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Fundamentals of Microscopy

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Abstract

Microscopy is the study of the fine structure and morphology of objects with the use of a microscope. Microscopes form magnified images, magnified from a few times in an optical stereo microscope to more than a million times in microscopes that can resolve individual atoms in suitable samples. Some instruments give information about a surface and not the specimen interior, but preparation methods can create an internal surface that may be imaged. Many modern microscopes are integrated with systems that give local chemical information, adding to the structural image. Apart from this, the size and visibility of the structure to be characterized generally determines which instruments are to be used. For example, the fracture of a multiphase polymer may require a light-optical technique for the ‘big picture’ but a study at higher resolution using electron microscopy and scanning probe microscopy to see fine details on the fracture surface.

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References

  1. M. Spencer, Fundamentals in Light Microscopy (Cambridge University Press, Cambridge, 1982).

    Google Scholar 

  2. D.J. Rawlins, Light Microscopy (BIOS Scientific Publishers, Oxford, 1992).

    Google Scholar 

  3. W.G. Hartley, Hartley’s Microscopy (Senecio Publishing, Charlbury, 1981).

    Google Scholar 

  4. S. Bradbury, An Introduction to the Optical Microscope (Oxford University Press, Oxford, 1984).

    Google Scholar 

  5. T.G. Rochow and P.A. Tucker, An Introduction to Microscopy by Means of Light, Electrons, X-rays, or Acoustics, 2nd ed. (Plenum, New York, 1994).

    Google Scholar 

  6. R. Telle and G. Petzow, in Materials Science and Technology, edited by E. Lifshin (VCH Publishers, Weinheim, 1993).

    Google Scholar 

  7. J.H. Richardson, Optical Microscopy for Materials Sciences (Marcel Dekker, New York, 1971).

    Google Scholar 

  8. C.W. Mason, Handbook of Chemical Microscopy (Wiley, New York, 1983).

    Google Scholar 

  9. N.H. Hartshorne and A. Stuart, Crystals and the Polarizing Microscope (Arnold, London, 1970).

    Google Scholar 

  10. P.C. Robinson and S. Bradbury, Qualitative Polarized-Light Microscopy (Oxford University Press, New York, 1992).

    Google Scholar 

  11. W.C. McCrone and J.G. Delly, Particle Atlas (Ann Arbor Science, Ann Arbor, MI, 1973).

    Google Scholar 

  12. D.B. Murphy, Fundamentals of Light Microscopy and Electronic Imaging (Wiley-Liss, Hoboken, NJ, 2001).

    Google Scholar 

  13. D.A. Hemsley, Ed. Applied Polymer Light Microscopy (Elsevier Applied Science, London, New York, 1989).

    Google Scholar 

  14. M.W. Davidson and M. Abramowitz, Optical Microscopy Primer. Available at http://micro.magnet.fsu.edu/primer/index.html. Accessed June 2006.

  15. Microscopy U: The Source for Microscopy Education. Available at http://www.microscopyu.com/. Accessed June 2006.

  16. Microscopy Resource Center. Available at http://www.olympusmicro.com/primer/index.html. Accessed June 2006.

  17. G.E. Schlueter and W.E. Gumpertz, Am. Lab. Apr (1976) 61.

    Google Scholar 

  18. M.W. Davidson and M. Abramowitz, Phase Contrast Microscopy. Available at http://micro.magnet.fsu.edu/primer/techniques/phasecontrast/phaseindex.html. Accessed June 2006.

  19. R. Hoffman, J. Microsc. 110 (1977) 209.

    Google Scholar 

  20. Principles and Applications of Two-Beam Interferometry. Available at http://www.microscopyu.com/articles/interferometry/twobeam.html. Accessed June 2006.

  21. Differential Interference Contrast. Available at http://www.microscopyu.com/articles/dic/dicindex.html. Accessed June 2006.

  22. Refractive Index Determination by Oblique Illumination. Available at http://www.olympusmicro.com/primer/java/oblique/becke/index.html. Accessed June 2006.

  23. E1976–98 Standard Test Method for the Automated Determinaton of Refractive Index of Glass Samples Using the Oil Immersion Method and a Phase Contrast Microscope, in ASTM Annual Books of Standards (ASTM International, 2003).

    Google Scholar 

  24. E.A. Wood, Crystals and Light (Dover, New York, 1977).

    Google Scholar 

  25. Introduction to Polarized Light Microscopy. Available at http://www.microscopyu.com/articles/polarized/polarizedintro.html. Accessed June 2006.

