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Solid State NMR of Porous Materials

Zeolites and Related Materials

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Solid State NMR

Part of the book series: Topics in Current Chemistry ((TOPCURRCHEM,volume 306))

Abstract

Solid state NMR spectroscopy applied to the science of crystalline micro- and mesoporous silica materials over the past 10 years is reviewed. A survey is provided of framework structure and connectivity analyses from chemical shift effects of various elements in zeolites including heteroatom substitutions, framework defects and pentacoordinated silicon for zeolites containing fluoride ions. New developments in the field of NMR crystallography are included. Spatial host–guest ordering and confinement effects of zeolite–sorbate complexes are outlined, with special emphasis on NMR applications utilizing the heteronuclear dipolar interaction. The characterization of zeolite acid sites and in situ NMR on catalytic conversions is also included. Finally, the motion of extra-framework cations is investigated in two tutorial cases of sodium hopping in sodalite and cancrinite.

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  1. Institute of Physical Chemistry, University of Münster, Corrensstr. 28/30, 48149, Münster, Germany

    Hubert Koller & Mark Weiß

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  1. Hubert Koller
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    Jerry C. C. Chan

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Koller, H., Weiß, M. (2011). Solid State NMR of Porous Materials. In: Chan, J. (eds) Solid State NMR. Topics in Current Chemistry, vol 306. Springer, Berlin, Heidelberg. https://doi.org/10.1007/128_2011_123

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