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Preparation of Layered Double Hydroxides

  • Jing He
  • Min Wei
  • Bo Li
  • Yu Kang
  • David G Evans
  • Xue DuanEmail author
Chapter
Part of the Structure and Bonding book series (STRUCTURE, volume 119)

Abstract

Layered double hydroxides (LDHs) comprise an extensive class of materials that are very easy to synthesize in the laboratory, albeit not always as pure phases. In this chapter, we review the wide variety of methods that are available for the synthesis of LDHs and focus on the way in which the physicochemical properties of the materials (such as phase purity, crystallinity and surface area) vary with synthesis method. The flexibility of the different methods is also discussed: some methods can be used to synthesize LDHs containing a wide range of constituent cations and anions, whilst others are more limited in scope. In some cases, the potential for scale-up of a method to produce larger quantities of material is also noted.

Layered double hydroxide Hydrotalcite Preparation LDH  

Abbreviations

CSC

4′-chloro-4-stilbenecarboxylic acid

DNA

Deoxyribonucleic acid

edta

Ethylenediamine tetraacetate

EG

Ethylene glycol

LDH

Layered double hydroxide

HTLc

Hydrotalcite-like compounds

ICTA

Indole-2-carboxylate

MAS

Magic angle spinning

NMR

Nuclear magnetic resonance

Phe

Phenylalanine

PXRD

Powder X-ray diffraction

SEM

Scanning electron microscope

TEM

Transmission electron microscope

THF

Tetrahydrofuran

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Authors and Affiliations

  • Jing He
    • 1
  • Min Wei
    • 1
  • Bo Li
    • 1
  • Yu Kang
    • 1
  • David G Evans
    • 1
  • Xue Duan
    • 1
    Email author
  1. 1.Ministry of Education Key Laboratory of Science and Technology of Controllable Chemical ReactionsBeijing University of Chemical TechnologyBeijingPeople's Republic of China

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