  26. P. Gay, An Introduction to Crystal Optics (Longmans, London, 1967).

    Google Scholar 

  27. N.H. Hartshorne, The Microscopy of Liquid Crystals (Microscope Publications, Chicago, 1974).

    Google Scholar 

  28. P.F. Kerr, Optical Mineralogy (McGraw-Hill, New York, 1959).

    Google Scholar 

  29. R. Oldenbourg, Nature 381 (1996) 811.

    PubMed  ADS  CAS  Google Scholar 

  30. J. Goldstein, D.E. Newbury, D.C. Joy, C.E. Lyman, P. Echlin, E. Lifshin, L.C. Sawyer and J.R. Michael, Scanning Electron Microscopy and X-ray Microanalysis, 3rd ed. (Plenum, New York, 2003).

    Google Scholar 

  31. S.L. Flegler, J.W. Heckman and K.L. Klomparens, Scanning and Transmission Electron Microscopy: An Introduction (Oxford University Press, Oxford, 1993).

    Google Scholar 

  32. L. Reimer, Image Formation in Low-Voltage Scanning Electron Microscopy (SPIE, Bellingham, WA, 1993).

    Google Scholar 

  33. L. Reimer and P.W. Hawkes, Eds. Scanning Electron Microscopy, Physics of Image Formation and Microanalysis (Springer, Berlin, 1998).

    Google Scholar 

  34. J.R. White and E.L. Thomas, Rubber Chem. Technol. 57 (1984) 457.

    CAS  Google Scholar 

  35. L.C. Sawyer and D.T. Grubb, Polymer Microscopy (Chapman and Hall, London, 1987, 1996).

    Google Scholar 

  36. C.J. Catto and K.C. Smith, J. Microsc. 98 (1973) 417.

    Google Scholar 

  37. Obtained using CASINO, Monte Carlo simulation software freely downloadable from [38], a site at Universitede Sherbrooke, Sherbrooke, Quebec, Canada.

    Google Scholar 

  38. D. Drouin, CASINO. http://www.gel.usherbrooke.ca/casino/. Accessed July 2006.

  39. T.E. Everhart, R.F. Herzog, M.S. Chang and W.J. DeVore. In Proc. 6th Intl. Conf. on X-ray Optics and Microanalysis, edited by G. Shinoda, K. Kohra and T. Ichinokawa (University of Tokyo, Tokyo, 1972), p. 81.

    Google Scholar 

  40. V.N.E. Robinson, Scanning 3 (1980) 15.

    CAS  Google Scholar 

  41. R. Autrata, Scanning Microsc. 3 (1989) 739.

    CAS  Google Scholar 

  42. E.D. Boyes, Microsc. Microanal. 6 (2000) 307.

    PubMed  ADS  CAS  Google Scholar 

  43. C. Gaillard, P.A. Stadelmann, C.J.G. Plummer and G. Fuchs, Scanning 26 (2004) 122.

    PubMed  CAS  Google Scholar 

  44. D.L. Vezie, W.W. Adams and E.L. Thomas, Polymer 36 (1995) 1761.

    CAS  Google Scholar 

  45. T. Tagawa, J. Mori, S. Aita and K. Ogura, Micron 9 (1978) 215.

    Google Scholar 

  46. D.W. Schwark, D.L. Vezie, J.R. Reffner, E.L. Thomas and B.K. Annis, J. Mater. Sci. Lett. 11 (1992) 352.

    CAS  Google Scholar 

  47. L.C. Sawyer, R.T. Chen, M.G. Jamieson, I.H. Musselman and P.E. Russell, J. Mater. Sci. 28 (1993) 225.

    CAS  Google Scholar 

  48. S.K. Chapman, Scanning Microsc. 13 (1999) 141.

    Google Scholar 

  49. A Guide to Scanning Microscope Observation. Available at http://www.jeolusa.com/sem/docs/sem_guide/guide.pdf. Accessed June 2006.

  50. D.B. Williams and C.B. Carter, Transmission Electron Microscopy: A Textbook for Materials Science (Plenum Press, New York, 1996).

    Google Scholar 

  51. L. Reimer, Transmission Electron Microscopy: Physics of Image Formation and Microanalysis (Springer, Berlin, 1997).

    Google Scholar 

  52. M.D. Graef, Introduction to Conventional Transmission Electron Microscopy (Cambridge University Press, Cambridge, 2003).

    Google Scholar 

  53. B. Fultz and J.M. Howe, Transmission Electron Microscopy and Diffractometry of Materials, 2nd Ed. (Springer, New York, 2002).

    Google Scholar 

  54. R.G. Vadimsky, in Methods of Experimental Physics, edited by R.A. Fava (Academic Press, New York, 1980).

    Google Scholar 

  55. D.T. Grubb, in Developments in Crystalline Polymers, edited by D.C. Bassett (Applied Science Publishers, London, 1982).

    Google Scholar 

  56. C.E. Hall, J. Appl. Phys. 22 (1951) 655.

    ADS  Google Scholar 

  57. B.D. Lauterwasser and E.J. Kramer, Philos. Mag. A39 (1979) 469.

    ADS  CAS  Google Scholar 

  58. P.B. Hirsch, A. Howie, R.B. Nicholson, D.W. Pashley and M.J. Whelan, Electron Microscopy of Thin Crystals (Butterworths, London, 1965).

