 39, 3161–3162.

    CAS  Google Scholar 

  181. Lagodzinskaya, G. V.; Klimenko, I. Y. J. Magn. Reson. 1982, 49, 1–7.

    CAS  Google Scholar 

  182. Kovesdi, I. J. Magn. Reson. 1981, 43, 1–7.

    CAS  Google Scholar 

  183. Raynes, W. T.; Buckingham, A. D.; Bernstein, H. J. J. Chem. Phys. 1962, 36, 3481–3488.

    CAS  Google Scholar 

  184. Buckingham, A. D. Can. J. Chem. 1960, 38, 300–307.

    CAS  Google Scholar 

  185. Buckingham, A. D.; Schaefer, T.; Schneider, W. G. J. Chem. Phys. 1960, 32, 1227–1233.

    CAS  Google Scholar 

  186. Laszlo, P. Prog. NMR Spectrosc. 1968, 3, 231–402.

    Google Scholar 

  187. Jameson, C. J.; Jameson, A. K.; Cohen, S. M. J. Magn. Reson. 1975, 19, 385–392.

    CAS  Google Scholar 

  188. Rummens, F. H. A. NMR Basic Princ. Prog. 1975, 10, 1–118.

    Google Scholar 

  189. Qiu, Z. W.; Grant, D. M.; Pugmire, R. J. J. Am. Chem. Soc. 1982, 104, 2747–2753.

    CAS  Google Scholar 

  190. Jameson, C. J. Bull. Magn. Reson. 1980, 3, 3–28.

    CAS  Google Scholar 

  191. Jameson, C. J.; Jameson, A. K.; Burrell, P. M. J. Chem. Phys. 1980, 73, 6013–6020.

    CAS  Google Scholar 

  192. Barfield, M.; Johnston, M. D. Jr. Chem. Rev. 1973, 73, 53–73.

    CAS  Google Scholar 

  193. Emsley, J. W.; Phillips, L.; Wray, V. Prog. NMR Spectrosc. 1975, 10, 83–756.

    Google Scholar 

  194. Batiz-Hernandez, H.; Bernheim, R. A. Prog. NMR Spectrosc. 1967, 3, 63–85; Hansen, P. E. Annu. Rep. NMR Spectrosc. 1983, 15, 105–233; Forsyth, D. A. Isotopes in Organic Chemistry, 1984, 6.

    CAS  Google Scholar 

  195. Jameson, C. J. NMR Spec. Per. Rep. R.S.C. 1980, 10, 1–17; Jameson, C. J.; Osten, H. J. Annu. Rep. NMR Spectrosc. 1986, 17, 1–78.

    Google Scholar 

  196. Anet, F. A. L.; Bagus, V. J.; Hewett, A. P. W.; Saunders, M. J. Am. Chem. Soc. 1980, 102, 3945–3946.

    CAS  Google Scholar 

  197. Lindman, B.; Forsén, S. NMR Basic Princ. Prog. 1976, 12, 1–365.

    Google Scholar 

  198. Webb, G. A. Annu. Rep. NMR Spectrosc. 1975, 6A, 1–145.

    Google Scholar 

  199. Orrell, K. G. Annu. Rep. NMR Spectrosc. 1979, 9, 1–124.

    CAS  Google Scholar 

  200. Reuben, J. Prog. NMR Spectrosc. 1973, 9, 1–70.

    Google Scholar 

  201. LaMar, G. N.; Horrocks, W. DeW., Jr.; Holm, R. H., Ed.; NMR of Paramagnetic Molecules, Academic Press: New York, 1973.

    Google Scholar 

  202. Jameson, C. J.; Jameson, A. K.; Cohen, S. M. Mol. Phys. 1975, 29, 1919–1927; J. Chem. Phys. 1976, 65, 3397–3400; Johnson, C. S.; Waugh, J. S. J. Chem. Phys. 1961, 35, 2020–2024; Lipsicas, M.; Siegel, M.; Piott, J.; Higgins, T.; Gerber, J. A. J. Magn. Reson. 1976, 22, 303–314.

    CAS  Google Scholar 

  203. Swift, T. J. pp. 53–177 in ref. 192.

    Google Scholar 

  204. Bulsing, J. M.; Sanders, J. K. M.; Hall, L. D. J. Chem. Soc., Chem. Commun. 1981, 1201–1203.

    Google Scholar 

  205. Witanowski, M.; Stefaniak, L.; Kamienski, B.; Biernet, S.; Webb, G. A. J. Magn. Reson. 1981, 43, 456–462.

    CAS  Google Scholar 

  206. Brown, A. J.; Howarth, O. W.; Moore, P. J. Am. Chem. Soc. 1978, 100, 713–718.

    CAS  Google Scholar 

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Authors and Affiliations

  1. Department of Chemistry, University of Illinois, Chicago, Illinois, 60680, USA

    Cynthia J. Jameson

  2. Department of Chemistry, The Open University, Milton Keynes, MK7 6AA, England

    Joan Mason

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  1. The Open University, Milton Keynes, Buckinghamshire, England

    Joan Mason

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Jameson, C.J., Mason, J. (1987). The Parameters of NMR Spectroscopy. In: Mason, J. (eds) Multinuclear NMR. Springer, Boston, MA. https://doi.org/10.1007/978-1-4613-1783-8_2

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