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Validation of an HPLC method for the determination of p-dichlorobenzene and naphthalene in mothrepellents

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Abstract

The determination of dichlorobenzene and naphthalene in commercial repellents used in Spain has been validated. This was done using an isocratic regime, to test the reverse -phase HPLC system with acetonitrile: water 65:35 (v: v) as the mobile phase, at 20 °C. This technique is proposed for the modular validation of the HPLC system. The results obtained with this method show good agreement with the results provided by the manufacturers of the mothrepellents.

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Author information

Authors and Affiliations

  1. Analytical Chemistry Department, University of Zaragoza, Crtra. Zaragoza, s/n, 22071, Huesca, Spain

    R.C. Díaz, M.A. Sarasa, C. Rios & J.J. Cuello

Authors
  1. R.C. Díaz
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  2. M.A. Sarasa
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  3. C. Rios
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  4. J.J. Cuello
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Editor information

Editors and Affiliations

  1. Duineneind 9, 2460, Kasterlee, Belgium

    Paul De Bièvre

  2. Bismarckstrasse 11, 69469, Weinheim, Germany

    Helmut Günzler

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© 1999 Springer-Verlag

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Díaz, R., Sarasa, M., Rios, C., Cuello, J. (1999). Validation of an HPLC method for the determination of p-dichlorobenzene and naphthalene in mothrepellents. In: De Bièvre, P., Günzler, H. (eds) Validation in Chemical Measurement. Springer, Berlin, Heidelberg. https://doi.org/10.1007/3-540-27034-5_15

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