    Google Scholar 

  59. E.L. Thomas, in The Structure of Crystalline Polymers, edited by I.H. Hall. (Elsevier Applied Science, London, 1984), p. 79.

    Google Scholar 

  60. J.R. White, J. Mater. Sci. 9 (1974) 1860.

    CAS  Google Scholar 

  61. M. Tosaka, R. Danev and K. Nagayama, Macromolecules 38 (2005) 7884.

    CAS  Google Scholar 

  62. M.J. Miles and J. Petermann, J. Macromol. Sci. Phys. 2 (1979) 243.

    Google Scholar 

  63. H.P. Zingsheim and L. Bachmann, Koll. Z. u Z. Polym. 246 (1971) 36.

    Google Scholar 

  64. D.J. Johnson and D. Crawford, J. Microsc. 98 (1973) 313.

    Google Scholar 

  65. D.L. Handlin and E.L. Thomas, Macromolecules 16 (1983) 1514.

    CAS  Google Scholar 

  66. L.W. Hobbs, Ultramicroscopy 23 (1987) 339.

    CAS  Google Scholar 

  67. V.E. Cosslett, Phys. Status Solidi 55 (1979) 545.

    CAS  Google Scholar 

  68. P. Goodman, Fifty Years of Electron Diffraction (Riedel, Dordrecht, 1981).

    Google Scholar 

  69. P.E. Champness, Electron Diffraction in the Transmission Electron Microscope (BIOS Scientific Publishers, Oxford, 2001).

    Google Scholar 

  70. D.L. Dorset, Structural Electron Crystallography (Springer, New York, 1995).

    Google Scholar 

  71. P. Buseck, J. Cowley and L. Eyring, Eds. High-Resolution Transmission Electron Microscopy and Associated Techniques (Oxford University Press, Oxford, 1988).

    Google Scholar 

  72. J.C.H. Spence, High-Resolution Electron Microscopy, 3rd ed. (Oxford University Press, Oxford, 2003).

    Google Scholar 

  73. F. Ernst and M. Rühle, Eds. High-Resolution Imaging and Spectrometry of Materials (Springer, New York, 2003).

    Google Scholar 

  74. D.C. Martin and E.L. Thomas, Polymer 36 (1995) 1743.

    CAS  Google Scholar 

  75. M. Tsuji and S. Kohjiya, Prog. Polym. Sci. 20 (1995) 259.

    CAS  Google Scholar 

  76. D.C. Martin, J. Chen, J. Yang, L.F. Drummy and C. Kübel, J. Polym. Sci. B Polym. Phys. 43 (2005) 1749.

    CAS  Google Scholar 

  77. C.J.G. Plummer, R. Gensler and H.-H. Kausch, Colloid Polym. Sci. 275 (1997) 1068.

    CAS  Google Scholar 

  78. M. Tsuji, M. Fujita, T. Shimizu and S. Kohjiya, Macromolecules 34 (2001) 4827.

    CAS  Google Scholar 

  79. M. Tosaka, M. Tsuji, S. Kohjiya, L. Cartier and B. Lotz, Macromolecules 32 (1999) 4905.

    CAS  Google Scholar 

  80. M.G. Dobb, A.M. Hindeleh, D.J. Johnson and B.P. Saville, Nature 253 (1975) 189.

    ADS  CAS  Google Scholar 

  81. C. Kübel, D.P. Lawrence and D.C. Martin, Macromolecules 34 (2001) 9053.

    Google Scholar 

  82. K. Shimamura, J.R. Minter and E.L. Thomas, J. Mater. Sci. Lett. 18 (1983) 54.

    Google Scholar 

  83. W.W. Adams, S. Kumar, D.C. Martin and K. Shimamura, Polym. Commun. 30 (1989) 285.

    CAS  Google Scholar 

  84. D.C. Martin and E.L. Thomas, Macromolecules 24 (1991) 2460.

    Google Scholar 

  85. D.C. Martin and E.L. Thomas, J. Mater. Sci. 26 (1991) 5171.

    CAS  Google Scholar 

  86. I.G. Voigt-Martin and H. Durst, Macromolecules 22 (1989) 186.

    Google Scholar 

  87. I.G. Voigt-Martin, H. Krug and D.V. Dyck, J. Phys., Paris 51 (1990) 2347.

    CAS  Google Scholar 

  88. D.C. Martin, L.L. Berger and K.H. Gardner, Macromolecules 24 (1991) 3921.

    CAS  Google Scholar 

  89. G. Binnig, H. Rohrer, C. Gerber and H. Weibel, Phys. Rev. Lett. 49 (1982) 57.

    ADS  Google Scholar 

  90. S. Magonov and M.-H. Whangbo, Surface Analysis with STM and AFM: Experimental and Theoretical Aspects of Image Analysis (VCH, Weinheim, 1996).

