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Nanoindentation Testing

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Nanoindentation

Part of the book series: Mechanical Engineering Series ((MES))

Abstract

The goal of the majority of nanoindentation tests is to extract elastic modulus and hardness of the specimen material from load-displacement measurements. Conventional indentation hardness tests involve the measurement of the size of a residual plastic impression in the specimen as a function of the indenter load. This provides a measure of the area of contact for a given indenter load. In a nanoindentation test, the size of the residual impression is often only a few microns and this makes it very difficult to obtain a direct measure using optical techniques. In nanoindentation testing, the depth of penetration beneath the specimen surface is measured as the load is applied to the indenter. The known geometry of the indenter then allows the size of the area of contact to be determined. The procedure also allows for the modulus of the specimen material to be obtained from a measurement of the “stiffness” of the contact, that is, the rate of change of load and depth.

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Notes

  1. 1.

    Recall that the term “indentation strain ” refers to the ratio a/R.

  2. 2.

    1 kgf = 9.806 N.

  3. 3.

    Generally we use the term “load” to indicate that which is applied to the indenter, and “force” to that which is measured by the force sensor. In some instruments, it is the load applied that is recorded, while in others (which have a force sensor), it is the force that is measured. Ideally load and force would be identical and so either term can be used.

References

  1. E.S. Berkovich, “Three-faceted diamond pyramid for micro-hardness testing,” Ind. Diamond Rev. 11 127, 1951, pp. 129–133.

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  2. B.R. Lawn, Fracture of Brittle Solids, 2nd Ed., Cambridge University Press, Cambridge, 1993.

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  3. F. Knoop, C.G. Peters, and W.B. Emerson, “A sensitive pyramidal-diamond tool for indentation measurements,” Research Paper 1220, Journal of Research, National Bureau of Standards, 23 1, 1939.

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  4. D.B. Marshall, T. Noma, and A.G. Evans, “A simple method for determining elastic-modulus-to-hardness ratios using Knoop indentation measurements,” J. Am. Ceram. Soc. 65, 1980, pp. C175–C176.

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Correspondence to Anthony C. Fischer-Cripps .

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© 2011 Springer Science+Business Media, LLC

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Fischer-Cripps, A.C. (2011). Nanoindentation Testing. In: Nanoindentation. Mechanical Engineering Series. Springer, New York, NY. https://doi.org/10.1007/978-1-4419-9872-9_2

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  • DOI: https://doi.org/10.1007/978-1-4419-9872-9_2

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  • Publisher Name: Springer, New York, NY

  • Print ISBN: 978-1-4419-9871-2

  • Online ISBN: 978-1-4419-9872-9

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