Skip to main content

An X-Ray Microprobe Facility Using Synchrotron Radiation

  • Chapter

Abstract

An X-ray microprobe for trace elemental analysis at micrometer spatial resolutions, using synchrotron radiation (SR), is under development. The facility consists of two beamlines, one including a 1:1 focusing mirror and the other an 8:1 ellipsoidal mirror. At present, “white light” is used for excitation of the characteristic X-ray fluorescence lines. Sensitivities in thin biological samples are in the range of 2–20 fg in 100μm2 areas in 5 min irradiation times. Scanning techniques, as well as microtomography and chemical speciation, are discussed. Application to a specific biomedical study is included.

Author to whom all correspondence and reprint requests should be addressed.

This is a preview of subscription content, log in via an institution.

Buying options

Chapter
USD   29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD   169.00
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
USD   219.99
Price excludes VAT (USA)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info
Hardcover Book
USD   219.99
Price excludes VAT (USA)
  • Durable hardcover edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Learn about institutional subscriptions

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

References

  1. K. W. Jones and B. M. Gordon, Anal Chem. 61, 341A (1989).

    CAS  Google Scholar 

  2. A. C. Thompson, J. H. Underwood, Y. Wu, R. D. Giauque, K. W. Jones, and M. L. Rivers, Nucl. Instr. Methods Phys. Res. A266, 318 (1988).

    CAS  Google Scholar 

  3. N, Gurker, X-Ray Spect. 14, 74 (1985).

    Article  Google Scholar 

  4. A. Knol, M. Bavdas, N. Gurker, P. Ketelsen, W. Petersen, M. H. Salehi, and T. Dietrich, J. Res. Natl. Bur. Stand. 93, 379 (1988).

    Google Scholar 

  5. P. Spanne and M. L. Rivers, Nucl. Instr. Methods Phys. Res. B24/25, 1063 (1987).

    Article  Google Scholar 

  6. B. M. Gordon, Biol. Trace Elem. Res. 12, 153 (1987).

    Article  CAS  Google Scholar 

  7. K. W. Jones and J. G. Pounds, Biol. Trace Elem. Res. 12, 3 (1987).

    Article  CAS  Google Scholar 

  8. G. Tolkiehn and W. Petersen, Nucl. Instr. Methods Phys. Res. 215, 515 (1983).

    Article  CAS  Google Scholar 

  9. P. A. Pella, D. E. Newbury, E. B. Steel, and D. H. Blackburn, Anal Chem. 58, 1133 (1986).

    Article  CAS  Google Scholar 

  10. R. D. Giauque, A. C. Thompson, J. H. Underwood, Y. Wu, K. W. Jones, and M. L. Rivers, Anal Chem. 60, 855 (1988).

    Article  PubMed  CAS  Google Scholar 

  11. K. Themner, N. E. G. Lövestam, U. A. S. Tapper, and K. G. Malmqvist, Nucl. Instr. Methods Phys. Res. B22, 126 (1987).

    Article  CAS  Google Scholar 

  12. B. M. Gordon, A. L. Hanson, K. W. Jones, J. G. Pounds, M. L. Rivers, G. Schidlovsky, P. Spanne, and S. R. Sutton, Nucl. Instr. Methods Phys. Res. B45, 527 (1990).

    Article  CAS  Google Scholar 

  13. R. S. Bockman, M. Repo, D. Warrell, J. G. Pounds, W. M. Kwiatek, G. J. Long, G. Schidlovsky, and K. W. Jones, X-Ray Microscopy II, D. Sayre, M. Howells, J. Kirz, and H. Rarback, eds., Springer-Verlag, New York, 1988, p. 391.

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Editor information

Editors and Affiliations

Rights and permissions

Reprints and permissions

Copyright information

© 1990 Springer Science+Business Media New York

About this chapter

Cite this chapter

Gordon, B.M. et al. (1990). An X-Ray Microprobe Facility Using Synchrotron Radiation. In: Zeisler, R., Guinn, V.P. (eds) Nuclear Analytical Methods in the Life Sciences. Humana Press, Totowa, NJ. https://doi.org/10.1007/978-1-4612-0473-2_15

Download citation

  • DOI: https://doi.org/10.1007/978-1-4612-0473-2_15

  • Publisher Name: Humana Press, Totowa, NJ

  • Print ISBN: 978-1-4612-6777-5

  • Online ISBN: 978-1-4612-0473-2

  • eBook Packages: Springer Book Archive

Publish with us

Policies and ethics