    Google Scholar 

  91. E. Meyer, H. Hug and R. Bennewitz, Scanning Probe Microscopy: The Lab on a Tip (Springer-Verlag, Berlin, Heidelberg, 2004).

    Google Scholar 

  92. R. Wiessendanger, Scanning Probe Microscopy and Spectroscopy: Methods and Applications (Cambridge University Press, Cambridge, 1994).

    Google Scholar 

  93. L.A. Bottomley, Anal. Chem. 70 (1998) 425R.

    CAS  Google Scholar 

  94. R. Overney and V. Tsukruk, in Scanning Probe Microscopy of Polymers, edited by B. Ratner and V. Tsukruk (ACS, Washington, DC, 1998), p. 2.

    Google Scholar 

  95. B.D. Ratner and V.V. Tsukruk, Eds. Scanning Probe Microscopy of Polymers. ACS Symp. Ser. Vol 694 (ACS, Washington DC, 1998).

    Google Scholar 

  96. S.N. Magonov and D.H. Reneker, Ann. Rev. Mater. Sci. 27 (1997) 175.

    CAS  Google Scholar 

  97. G. Krausch, Spec. Publ. Roy. Soc. Chem. 263 (2001) 291.

    CAS  Google Scholar 

  98. S.N. Magonov, in Handbook of Surfaces and Interfaces of Materials 2, edited by H.S. Nalwa (Academic Press, San Diego, 2001), p. 393.

    Google Scholar 

  99. D.A. Chernoff and S.N. Magonov, in Comprehensive Desk Reference of Polymer Characterization and Analysis, edited by R.F. Brady (ACS, Oxford Press, 2003), p. 490.

    Google Scholar 

  100. V.V. Tsukruk and N.D. Spencer, Eds. Recent Advances in Scanning Probe Microscopy of Polymers (Proc. Symp. August 2000), in Macromol. Symp. 167 (2001).

    Google Scholar 

  101. J.D. Batteas, C.A. Michaels and G.C. Walker, Eds. Applications of Scanned Probe Microscopy to Polymers ACS Symp. Ser. 897 (ACS, Washington DC, 2005).

    Google Scholar 

  102. D. Sarid, Scanning Force Microscopy: With Applications to Electric, Magnetic, and Atomic Forces (Oxford University Press, Oxford, 1994).

    Google Scholar 

  103. R. Garcia and R. Perez, Surface Science Reports 47 (2002) 197.

    MATH  ADS  CAS  Google Scholar 

  104. A. Schirmeisen, B. Anczykowski and H. Fuchs, in Applied Scanning Probe Methods, edited by B. Bushan, H. Fuchs and S. Hosaka (Springer-Verlag, Berlin, 2003), p. 3.

    Google Scholar 

  105. F.J. Giessibl, Rev. Mod. Phys. 75 (2003) 949.

    ADS  CAS  Google Scholar 

  106. J.S. Villarrubia, in Applied Scanning Probe Methods, edited by B. Bushan, H. Fuchs and S. Hosaka, (Springer-Verlag, Berlin, 2003), p. 147.

    Google Scholar 

  107. D.H. Reneker, R. Patil, S.J. Kim and V. Tsukruk, in Crystallization of Polymers, NATO ASI Series, Vol 405, edited by M. Dosière, (Kluwer, Dordrecht, 1993), p. 357.

    Google Scholar 

  108. B. Lotz, J.C. Wittmann and A.J. Lovinger, Polymer 37 (1996) 4979.

    CAS  Google Scholar 

  109. B. Lotz, Adv. Polym. Sci. 180 (2005) 17.

    CAS  Google Scholar 

  110. J.K. Hobbs, A.K. Winkel, T.J. McMaster, A.D.L. Humphris, A.A. Baker, S. Blakely, M. Aissaoui and M.J. Miles, Macromol. Symp. 167 (2001) 1.

    CAS  Google Scholar 

  111. S.N. Magonov and N.A. Yerina, in Handbook of Microscopy for Nanotechnology, edited by N. Yao and Z.L. Wang (Springer, 2005), p. 113.

    Google Scholar 

  112. S.N. Magonov and Y. Godovsky, American Laboratory 30 (1998) 15.

    CAS  Google Scholar 

  113. D.A. Ivanov and S.N. Magonov, in Polymer Crystallization: Observations, Concepts and Interpretations, edited by J.-U. Sommer and G. Reiter (Springer, New York, 2003).

