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Importance of in-situ EDXRF Measurements in the Preservation and Conservation of Material Culture

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X-rays for Archaeology

Abstract

The paper presents a series of in-situ Energy Dispersive X-ray Fluorescence (EDXRF) measurements performed in Greece and Cyprus for the characterization and quantitative analysis of valuable archaeological and historical artifacts, such as pigments on wall paintings and ceramics as well as gold and bronze alloys on sculpture and jewelry. The various types of instrumentation and analytical procedures used for the quantification of in-situ XRF data will be discussed. The experience acquired from the above investigations will be critically reviewed in order to assess the importance, as well as the limitations of in-situ EDXRF analyses in the preservation and conservation of our cultural heritage.

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References

  1. X-Ray Spectrometry, Vol. 29 (2000).

    Google Scholar 

  2. M. Mantler and M. Schreiner, I 29 (2000) 3

    Google Scholar 

  3. C. Neelmejer, I. Brissaud, T. Calligaro, G. Demortier, A. Hautojarvi, M. Mader, L. Martinot, M. Schreiner, T. Tuurnala and G. Weber, X-Ray Spectrometry 29 (2000) 101

    Article  Google Scholar 

  4. R. Cesareo, G. E. Gigante, A. Castellano, M. A. Rosales, M. Aliphat, F. DeLa Fuente, J. J. Meitin, A. Mendoza, J. S. Iwanczyk and J. A. Pantazis, J.Trace and Microprobe Techniques, 14 (1996) 711

    Google Scholar 

  5. Caruso, R. Cesareo, C. Giardino, G. E. Gigante, Supplement de La Revue d’ Archeomè trie (1996) 157

    Google Scholar 

  6. G. Vittiglio, K. Janssens, B. Vekemans, F. Adams, A. Oost, Spectrochimica Acta, B 54 (1999) 1697

    Article  Google Scholar 

  7. S. Sciuti, G. Fronterotta, M. Vendittelli, A. Longoni and C. Fiorini, Studies in Conservation, 46 (2001) 132

    Google Scholar 

  8. M. Uda, S. Sassa, K. Tanigushi, S. Nomura, S. Yoshimura, J. Kondo, N. Iskander, B. Zaglhloul, Naturwissenschaften 87 (2000) 260

    Article  Google Scholar 

  9. M. Uda, M. Nakamura, S. Yoshimura, J. Kondo, S. Sassa, M. Saita, Y. Shirai, S. Hasegawa, Y. Baba, K. Ikeda, Y. Ban, A. Matsuo, M. Tamada, H. Sunaga, H. Oshio, D. Yamashita, Y. Nakajima, T. Utaka, Nucl. Instr. Meth. B 189 (2002) 382

    Article  Google Scholar 

  10. K. Janssens, G. Vittiglio, I. Deraedt, A. Aerts, B. Vekemans, L. Vincze, F. Wei, I. Deryck, O. Schalm, F. Adams, A. Rindby, A. Knochel, A. Simionovici and A. Snigirev, X-Ray Spectrometry 29 (2000) 73

    Article  Google Scholar 

  11. R. Cesareo, G. E. Gigante, A. Castellano, Nucl. Instr. Meth. A428 (1999) 171

    Google Scholar 

  12. P. Leutenegger, A. Longoni, C. Fiorini, L. Struder, J. Kemmer, P. Lechner, S. Sciuti, R. Cesareo, Nucl. Instr. Meth. A, 439 (2000) 458

    Article  Google Scholar 

  13. J. A. Huber, J. A. Pantazis, V. Jordanov, Nucl. Instr. and Meth. B99 (1995) 665

    Google Scholar 

  14. R. Redus, J. Pantazis, A. Huber, T. Pantazis, IEEE Trans. Nucl. Sci., in press

    Google Scholar 

  15. L. Struder, N. Meidinger, D. Stotter, J. Kemmer, P. Lechner, P. Leutenegger, H. Soltau, F. Eggert, M. Rohde, and T. Schulein, Microsc. Microanal. 4 (1999) 622

    Google Scholar 

  16. A. G. Karydas, Ch. Zarkadas, A. Kyriakis, J. Pantazis, A. Huber, R. Redus C. Potiriadis, Th. Paradellis, X-Ray Spectrometry, in press

    Google Scholar 

  17. M. A. Kumakhov, X-Ray Spectrometry, 29 (2000) 343

    Article  Google Scholar 

  18. H. Ebel, X-ray Spectrometry, 28 (1999) 255

    Article  Google Scholar 

  19. H. Brecoulaki, V. Perdikatsis, “Ancient Painting on Macedonian Funerary Monuments, IV-III centuries BC: A comparative study on the use of color”, in Color in Ancient Greece, International Symposium, The J. Paul Getty Museum and the Aristotelian University of Thessaloniki, 12–16 April 2000, Thessaloniki, in press.

