Skip to main content

Membrane Characterization

  • Chapter
  • First Online:
Book cover Carbon-based Membranes for Separation Processes

Abstract

In this chapter, typical examples of CMSM characterizations are shown. The characterization methods are classified into permeability measurement and physical characterization. Permeability measurement is further classified into gas and liquid permeabilities. Most of CMSMs have been characterized by gas permeation and separation, and many examples have already been shown in the preceding chapters. Therefore, only examples for characterization by liquid permeation experiments are included in this chapter. Physical characterization includes TGA, WAXD, SEM, TEM, AFM, FTIR and pore size measurement by adsorption. There are many other characterization methods, but the above methods have been most commonly used in the CMSM literature.

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Chapter
USD 29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD 129.00
Price excludes VAT (USA)
  • Available as EPUB and PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
USD 169.99
Price excludes VAT (USA)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info
Hardcover Book
USD 169.99
Price excludes VAT (USA)
  • Durable hardcover edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

References

  1. Strano MS, Zydney AL, Barth H, Wooler G, Agarwal H, Foley HC (2002) Ultrafiltration membrane synthesis by nanoscale templating of porous carbon. J Membr Sci 198 (2): 173-186

    Article  CAS  Google Scholar 

  2. Strano MS, Agarwal H, Pedrick J, Redman D, Foley HC (2003) Templated pyrolytic carbon: The effect of poly(ethylene glycol) molecular weight on the pore size distribution of poly(fufuryl alcohol)-derived carbon. Carbon 41 (13): 2501-2508

    Article  CAS  Google Scholar 

  3. Rajagopalan R, Merritt A, Tseytlin A, Foley HC (2006) Modification of macroporous stainless steel supports with silica sub-micron particles for size selective carbon membranes with improved flux. Carbon 44 (10): 2051-2058

    Article  CAS  Google Scholar 

  4. Merritt A, Rajagopalan R, Foley HC (2007) High performance nanoporous carbon membranes for air separation. Carbon 45 (6): 1267-1278

    Article  CAS  Google Scholar 

  5. Shah TN, Foley HC, Zydney AL (2007) Development and characterization of nanoporous carbon membranes for protein ultrafiltration. J Membr Sci 295 (1-2): 40-49

    Article  CAS  Google Scholar 

  6. Kim YY, Park HB, Lee YM (2004) Carbon molecular sieve membranes derived from thermally labile polymer containing blend polymers and their gas separation properties. J Membr Sci 243 (1-2): 9-14

    Article  CAS  Google Scholar 

  7. David LIB, Ismail AF (2003) Influence of the thermastabilization process and soak time during pyrolysis process on the polyacrylonitrile carbon membrane for O2/N2 separation. J Membr Sci 213 (1-2): 285-291

    Article  CAS  Google Scholar 

  8. Centeno TA, Fuertes AB (2000) Carbon molecular sieve gas separation membranes based on poly(vinylidene chloride-co-vinyl chloride). Carbon 38 (7): 1067-1073

    Article  CAS  Google Scholar 

  9. Xiao Y, Chung T-S, Guan HM, Guiver MD (2007) Synthesis, cross-linking and carbonization of co-polyamides containing internal acetylene units for gas separation. J Membr Sci 302 (1-2): 254-264

    Article  CAS  Google Scholar 

  10. Shiflett MB, Pedrick JF, McLean SR, Subramoney S, Foley HC (2006) Characterization of supported nanoporous carbon membranes. Adv Mater 12 (1): 21-25

    Article  Google Scholar 

  11. Linkov Y, Sanderson RD, Jacobs EP (1994) Scanning probe microscopy study of carbon membrane surfaces. J Mater Sci Lett 13 (8): 600-601

    Article  CAS  Google Scholar 

  12. Yoshimune M, Fujiwara I, Haraya K (2007) Carbon molecular sieve membranes derived from trimethylsilyl substituted poly(phenylene oxide) for gas separation. Carbon 45 (3): 553-560

    Article  CAS  Google Scholar 

  13. Nguyen C, Do DD, Haraya K, Wang K (2003) The structural characterization of carbon molecular sieve membrane (CMSM) via gas adsorption. J Membr Sci 220 (1-2): 177-182

    Article  CAS  Google Scholar 

  14. Nguyen C, Do DD (1999) Adsorption of supercritical gases in porous media: Determination of micropore size distribution. J Phys Chem B 103 (33): 6900-6908

    Article  CAS  Google Scholar 

  15. Katsaros FK, Steriotis TA, Ramanos GE, Konstantakou M, Stubos AK, Kanellopoulos NK (2007) Preparation and characterization of gas selective microporous carbon membranes. Microporous Mesoporous Mater 99 (1-2): 181-189

    Article  CAS  Google Scholar 

  16. Katsaros FK, Steriotis TA, Stefanopoulos KL, Kanellopoulos NK, Mitropoulos AC, Meissner M, Hoser A, (2000) Neutron diffraction study of adsorbed CO2 on a carbon membrane. Physica B 276-278: 901-902

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Ahmad Fauzi Ismail .

Rights and permissions

Reprints and permissions

Copyright information

© 2011 Springer Science+Business Media, LLC

About this chapter

Cite this chapter

Ismail, A.F., Rana, D., Matsuura, T., Foley, H.C. (2011). Membrane Characterization. In: Carbon-based Membranes for Separation Processes. Springer, New York, NY. https://doi.org/10.1007/978-0-387-78991-0_6

Download citation

Publish with us

Policies and ethics