    Google Scholar 

  114. C.-M. Chan and L. Li, Adv. Polym. Sci. 188 (2005) 1.

    CAS  Google Scholar 

  115. W.P. King and K.E. Goodson, Developments in Heat Transfer 13 (2004) 131.

    CAS  Google Scholar 

  116. D.M. Price, M. Reading and T.J. Lever, J. Therm. Anal. Calorimetry 56 (1999) 673.

    CAS  Google Scholar 

  117. B. Wunderlich, Polym. Mater. Sci. Eng. 81 (1999) 242.

    CAS  Google Scholar 

  118. H.M. Pollock and A. Hammiche, J. Phys. D Appl. Phys. 34 (2001) R23.

    ADS  CAS  Google Scholar 

  119. M.J. Abad, A. Ares, J. Cano, F.J. Diez, J. Lopez, C. Ramirez and L. Barral, Recent Res. Dev. Appl. Polym. Sci. 1 (2002) 221.

    CAS  Google Scholar 

  120. M.R. VanLandingham, J.S. Villarrubia, W.F. Guthrie and G.F. Meyers, Macromol. Symp. 167 (2001) 15.

    CAS  Google Scholar 

  121. V. Tsukruk and V. Gorbunov, Probe Microsc. 2 (2002) 241.

    Google Scholar 

  122. G.H. Michler, J. Macromol. Sci., Phys. B40 (2001) 277.

    CAS  Google Scholar 

  123. T. Hugel and M. Seitz, Macromol. Rapid Commun. 22 (2001) 989.

    CAS  Google Scholar 

  124. B. Bushan, in Applied Scanned Probe Methods, edited by B. Bushan, H. Fuchs and S. Hosaka (Springer-Verlag, Berlin, Heidelberg, 2004), p. 171.

    Google Scholar 

  125. C.M. Mate, IBM J. Res. Dev. 39 (1995) 617.

    CAS  Google Scholar 

  126. J.A. Zasadzinski, Curr. Opin. Colloid Interface Sci. 1 (1996) 264.

    CAS  Google Scholar 

  127. K. Feldman, M. Fritz, G. Hahner, A. Marti and N.D. Spencer, Tribol. Int. 31 (1998) 99.

    CAS  Google Scholar 

  128. D. Vezenov, A. Noy and P. Ashby, J. Adhes. Sci. Technol. 19 (2005) 313.

    CAS  Google Scholar 

  129. G.J. Vancso, H. Hillborg and H. Schoenherr, Adv. Polym. Sci. 182 (2005) 55.

    CAS  Google Scholar 

  130. M.C. Goh, Adv. Chem. Phys. 91 (1995) 1.

    CAS  Google Scholar 

  131. V.V. Tsukruk and D.H. Reneker, Polymer 36 (1995) 1791.

    CAS  Google Scholar 

  132. J.L. Keddie, Mater. Sci. Eng. R R21 (1997) 101.

    CAS  Google Scholar 

  133. D.C. Sundberg and Y.G. Durant, Polym. Reaction Eng. 11 (2003) 379.

    CAS  Google Scholar 

  134. J. Li, W. Liang, G.F. Meyers and W.A. Heeschen, Polym. News 29 (2004) 335.

    CAS  Google Scholar 

  135. S.E. Woodcock, W.C. Johnson and Z. Chen, Polym. News 29 (2004) 176.

    CAS  Google Scholar 

  136. J.-K. Kim and A. Hodzic, J. Adhesion 79 (2003) 383.

    CAS  Google Scholar 

  137. M. Munz, B. Cappella, H. Sturm, M. Geuss and E. Schulz, Adv. Polym. Sci. 164 (2003) 87.

    CAS  Google Scholar 

  138. G.K. Bar and G.F. Meyers, MRS Bull. 29 (2004) 464.

    CAS  Google Scholar 

  139. J. Teetsov, L. Denault, A. Alizadeh, S. Ghanti, W. Cicha and E. Hall, Annual Technical Conference —Society of Plastics Engineers 62nd (2004) 2357.

