Abstract
The ultrasonic wave reflection method, which measures the reflection coefficient (or reflection loss) of high frequency shear waves at an interface between a steel plate and a cementitious material, was used to monitor the early hydration process of Portland cement mortars with water-cement ratios of 0.35, 0.5 and 0.6. To obtain independent measures of cement hydration, chemical shrinkage and calcium hydroxide content of cement pastes with the same water-cement ratios were determined. The obtained results show that, at ages up to three days, the reflection loss measured on the mortars has a strong linear relationship to the chemical shrinkage and the calcium hydroxide content of the appropriate cement paste.
Access this chapter
Tax calculation will be finalised at checkout
Purchases are for personal use only
Preview
Unable to display preview. Download preview PDF.
References
T. Öztürk, J. Rapoport, J. S. Popovics, S. P. Shah, Monitoring the setting and hardening of cement-based materials with ultrasound, Concr. Sci. Eng. 1 (2) 83–91 (1999).
J. Rapoport, J. S. Popovics, K. V. Subramaniam, S. P. Shah, The use of ultrasound to monitor the stiffening process of Portland cement concrete with admixtures, ACI Mat. J. 97,(6), 675–683 (2000).
T. Voigt, The Application of an Ultrasonic Shear Wave Reflection Method for Nondestructive Testing of Cement-Based Materials at Early Ages: An Experimental and Numerical Analysis (PhD Thesis, University of Leipzig, Germany, Books on Demand, Norderstedt, 244 p., 2005)
S. Mindess, J. F. Young, D. Darwin, Concrete (Prentice Hall, Upper Saddle River, NJ, 2nd ed., 644 pp., 2003)
B. El-Jazairi, J. M. Illston, Hydration of cement paste using the semi-isothermal method of derivative Thermogravimetry, Cem. Con. Res. 10 (3), 361–366 (1980).
P. Mounanga, A. Khelidj, A. Loukili, V. Baroghel-Bouny, Predicting Ca(OH)2 content and chemical shrinkage of hydrating cement pastes using analytical approach, Cem. Con. Res. 34(2) 255–265 (2004).
J. I., Bhatty, K. J. Reid, Use of thermal analysis in the hydration studies of a type I Portland cement produced from mineral tailings, Therm. Acta 91 (1), 95–105 (1985).
J. I. Bhatty, D. Dollimore, G. A. Gamlen, R. J. Mangabhai, H. Olmez, Estimation of calcium hydroxide in OPC, OPC/PFA and OPC/PFA/polymer modified systems, Therm. Acta 106, 115–123 (1986).
H. G. Midgley, Determination of calcium hydroxide in set Portland cements, Cem. Con. Res. 9(1), 77–82 (1979).
T. Voigt, S.P. Shah, Properties of early age Portland cement mortar monitored with a shear wave reflection method, ACI Mat. J. 101(6), 473–482 (2004).
F. Jung, Ein einfaches Verfahren zur zerstöxrungsfreien Prüfung der Festigkeit von Beton (A simple method for nondestructive testing of the strength of concrete), Beton- und Stahlbeton 69(1), 16–19 (1974) (in German).
T. Knudsen, M. Geiker, Chemical shrinkage as an indicator of the stage of hardening. In RILEM (Ed.), International Conference on Concrete of Early Ages. Editions Anciens ENPC, Paris, vol. 1, pp. 163–165 (1982).
M. Geiker, Studies of Portland cement hydration by measurements of chemical shrinkage and a systematic evaluation of hydration curves by means of the dispersion model, (PhD thesis, Institute of Mineral Industry, Technical University of Denmark, Denmark, 1983)
L. J. Parrott, M. Geiker, W. A. Gutteridge, D. Killoh, Monitoring Portland cement hydration: Comparison of methods, Cem. Conc. Res. 20(6), 919–926 (1990).
T. Voigt, C.U. Grosse, Z. Sun, S. P. Shah, H.-W. Reinhardt, Comparison of ultrasonic wave transmission and reflection measurements with P- and S-waves on early age mortar and concrete, Mat. Struct. 38 (282), 729–738 (2004).
T. C. Powers, Absorption of water by Portland cement paste during the hardening process. Ind. Eng. Chem. 27(7), 790–794 (1935).
W. Czernin, Cement chemistry and physics for civil engineers (Chemical Publishing Co., Inc, New York, 139 pp., 1962).
M. Geiker, T. Knudsen, Chemical shrinkage of Portland cement pastes, Cem. Con. Res. 12(5), 603–610 (1982).
E. Tazawa, S. Miyazawa, T. Kasai, Chemical shrinkage and autogenous shrinkage of hydrating cement paste, Cem. Con. Res. 25(2), 288–292 (1995).
S. Boivin, P. Acker, S. Rigaud, B. Clavaud, Experimental assessment of chemical shrinkage of hydrating cement pastes. In Tazawa, E. (Ed.), Autogenous shrinkage of concrete. Spon Press, Proceedings of the International Workshop organized by the JCI (Japan Concrete Institute), pp. 81–92 (1999).
Author information
Authors and Affiliations
Editor information
Editors and Affiliations
Rights and permissions
Copyright information
© 2006 Springer
About this paper
Cite this paper
Voigt, T., Shah, S.P. (2006). CHEMICAL SHRINKAGE AND CALCIUM HYDROXIDE CONTENT OF EARLY AGE PORTLAND CEMENT MONITORED WITH ULTRASONIC SHEAR WAVE REFLECTIONS. In: KONSTA-GDOUTOS, M.S. (eds) Measuring, Monitoring and Modeling Concrete Properties. Springer, Dordrecht. https://doi.org/10.1007/978-1-4020-5104-3_39
Download citation
DOI: https://doi.org/10.1007/978-1-4020-5104-3_39
Publisher Name: Springer, Dordrecht
Print ISBN: 978-1-4020-5103-6
Online ISBN: 978-1-4020-5104-3
eBook Packages: EngineeringEngineering (R0)