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3D 13C MAS NMR Experiment Correlating Order and Dynamics

  • Y. Yang
  • A. Hagemeyer
  • K. Zemke
  • H. W. Spiess
Conference paper

Abstract

The 2D exchange MAS NMR experiment for detecting ultraslow molecular dynamics and the rotor-synchronized 2D experiment for studying the degree of molecular orientation in partially ordered solids are combined into a rotor-synchronized 3D experiment, which correlates molecular order and dynamics. The experiment is outlined and demonstrated experimentally on highly oriented poly (oxymethylene), POM.

PACS numbers

76.60.Es 66.30.-h 61.41.e 

References

  1. 1.
    Y. Yang, A. Hagemeyer, H.W. Spiess, Macromolecules 22, 1004 (1989).ADSCrossRefGoogle Scholar

Copyright information

© Springer-Verlag Berlin Heidelberg 1990

Authors and Affiliations

  • Y. Yang
    • 1
    • 2
  • A. Hagemeyer
    • 1
  • K. Zemke
    • 1
  • H. W. Spiess
    • 1
  1. 1.Max-Planck-Institut für PolymerforschungMainzGermany
  2. 2.Inst.Mater.Sci.Fudan UniversityShanghaiP.R.C.

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