    CAS  Google Scholar 

  140. F.M. Mirabella, Jr. and A. Weiskettel, Polym. News 30 (2005) 143.

    CAS  Google Scholar 

  141. G. Binnig, C.F. Quate and C. Gerber, Phys. Rev. Lett. 56 (1986) 930.

    PubMed  ADS  Google Scholar 

  142. O. Marti, J. Colchero and J. Mlynek, Nanotechnology 1 (1990), 141.

    ADS  Google Scholar 

  143. G. Neubauer, S.R. Cohen, G.M. McClelland, D. Horne and C.M. Mate, Rev. Sci. Instrum. 61 (1990) 2296.

    ADS  CAS  Google Scholar 

  144. M. Radmacher, R.W. Tillmann and H.E. Gaub, Biophys. J. 64 (1993) 735.

    CAS  Google Scholar 

  145. H.-N. Lin, T.-T. Hung, E.-C. Chang and S.-A. Chen, Appl. Phys. Lett. 74 (1999) 2785.

    ADS  CAS  Google Scholar 

  146. A. Majumdar, J.P. Carrejo and J. Lai, Appl. Phys. Lett. 62 (1993) 2501.

    ADS  CAS  Google Scholar 

  147. F. Houze, R. Meyer, O. Schneegans and L. Boyer, Appl. Phys. Lett. 69 (1996) 1975.

    ADS  CAS  Google Scholar 

  148. R.C. Barrett and C.F. Quate, J. Appl. Phys. 70 (1991) 2725.

    ADS  CAS  Google Scholar 

  149. J. Loos, A. Alexeev and M.M. Koetse, Ultramicroscopy 106 (2006) 191.

    PubMed  Google Scholar 

  150. M. Knite, V. Teteris, B. Polyakov and D. Erts, Mater. Sci. Eng. C C19 (2002) 15.

    CAS  Google Scholar 

  151. S.-H. Cho and S.-M. Park. 208th Meeting of The Electrochemical Society, Oct. 16–21 2005, ECS, Los Angeles, (2005), p. 2548.

    Google Scholar 

  152. Q. Zhong, D. Innis, K. Kjoller and V. Elings, Surf. Sci. Lett. 290 (1993), L688.

    CAS  Google Scholar 

  153. D.A. Chernoff, in Proc. JMSA Proceedings Microscopy and MicroAnalysis 1995, edited by G.W. Bailey et al. (Jones and Begell, New York, 1995), p. 888.

    Google Scholar 

  154. Y. Martin and H.K. Wickramasinghe, Appl. Phys. Lett. 50 (1987) 1455.

    ADS  Google Scholar 

  155. Y. Martin, D.W. Abraham and H.K. Wickramasinghe, Appl. Phys. Lett. 52 (1988) 1103.

    ADS  Google Scholar 

  156. A.V. Krayev and R.V. Talroze, Polymer 45 (2004) 8195.

    CAS  Google Scholar 

  157. E. Schulz, H. Sturm, W. Stark and V. Bovtoun. Proceedings of the 1996 IEEE 9th International Symposium on Electrets, ISE 9, Sep. 25–27 1996, Shanghai, China, (IEEE, New York, 1996), p. 334

    Google Scholar 

  158. T.R. Albrecht, S. Akamine, T.E. Carver and C.F. Quate, J. Vac. Sci. Technol. A 6 (1990) 3386.

    ADS  Google Scholar 

  159. M. Nonnenmacher, J. Greschner, O. Wolter and R. Kassing, J. Vac. Sci. Technol. B 9 (1991) 1358.

    CAS  Google Scholar 

  160. Nanosciences, CNTekTM AFM Probes. Available at http://www.nanoscience.com/products/carbon_nanotube_probes.html. Accessed December 2006.

  161. Nanosciences, Hi’RES AFM Probes. Available at http://www.spmtips.com/products/cantilevers/datasheets/hi-res/. Accessed December 2006.

  162. D.A. Walters, D. Hampton, B. Drake, H.G. Hansma and P.K. Hansma, Appl. Phys. Lett. 65 (1994) 787.

    ADS  CAS  Google Scholar 

  163. A. Folch, M.S. Wrighton and M.A. Schmidt, J. Microelectromech. Systems 6 (1997) 303.

    CAS  Google Scholar 

  164. R.B. Marcus, T.S. Ravi, T. Gmitter, K. Chin, D. Liu, W.J. Orvis, D.R. Ciarlo, C.E. Hunt and J. Trujillo, Appl. Phys. Lett. 56 (1990) 236.

    ADS  CAS  Google Scholar 

  165. S.S. Wong, A.T. Woolley, T.W. Odom, J.-L. Huang, P. Kim, D.V. Vezenov and C.M. Lieber, Appl. Phys. Lett. 73 (1998) 3465.

    ADS  CAS  Google Scholar 

  166. J.H. Afner, C.-L. Cheung, A.T. Woolley and C.M. Lieber, Prog. Biophys. Mol. Biol. 77 (2001) 73.

    Google Scholar 

  167. D. Klinov and S. Magonov, Appl. Phys. Lett. 84 (2004) 2697.

    ADS  CAS  Google Scholar 

  168. M.S. Isaacson, in Principles and Techniques of Electron Microscopy, edited by M. Hayat (Van Nostrand, New York, 1977).

    Google Scholar 

  169. D.T. Grubb, J. Mater. Sci. 9 (1974) 1715.

    CAS  Google Scholar 

  170. G. Kanig, Koll. Z. u Z. Polym. 251 (1973) 176.

    Google Scholar 

  171. G. Kanig, J. Crystal Growth 48 (1980) 303.

    ADS  CAS  Google Scholar 

  172. D.C. Bassett and A.M. Hodge, Polymer 19 (1978) 469.

    CAS  Google Scholar 

  173. D.C. Bassett and A.M. Hodge, Proc. Roy. Soc. A377 (1981) 25.

    ADS  Google Scholar 

  174. D.C. Bassett, Crit. Rev.Solid State Mater Sci. 12 (1984) 97.

    CAS  Google Scholar 

  175. J.K. Hobbs, in Polymer Crystallization: Observations, Concepts and Interpretations, edited by J.-U. Sommer and G. Reiter (Springer, New York, 2003), p. 82.

