Skip to main content

CHEMICAL SHRINKAGE AND CALCIUM HYDROXIDE CONTENT OF EARLY AGE PORTLAND CEMENT MONITORED WITH ULTRASONIC SHEAR WAVE REFLECTIONS

  • Conference paper
Measuring, Monitoring and Modeling Concrete Properties

Abstract

The ultrasonic wave reflection method, which measures the reflection coefficient (or reflection loss) of high frequency shear waves at an interface between a steel plate and a cementitious material, was used to monitor the early hydration process of Portland cement mortars with water-cement ratios of 0.35, 0.5 and 0.6. To obtain independent measures of cement hydration, chemical shrinkage and calcium hydroxide content of cement pastes with the same water-cement ratios were determined. The obtained results show that, at ages up to three days, the reflection loss measured on the mortars has a strong linear relationship to the chemical shrinkage and the calcium hydroxide content of the appropriate cement paste.

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Chapter
USD 29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD 169.00
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
USD 219.99
Price excludes VAT (USA)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info
Hardcover Book
USD 219.99
Price excludes VAT (USA)
  • Durable hardcover edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

References

  1. T. Öztürk, J. Rapoport, J. S. Popovics, S. P. Shah, Monitoring the setting and hardening of cement-based materials with ultrasound, Concr. Sci. Eng. 1 (2) 83–91 (1999).

    Google Scholar 

  2. J. Rapoport, J. S. Popovics, K. V. Subramaniam, S. P. Shah, The use of ultrasound to monitor the stiffening process of Portland cement concrete with admixtures, ACI Mat. J. 97,(6), 675–683 (2000).

    Google Scholar 

  3. T. Voigt, The Application of an Ultrasonic Shear Wave Reflection Method for Nondestructive Testing of Cement-Based Materials at Early Ages: An Experimental and Numerical Analysis (PhD Thesis, University of Leipzig, Germany, Books on Demand, Norderstedt, 244 p., 2005)

    Google Scholar 

  4. S. Mindess, J. F. Young, D. Darwin, Concrete (Prentice Hall, Upper Saddle River, NJ, 2nd ed., 644 pp., 2003)

    Google Scholar 

  5. B. El-Jazairi, J. M. Illston, Hydration of cement paste using the semi-isothermal method of derivative Thermogravimetry, Cem. Con. Res. 10 (3), 361–366 (1980).

    Article  Google Scholar 

  6. P. Mounanga, A. Khelidj, A. Loukili, V. Baroghel-Bouny, Predicting Ca(OH)2 content and chemical shrinkage of hydrating cement pastes using analytical approach, Cem. Con. Res. 34(2) 255–265 (2004).

    Article  Google Scholar 

  7. J. I., Bhatty, K. J. Reid, Use of thermal analysis in the hydration studies of a type I Portland cement produced from mineral tailings, Therm. Acta 91 (1), 95–105 (1985).

    Article  Google Scholar 

  8. J. I. Bhatty, D. Dollimore, G. A. Gamlen, R. J. Mangabhai, H. Olmez, Estimation of calcium hydroxide in OPC, OPC/PFA and OPC/PFA/polymer modified systems, Therm. Acta 106, 115–123 (1986).

    Article  Google Scholar 

  9. H. G. Midgley, Determination of calcium hydroxide in set Portland cements, Cem. Con. Res. 9(1), 77–82 (1979).

    Article  Google Scholar 

  10. T. Voigt, S.P. Shah, Properties of early age Portland cement mortar monitored with a shear wave reflection method, ACI Mat. J. 101(6), 473–482 (2004).

    Google Scholar 

  11. F. Jung, Ein einfaches Verfahren zur zerstöxrungsfreien Prüfung der Festigkeit von Beton (A simple method for nondestructive testing of the strength of concrete), Beton- und Stahlbeton 69(1), 16–19 (1974) (in German).

    Google Scholar 

  12. T. Knudsen, M. Geiker, Chemical shrinkage as an indicator of the stage of hardening. In RILEM (Ed.), International Conference on Concrete of Early Ages. Editions Anciens ENPC, Paris, vol. 1, pp. 163–165 (1982).

    Google Scholar 

  13. M. Geiker, Studies of Portland cement hydration by measurements of chemical shrinkage and a systematic evaluation of hydration curves by means of the dispersion model, (PhD thesis, Institute of Mineral Industry, Technical University of Denmark, Denmark, 1983)

    Google Scholar 

  14. L. J. Parrott, M. Geiker, W. A. Gutteridge, D. Killoh, Monitoring Portland cement hydration: Comparison of methods, Cem. Conc. Res. 20(6), 919–926 (1990).

    Article  Google Scholar 

  15. T. Voigt, C.U. Grosse, Z. Sun, S. P. Shah, H.-W. Reinhardt, Comparison of ultrasonic wave transmission and reflection measurements with P- and S-waves on early age mortar and concrete, Mat. Struct. 38 (282), 729–738 (2004).

    Article  Google Scholar 

  16. T. C. Powers, Absorption of water by Portland cement paste during the hardening process. Ind. Eng. Chem. 27(7), 790–794 (1935).

    Article  Google Scholar 

  17. W. Czernin, Cement chemistry and physics for civil engineers (Chemical Publishing Co., Inc, New York, 139 pp., 1962).

    Google Scholar 

  18. M. Geiker, T. Knudsen, Chemical shrinkage of Portland cement pastes, Cem. Con. Res. 12(5), 603–610 (1982).

    Article  Google Scholar 

  19. E. Tazawa, S. Miyazawa, T. Kasai, Chemical shrinkage and autogenous shrinkage of hydrating cement paste, Cem. Con. Res. 25(2), 288–292 (1995).

    Article  Google Scholar 

  20. S. Boivin, P. Acker, S. Rigaud, B. Clavaud, Experimental assessment of chemical shrinkage of hydrating cement pastes. In Tazawa, E. (Ed.), Autogenous shrinkage of concrete. Spon Press, Proceedings of the International Workshop organized by the JCI (Japan Concrete Institute), pp. 81–92 (1999).

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Editor information

Editors and Affiliations

Rights and permissions

Reprints and permissions

Copyright information

© 2006 Springer

About this paper

Cite this paper

Voigt, T., Shah, S.P. (2006). CHEMICAL SHRINKAGE AND CALCIUM HYDROXIDE CONTENT OF EARLY AGE PORTLAND CEMENT MONITORED WITH ULTRASONIC SHEAR WAVE REFLECTIONS. In: KONSTA-GDOUTOS, M.S. (eds) Measuring, Monitoring and Modeling Concrete Properties. Springer, Dordrecht. https://doi.org/10.1007/978-1-4020-5104-3_39

Download citation

  • DOI: https://doi.org/10.1007/978-1-4020-5104-3_39

  • Publisher Name: Springer, Dordrecht

  • Print ISBN: 978-1-4020-5103-6

  • Online ISBN: 978-1-4020-5104-3

  • eBook Packages: EngineeringEngineering (R0)

Publish with us

Policies and ethics