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Nondestructive Determination of Arsenic in urine by Epithermal Neutron Activation Analysis and Compton Suppression

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Nuclear Analytical Methods in the Life Sciences

Abstract

Epithermal neutron activation analysis, in conjunction with Compton suppression, has been employed to determine arsenic levels in artificially doped urine samples. Typical detection limits were of the order of 10 ng/g. Replicate determinations gave precision values between 2 and 12%, whereas accuracy measurements were between ± 1 and ±20%. Biological and geological reference materials from the National Institute of Standards and Technology (NIST) were also analyzed for arsenic content. Typically, the precision achieved again was between 2 and 12%, whereas the accuracy measurements were in excellent agreement with the certified values.

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References

  1. E. L. Baker, C. G. Hayes, P. J. Landrigan, J. L. Hanke, R. T. Leger, W. J. Houseworth, and J. M. Harrington, Am. J. Epidemiol. 106, 261 (1977).

    PubMed  Google Scholar 

  2. F. Peter, G. Growcock, and G. Strung, Anal. Chim. Acta 104, 177 (1979).

    Article  CAS  Google Scholar 

  3. J. P. Buchet, R. Lauwerys, and H. Roels, Int. Arch. Occup. Environ. Health 46, 11 (1980).

    Article  PubMed  CAS  Google Scholar 

  4. G. V. Iyengar, Biol. Trace Element Res. 12, 263 (1987).

    Article  CAS  Google Scholar 

  5. K. Heydorn, Neutron Activation Analysis for Clinical Trace Element Research, vol. 2, CRC Press, Boca Raton, FL, 1984, pp. 79–80.

    Google Scholar 

  6. R. Cornelius, A. Speecke, and J. Hoste, Anal. Chim. Acta 78, 317 (1975).

    Article  Google Scholar 

  7. N. V. Bagdavadze, and L. M. Mosulishvili, J. Radioanal Chem. 24, 65 (1974).

    Article  Google Scholar 

  8. L. E. Wangen, and E. S. Gladney, Anal Chim. Acta 96, 271 (1977).

    Article  Google Scholar 

  9. S. Landsberger and A. Simsons, Biol. Trace Element Res. 13, 357 (1987).

    Article  CAS  Google Scholar 

  10. R. O. Peach, Neutron Spectrum Unfolding of the University of Illinois Advanced TRIGA, M. S. Thesis, Dept. Nuclear Eng., University of Illinois, Urbana, IL, 1988.

    Google Scholar 

  11. L. A. Currie, Anal. Chem. 40, 540 (1968).

    Article  Google Scholar 

  12. R. Zeisler, R. R. Greenberg, and S. F. Stone, J. Nucl. Radioal. Chem. 124, 47 (1988).

    Article  CAS  Google Scholar 

  13. E. S. Gladney, B. T. O’Malley, I. Roelandts, and T. E. Gills, Compilation of Elemental Concentration Data of NBS Clinical, Biological, Geological, and Environmental Standard Reference Material, NIST Special Report 260411 US Department of Commerce, Washington, DC, 1987.

    Google Scholar 

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© 1990 Springer Science+Business Media New York

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Landsberger, S., Swift, G., Neuhoff, J. (1990). Nondestructive Determination of Arsenic in urine by Epithermal Neutron Activation Analysis and Compton Suppression. In: Zeisler, R., Guinn, V.P. (eds) Nuclear Analytical Methods in the Life Sciences. Humana Press, Totowa, NJ. https://doi.org/10.1007/978-1-4612-0473-2_4

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  • DOI: https://doi.org/10.1007/978-1-4612-0473-2_4

  • Publisher Name: Humana Press, Totowa, NJ

  • Print ISBN: 978-1-4612-6777-5

  • Online ISBN: 978-1-4612-0473-2

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