Skip to main content

Infrared Spectroscopy

  • Chapter
  • First Online:
Food Analysis

Part of the book series: Food Analysis ((FSTS))

Abstract

Infrared (IR) spectroscopy refers to measurement of the absorption of different frequencies of IR radiation by foods or other solids, liquids, or gases. IR spectroscopy began in 1800 with an experiment by Herschel. When he used a prism to create a spectrum from white light and placed a thermometer at a point just beyond the red region of the spectrum, he noted an increase in temperature. This was the first observation of the effects of IR radiation. By the 1940s, IR spectroscopy had become an important tool used by chemists to identify functional groups in organic compounds. In the 1970s, commercial near-IR reflectance instruments were introduced that provided rapid quantitative determinations of moisture, protein, and fat in cereal grains and other foods. Today, IR spectroscopy is used widely in the food industry for both qualitative and quantitative analysis of ingredients and finished foods.

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Chapter
USD 29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD 64.99
Price excludes VAT (USA)
  • Available as EPUB and PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
USD 84.99
Price excludes VAT (USA)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

References

  1. AOAC International (2007) Official methods of analysis, 18th edn., 2005; Current through revision 2, 2007 (On-line). AOAC International, Gaithersburg, MD

    Google Scholar 

  2. Lahner BS (1996) Evaluation of Aegys MI 600 Fourier transform infrared milk analyzer for analysis of fat, protein, lactose, and solids nonfat: A compilation of eight independent studies. J AOAC Int 79:1388

    Google Scholar 

  3. van de Voort FR, Ismail AA, Sedman J (1995) A rapid, automated method for the determination of cis and trans content of fats and oils by Fourier transform infrared spectroscopy. J Am Oil Chem’ Soc 72:873

    Article  Google Scholar 

  4. Gurdeniz G, Toklati F, Ozen B (2007) Differentiation of mixtures of monovarietal olive oils by mid-infrared spectroscopy and chemometrics. Eur J Lipid Sci Technol 109:1194–1202

    Article  CAS  Google Scholar 

  5. An introduction to Raman for the infrared spectroscopist. Inphotonics Technical Note No. 11, Norwood, MA (http://www.inphotonics.com/technote11.pdf)

  6. Thygesen LG, Lokke MM, Micklander E, Engelsen SB (2003) Vibrational microspectroscopy of food. Raman vs. FT-IR. Trends Food Sci Technol 14:50–57

    Article  CAS  Google Scholar 

  7. Martens H, Naes T (2001) Multivariate calibration by data compression. Ch. 4, In: Williams PC, Norris KH (eds) Near infrared technology in the agricultural and food industries, 2nd edn. American Association of Cereal Chemists, St. Paul, MN, p 75

    Google Scholar 

  8. Martens H, Naes T (2001) Multivariate calibration by data compression. Ch. 4, In: Williams PC, Norris KH (eds) Near infrared technology in the agricultural and food industries, 2nd edn. American Association of Cereal Chemists, St. Paul, MN, pp 59–100

    Google Scholar 

  9. Delwiche SR, Chen YR, Hruschka WR (1995) Differentiation of hard red wheat by near-infrared analysis of bulk samples. Cereal Chem 72:243

    CAS  Google Scholar 

  10. Evans DG, Scotter CN, Day LZ, Hall MN (1993) Determination of the authenticity of orange juice by discriminant analysis of near infrared spectra. A study of pretreatment and transformation of spectral data. J Near Infrared Spectrosc 1:33

    Article  CAS  Google Scholar 

  11. Bertran E, Blanco M, Coello J, Iturriaga H, Maspoch S, Montoliu I (2000) Near infrared spectrometry and pattern recognition as screening methods for the authentication of virgin olive oils of very close geographical origins. J Near Infrared Spectrosc 8:45

    Article  CAS  Google Scholar 

  12. Alomar D, Gallo C, Castaneda M, Fuchslocher R (2003) Chemical and discriminant analysis of bovine meat by near infrared reflectance spectroscopy (NIRS). Meat Sci 63:441

    Article  CAS  Google Scholar 

  13. Osborne BG, Fearn T, Hindle PH (1993) Practical NIR spectroscopy with application in food and beverage analysis. Longman, Essex, UK

    Google Scholar 

  14. Williams PC, Norris KH (eds) (2001) Near-infrared technology in the agricultural and food industries, 2nd edn. American Association of Cereal Chemists, St. Paul, MN

    Google Scholar 

  15. Ozaki Y, McClure WF, Christy AA (2006) Near-infrared spectroscopy in food science and technology. Wiley, Hoboken, NJ

    Book  Google Scholar 

  16. Woodcock T, Downey G, O’Donnel CP (2008) Review: better quality food and beverages: the role of near infrared spectroscopy. J Near Infrared Spectrosc 16:1

    Article  CAS  Google Scholar 

  17. AACC International (2010) Approved methods of analysis, 11th edn (On-line). The American Association of Cereal Chemists, St. Paul, MN

    Google Scholar 

  18. Kays SE, Windham WR, Barton FE (1998) Prediction of total dietary fiber by near-infrared reflectance spectroscopy in high-fat and high-sugar-containing cereal products. J Agric Food Chem 46:854

