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Niob pp 232-275 | Cite as

Verbindungen mit Chlor

  • Herbert Lehl
Chapter
Part of the Nb. Niob. Niobium (System-Nr. 49) book series (GMELIN, volume N-b / B / 4)

Zusammenfassung

Wird analog dem K4Nb6Cl18 (s. S. 237) aus Nb3Cl8 (s. „Niob“ B 1, S. 159) und LiCl oder durch 6 d Glühen von wasserfreiem Nb6Cl14 (s. „Niob“ B 1, S. 152) mit überschüssigem LiCl bei etwa 800°C dargestellt, mit Äther gewaschen und getrocknet, Hughes u.a. [1]. Hauptabsorptionsmaxima im Elektronenspektrum (Bereich 4000 bis 50000 cm−1) von festem Li4Nb6C118 und dessen Lösungen in H2O, mit HCl gesättigtem Äthanol, Aceton, Nitromethan, Acetonitril und Dimethylsulfoxid s. bei Fleming, McCarley [2].

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© Springer-Verlag Berlin Heidelberg 1972

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  • Herbert Lehl

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