    Google Scholar 

  176. L.C. Sawyer and M. Jaffe, J. Mater. Sci. 21 (1986) 1897.

    CAS  Google Scholar 

  177. R.C. Williams and H.W. Fischer, J. Mol. Biol. 52 (1970) 121.

    PubMed  CAS  Google Scholar 

  178. Y. Fujiyoshi, T. Kobayashi, K. Ishizuka, N. Uyeda, Y. Ishida and Y. Harada, Ultramicroscopy 5 (1980) 459.

    CAS  Google Scholar 

  179. J. Chang, M. Marsh, F. Rixon and W. Chiu, Microsc. Microanal. 11 (Suppl 2) (2005) 308.

    Google Scholar 

  180. K. Kobayashi and K. Sakaoku, Lab. Invest. 14 (1965) 1097.

    PubMed  CAS  Google Scholar 

  181. D.L. Dorset and F. Zemlin, Ultramicroscopy 17 (1985) 229.

    CAS  Google Scholar 

  182. J.G. Grasselli and B.J. Bulkin. Eds. Analytical Raman Spectroscopy (Wiley, New York, 1991).

    Google Scholar 

  183. A. Garton, D.N. Batchelder and C. Cheng, Appl. Spectrosc. 47 (1993) 922.

    ADS  CAS  Google Scholar 

  184. R.F. Egerton, Electron Energy Loss Spectroscopy in the Electron Microscope (Plenum Press, New York, 1986).

    Google Scholar 

  185. C.C. Ahn, Ed. Transmission Electron Energy Loss Spectrometry in Materials Science and The EELS Atlas (Wiley-VCH, 2004).

    Google Scholar 

  186. M.R. Libera and M.M. Disko, in Transmission Electron Energy Loss Spectrometry in Materials Science and The EELS Atlas, edited by C.C. Ahn (Wiley-VCH 2004), p. 419.

    Google Scholar 

  187. K.F.J. Heinrich and D.E. Newbury, Electron Probe Quantitation (Plenum Press, New York, 1991).

    Google Scholar 

  188. N.J. DiNardo, in Materials Science and Technology, edited by E. Lifshin, (VCH Publishers, Weinheim, 1994).

    Google Scholar 

  189. D.C. Joy, A.D. Romig and J.I. Goldstein, Principles of Analytical Electron Microscopy (Plenum, New York, 1986).

    Google Scholar 

  190. E.L. Hall, in Materials Science and Technology Vol 2A, edited by E. Lifshin (VCH Publishers, Weinheim, 1993).

    Google Scholar 

  191. J.C. Russ, Computer-Assisted Microscopy—The Measurement and Analysis of Images (Plenum Press, New York, 1990).

    Google Scholar 

  192. H.E. Exner, in Materials Science and Technology, edited by E. Lifshin (VCH Publishers, Weinheim, 1994).

    Google Scholar 

  193. D.P. Hader, Image Analysis: Methods and Applications, 2nd ed. (CRC Press, Boca Raton, 2002).

    Google Scholar 

  194. J.C. Russ, The Image Processing Handbook, 4th ed. (CRC Press, Boca Raton, 2002).

    Google Scholar 

  195. J.C. Russ and R.T. Dehoff, Practical Stereology, 2nd ed. (Springer, New York, 2000).

    Google Scholar 

  196. C.V. Howard and M.G. Reed, Unbiased Stereology (Advanced Methods), 2nd ed. (BIOS Scientific Publishers, Oxford, 2005).

    Google Scholar 

  197. J.K. Taylor and C. Cihon, Statistical Techniques for Data Analysis, 2nd ed. (Chapman & Hall/CRC, Boca Raton, 2004).

    MATH  Google Scholar 

  198. A.C. Tamhane and D.D. Dunlop, Statistics and Data Analysis: From Elementary to Intermediate (Prentice Hall, Englewood Cliffs, NJ, 1999).

    Google Scholar 

  199. N.A. Burnham, X. Chen, C.S. Hodges, G.A. Matei, C.J.T. Roberts, M.C. Davie and S.J.B. Tendler, Nanotechnology 14 (2003) 1.