    Article  CAS  Google Scholar 

  19. Kays SE, Barton FE (2002) Near-infrared analysis of soluble and insoluble dietary fiber fractions of cereal food products. J Agric Food Chem 50:3024

    Article  CAS  Google Scholar 

  20. Kays WE, Barton FE, Windham WR (2000) Predicting protein content by near infrared reflectance spectroscopy in diverse cereal food products. J Near Infrared Spectrosc 8:35

    Article  CAS  Google Scholar 

  21. Oh EK, Grossklaus D (1995) Measurement of the components in meat patties by near infrared reflectance spectroscopy. Meat Sci 41:157

    Article  CAS  Google Scholar 

  22. Geesink GH, Schreutelkamp FH, Frankhuizen R, Vedder HW, Faber NM, Kranen RW, Gerritzen MA (2003) Prediction of pork quality attributes from near infrared reflectance spectra. Meat Sci 65:661

    Article  CAS  Google Scholar 

  23. Naganathan GK, Grimes LM, Subbiah J, Calkins CR, Samal A, Meyer G (2008) Visible/near-infrared hyperspectral imaging for beef tenderness prediction. Comput Electron Agric 64:225

    Article  Google Scholar 

  24. Windham WR, Lawrence KC, Feldner PW (2003) Prediction of fat content in poultry meat by near-infrared transmission analysis. J Appl Poult Res 12:69

    Article  CAS  Google Scholar 

  25. Solberg C, Fredriksen G (2001) Analysis of fat and dry matter in capelin by near infrared transmission spectroscopy. J Near Infrared Spectrosc 9:221

    Article  CAS  Google Scholar 

  26. Isakkson T, Nærbo G, Rukke EO (2001) In-line determination of moisture in margarine, using near infrared diffuse transmittance. J Near Infrared Spectrosc 9:11

    Article  Google Scholar 

  27. Pierce MM, Wehling RL (1994) Comparison of sample handling and data treatment methods for determining moisture and fat in Cheddar cheese by near-infrared spectroscopy. J Agri Food Chem 42:2830

    Article  CAS  Google Scholar 

  28. Rodriquez-Otero JL, Hermida M, Cepeda A (1995) Determination of fat, protein, and total solids in cheese by near infrared reflectance spectroscopy. J AOAC Int 78:802

    Google Scholar 

  29. Wu D, He Y, Feng S (2008) Short-wave near-infrared spectroscopy analysis of major compounds in milk powder and wavelength assignment. Anal Chim Acta 610:232

    Article  CAS  Google Scholar 

  30. Tarkosova J, Copikova J (2000) Determination of carbohydrate content in bananas during ripening and storage by near infrared spectroscopy. J Near Infrared Spectrosc 8:21

    Article  CAS  Google Scholar 

  31. Segtman VH, Isakkson T (2000) Evaluating near infrared techniques for quantitative analysis of carbohydrates in fruit juice model systems. J Near Infrared Spectrosc 8:109

    Article  Google Scholar 

  32. Camps C Christen D (2009) Non-destructive assessment of apricot fruit quality by portable visible-near infrared spectroscopy. LWT – Food Sci Technol 42:1125

    Google Scholar 

  33. Psotka J, Shadow W (1994) NIR analysis in the wet corn refining industry – A technology review of methods in use. Int Sugar J 96:358

    CAS  Google Scholar 

  34. Tarkosova J, Copikova J (2000) Fourier transform near infrared spectroscopy applied to analysis of chocolate. J Near Infrared Spectrosc 8:251

    Article  CAS  Google Scholar 

  35. Villareal CP, De la Cruz NM, Juliano BO (1994) Rice amylose analysis by near-infrared transmittance spectroscopy. Cereal Chem 71:292

    CAS  Google Scholar 

  36. Delwiche SR, Bean MM, Miller RE, Webb BD, Williams PC (1995) Apparent amylose content of milled rice by near-infrared reflectance spectrophotometry. Cereal Chem 72:182

    CAS  Google Scholar 

  37. Yildiz G, Wehling RL, Cuppett SL (2001) Method for determining oxidation of vegetable oils by near-infrared spectroscopy. J Am Oil Chem Soc 78:495

    Article  CAS  Google Scholar 

  38. Ng CL, Wehling RL, Cuppett SL (2007) Method for determining frying oil degradation by near-infrared spectroscopy. J Agric Food Chem 55:593

    Article  CAS  Google Scholar 

  39. Wehling RL, Jackson DS, Hooper DG, Ghaedian AR (1993) Prediction of wet-milling starch yield from corn by near-infrared spectroscopy. Cereal Chem 70:720

    CAS  Google Scholar 

  40. Paulsen MR, Singh M (2004) Calibration of a near-infrared transmission grain analyzer for extractable starch in maize. Biosyst Eng 89:79

    Article  Google Scholar 

  41. Psotka J (2001) Challenges of making accurate on-line near-infrared measurements. Cereal Foods World 46:568

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Randy L. Wehling .

Rights and permissions

Reprints and permissions

Copyright information

© 2010 Springer Science+Business Media, LLC

About this chapter

Cite this chapter

Wehling, R.L. (2010). Infrared Spectroscopy. In: Food Analysis. Food Analysis. Springer, Boston, MA. https://doi.org/10.1007/978-1-4419-1478-1_23

Download citation

Publish with us

Policies and ethics