Abstract
The range of 13C chemical shifts is normally 0-230 ppm. In a proton- decoupled spectrum they are found as sharply resolved single peaks, and they are measured with reference to TMS taken as zero, although addition of TMS is often not carried out since the position of the solvent signal with reference to TMS is known, and the signals may be calibrated with reference to the solvent signal. The chemical shifts of common solvents are presented in Table 4.1.
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© 1986 Springer-Verlag New York Inc.
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Atta-ur-Rahman (1986). Chemical Shifts and Spin—Spin Couplings in 13C-NMR Spectroscopy. In: Nuclear Magnetic Resonance. Springer, New York, NY. https://doi.org/10.1007/978-1-4612-4894-1_4
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DOI: https://doi.org/10.1007/978-1-4612-4894-1_4
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