    ADS  CAS  Google Scholar 

  200. J.P. Cleveland, I. Manne, D. Bocek and P.K. Hansma, Rev. Sci. Instrum. 64 (1993) 403.

    ADS  CAS  Google Scholar 

  201. C.T. Gibson, G.S. Watson and S. Myhra, Nanotechnology 7 (1996) 259.

    ADS  Google Scholar 

  202. J.R. Pratt, J.A. Kramar, D.B. Newell and D.T. Smith, Meas. Sci. Technol. 16 (2005) 2129.

    CAS  Google Scholar 

  203. M.A. Poggl, A.W. McFarland, J.S. Colton and L.A. Bottomley, Anal. Chem. 77 (2005) 1192.

    Google Scholar 

  204. J.E. Sader, J.W.M. Chon and P. Mulvaney, Rev. Sci. Instrum. 70 (1999) 3967.

    ADS  CAS  Google Scholar 

  205. J.L. Hutter and J. Bechhoefer, Rev. Sci. Instrum. 64 (1993) 1868.

    ADS  CAS  Google Scholar 

  206. J.E. Sader, J. Appl. Phys. 84 (1998) 64.

    ADS  CAS  Google Scholar 

  207. M.J. Higgins, R. Proksch, J.E. Sader, M. Polcik, S.M. Endoo, J.P. Cleveland and S.P. Jarvis, Rev. Sci. Instrum. 77 (2006) 13701.

    ADS  Google Scholar 

  208. E1813-96 Standard Practice for Measuring and Reporting Probe Tip Shape in Scanning Probe Microscopy, in ASTM Annual Books of Standards, Vol. 03.06 (ASTM International, 2002).

    Google Scholar 

  209. J.S. Villarrubia, J. Res. Natl. Inst. Stand. Technol. 102 (1997) 425.

    Google Scholar 

  210. K. Wetzig and D. Schulze, Eds. In Situ Scanning Electron Microscopy in Materials Research (Akademie Verlag, Berlin, 1995).

    Google Scholar 

  211. A.W. Agar, R.H. Alderson and D. Chescoe, Principles and Practice of Electron Microscope Operation, Vol 2 of Practical Methods in Electron Microscopy, edited by A.M. Glauert (North-Holland, Amsterdam, 1974).

    Google Scholar 

  212. E.P. Butler and K.F. Hale, Dynamic Experiments in the Electron Microscope, Vol 9 of Practical Methods in Electron Microscopy, edited by A.M. Glauert. (North-Holland, Amsterdam, 1981).

    Google Scholar 

  213. J.A. Reffner, Am., Lab. May (1984) 29.

    Google Scholar 

  214. A.M. Donald and B.L. Thiel, in Structure and Dynamics of Materials in the Mesoscopic Domain, Proceedings of the Royal Society-Unilever Indo-UK Forum in Materials Science and Engineering, edited by M. Lal (World Scientific, 1999), p. 1.

    Google Scholar 

  215. D.J. Stokes, J.-Y. Mugnier and C.J. Clarke, J. Microsc. 213 (2004) 198.

    PubMed  CAS  MathSciNet  Google Scholar 

  216. S. Kitching and A.M. Donald, J. Microsc. 190 (1998) 357.

    CAS  Google Scholar 

  217. P.J. James, T.J. McMaster, J.M. Newton and M.J. Miles, Polymer 41 (2000) 4223.

    CAS  Google Scholar 

  218. G.V. Lubarsky, M.R. Davidson and R.H. Bradley, Surf. Sci. 558 (2004) 135.

    ADS  CAS  Google Scholar 

  219. J.W.S. Hearle, J.T. Sparrow and P.M. Cross, The Use of the Scanning Electron Microscope (Pergamon, Oxford, 1972).

    Google Scholar 

  220. G.R. Loppnow and R.A. Mathis, Rev. Sci. Instrum. 66 (1989) 2628.

    ADS  Google Scholar 

  221. K.A. Taylor, R.A. Milligan, C. Raeburn and P.N.T. Unwin, Ultramicroscopy 13 (1984) 185.

    PubMed  CAS  Google Scholar 

  222. P.K. Vinson, J.R. Bellare, H.T. Davis, W.G. Miller and L.E. Scriven, J. Colloid Interface Sci. 142 (1992) 74.

    Google Scholar 

  223. M.S. Silverstein, Y. Talmon and M. Narkis, Polymer 30 (1989) 416.

    CAS  Google Scholar 

  224. N.H. Hartshorne, The Microscope 23 (1975) 177.

    CAS  Google Scholar 

  225. S. Rastogi, in Polymer Crystallization: Observations, Concepts and Interpretations, edited by J.-U. Sommer and G. Reiter (Springer, New York, 2003).

    Google Scholar 

  226. J.A. Moore and J.-H. Kim, Macromolecules 25 (1992) 1427.

    CAS  Google Scholar 

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© 2008 Linda C. Sawyer, David T. Grubb

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(2008). Fundamentals of Microscopy. In: Polymer Microscopy. Springer, New York, NY. https://doi.org/10.1007/978-0-387-72628-1_2

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