    Google Scholar 

  20. H. Brecoulaki, “Sur la techné de la peinture grecque ancienne d’après les monuments funéraires de Macédoine”, Bulletin de Correspondance Hellénique 124, 2000, p. 189–216.

    Google Scholar 

  21. Chr. Doumas, Proceedings of the first International symposium on The Wall Paintings of Thera, Vol. I, Athens 2000, p. 15–20

    Google Scholar 

  22. Philippakis, V. Perdikatsis, Th. Paradellis, Studies in Conservation 21 (1976) 143.

    Article  Google Scholar 

  23. S. Profi, V. Perdikatsis, S. Philippakis, Studies in Conservation 22 (1977) 107.

    Article  Google Scholar 

  24. V. Perdikatsis, La couleur Dans Peinture L’Emaillage De L’Egypte Ancienne, Centro Universitario Europeo, Bari, 1998 p. 103–108.

    Google Scholar 

  25. V. Perdikatsis, V. Kilikoglou, S. Sotiropoulou, E. Chryssikopoulou, Proceedings of the first International symposium on The Wall Paintings of Thera, Vol. I, Athens 2000, p. 103–118

    Google Scholar 

  26. T. Pantazis, A. G. Karydas, C. Doumas, A. Vlachopoulos, P. Nomikos, E. Thomson, C. Vecoli, M. Dinsmore, Proceedings of the 4th Int. Aegean Conf., Metron, Aegaeum 25 New Haven, USA, in press

    Google Scholar 

  27. E. Aloupi, A. G. Karydas and T. Paradellis, X-Ray Spectrometry, 29 (2000) 18

    Article  Google Scholar 

  28. P. Craddock, N. Meek’s, M. Cowell, A. Middleton, D. Hook, A. Ramage, E. Geckinli, Art of the Greek Goldsmith, 1998.

    Google Scholar 

  29. Y. Maniatis, A. G. Karydas, E. Mangou, Th. Paradellis, Ion beam study of art and archaeological objects, European Cooperation in the field of Scientific and Technical research”, EUR 19218, 2000, p. 110–116

    Google Scholar 

  30. A. Hartmann, Prahistorishe Goldfunde Aus Europa II, Gebr. Mann Verlag, 1982.

    Google Scholar 

  31. G. Demortier, Proceedings of the Materials Research Society Symposium, 1989, p. 193–198

    Google Scholar 

  32. R. Tylecote, The early history of metallurgy in Europe, 1987.

    Google Scholar 

  33. E. Aloupi, A. G. Karydas, P. Kokkinias, T. Paradellis, A. Lekka and V. Karageorgis, Non-destructive analysis and visual recording survey of the pottery collection in the Nicosia Museum, Cyprus in Archaeometry issues in Greek prehistory and antiquity, The Hellenic Society of Archaeometry (Eds. Y. Bassiakos, E. Aloupi, Y. Facorellis), Athens 2001, p. 397–410.

    Google Scholar 

  34. W. Noll, R. Holm, and L. Born, Painting of ancient ceramics, Angewandte Chemie, (Internat. edn.), 14(9), 1975, p. 602–613.

    Google Scholar 

  35. E. Aloupi, V. Perdikatsis and A. Lekka, Assessment of the White Slip classification slip based on physicochemical aspects of the technique, in White Slip Ware, ed. V. Karageorghis, The A.G. Leventis Foundation, Nicosia, 1999, p. 15–26

    Google Scholar 

  36. E. Aloupi, The nature of pigments in Bichrome wheel-made ware, KVHAA Konferenser 54:215–219. Stockholm 2001.

    Google Scholar 

  37. R. E. Jones, Greek and Cypriot Pottery, The British School at Athens, Fitch Laboratory OP1, 1986, p. 765, 808.

    Google Scholar 

  38. V. Argyropoulos, Z. Antonopoulou, A. G. Karydas, B. Perdikatsis, G. Economou, Proceedings of the 1st International Conference held in Rhodes “Vulnerabiltiy of 20th Century Heritage to Hazards and Prevention Measures”, in press

    Google Scholar 

  39. H. Strandberg, L-G. Johansson and O. Lindqvist, The Atmospheric corrosion of statue bronzes exposed to SO2 and NO2, Materials and Corrosion, 1997 p. 48

    Google Scholar 

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This paper is dedicated to the memory of Dr. Themis Paradellis, whose pioneering work on the application of EDXRF techniques in the study of Cultural Heritage in Greece inspired all co-authors in this article.

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Karydas, A. et al. (2005). Importance of in-situ EDXRF Measurements in the Preservation and Conservation of Material Culture. In: Uda, M., Demortier, G., Nakai, I. (eds) X-rays for Archaeology. Springer, Dordrecht. https://doi.org/10.1007/1-4020-3581-0_2

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